JP2011519806A5 - - Google Patents
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- Publication number
- JP2011519806A5 JP2011519806A5 JP2011504454A JP2011504454A JP2011519806A5 JP 2011519806 A5 JP2011519806 A5 JP 2011519806A5 JP 2011504454 A JP2011504454 A JP 2011504454A JP 2011504454 A JP2011504454 A JP 2011504454A JP 2011519806 A5 JP2011519806 A5 JP 2011519806A5
- Authority
- JP
- Japan
- Prior art keywords
- compound
- mixture
- feooh
- electrically conductive
- group
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 150000001875 compounds Chemical class 0.000 claims 26
- 238000000034 method Methods 0.000 claims 16
- 239000000203 mixture Substances 0.000 claims 14
- XEEYBQQBJWHFJM-UHFFFAOYSA-N iron Substances [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 claims 6
- 239000003638 chemical reducing agent Substances 0.000 claims 5
- 239000004020 conductor Substances 0.000 claims 5
- CIWBSHSKHKDKBQ-JLAZNSOCSA-N Ascorbic acid Chemical compound OC[C@H](O)[C@H]1OC(=O)C(O)=C1O CIWBSHSKHKDKBQ-JLAZNSOCSA-N 0.000 claims 4
- 125000004437 phosphorous atom Chemical group 0.000 claims 4
- 229910052698 phosphorus Inorganic materials 0.000 claims 4
- 239000007787 solid Substances 0.000 claims 4
- 239000012798 spherical particle Substances 0.000 claims 4
- 229910002588 FeOOH Inorganic materials 0.000 claims 3
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims 2
- 229910018119 Li 3 PO 4 Inorganic materials 0.000 claims 2
- WHXSMMKQMYFTQS-UHFFFAOYSA-N Lithium Chemical compound [Li] WHXSMMKQMYFTQS-UHFFFAOYSA-N 0.000 claims 2
- HBBGRARXTFLTSG-UHFFFAOYSA-N Lithium ion Chemical compound [Li+] HBBGRARXTFLTSG-UHFFFAOYSA-N 0.000 claims 2
- 229960005070 ascorbic acid Drugs 0.000 claims 2
- 235000010323 ascorbic acid Nutrition 0.000 claims 2
- 239000011668 ascorbic acid Substances 0.000 claims 2
- 238000001035 drying Methods 0.000 claims 2
- 229910052742 iron Inorganic materials 0.000 claims 2
- 229910052744 lithium Inorganic materials 0.000 claims 2
- 229910001416 lithium ion Inorganic materials 0.000 claims 2
- VNWKTOKETHGBQD-UHFFFAOYSA-N methane Chemical compound C VNWKTOKETHGBQD-UHFFFAOYSA-N 0.000 claims 2
- 235000000346 sugar Nutrition 0.000 claims 2
- 229920000049 Carbon (fiber) Polymers 0.000 claims 1
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims 1
- 150000001298 alcohols Chemical class 0.000 claims 1
- 239000006229 carbon black Substances 0.000 claims 1
- 239000004917 carbon fiber Substances 0.000 claims 1
- 239000002134 carbon nanofiber Substances 0.000 claims 1
- 239000002041 carbon nanotube Substances 0.000 claims 1
- 229910021393 carbon nanotube Inorganic materials 0.000 claims 1
- 229910052804 chromium Inorganic materials 0.000 claims 1
- 229920001940 conductive polymer Polymers 0.000 claims 1
- 235000019441 ethanol Nutrition 0.000 claims 1
- 238000010304 firing Methods 0.000 claims 1
- 229910002804 graphite Inorganic materials 0.000 claims 1
- 239000010439 graphite Substances 0.000 claims 1
- 229910052748 manganese Inorganic materials 0.000 claims 1
- 229910052759 nickel Inorganic materials 0.000 claims 1
- 230000003647 oxidation Effects 0.000 claims 1
- 238000007254 oxidation reaction Methods 0.000 claims 1
- 239000002243 precursor Substances 0.000 claims 1
- 238000001694 spray drying Methods 0.000 claims 1
- 150000008163 sugars Chemical class 0.000 claims 1
- 229910052720 vanadium Inorganic materials 0.000 claims 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims 1
- 229910006540 α-FeOOH Inorganic materials 0.000 claims 1
- 229910003153 β-FeOOH Inorganic materials 0.000 claims 1
- 229910006299 γ-FeOOH Inorganic materials 0.000 claims 1
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US4580208P | 2008-04-17 | 2008-04-17 | |
| US61/045,802 | 2008-04-17 | ||
| PCT/EP2009/054488 WO2009127674A1 (en) | 2008-04-17 | 2009-04-16 | Process for the preparation of crystalline lithium-, iron- and phosphate-comprising materials |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JP2011519806A JP2011519806A (ja) | 2011-07-14 |
| JP2011519806A5 true JP2011519806A5 (enExample) | 2012-06-14 |
Family
ID=40874939
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2011504454A Pending JP2011519806A (ja) | 2008-04-17 | 2009-04-16 | リチウム、鉄及びリン酸を含有する結晶性材料の製造方法 |
Country Status (8)
| Country | Link |
|---|---|
| US (2) | US20110049443A1 (enExample) |
| EP (1) | EP2285740B1 (enExample) |
| JP (1) | JP2011519806A (enExample) |
| KR (1) | KR101592049B1 (enExample) |
| CN (1) | CN102066241B (enExample) |
| CA (1) | CA2721029A1 (enExample) |
| TW (1) | TW201010944A (enExample) |
| WO (1) | WO2009127674A1 (enExample) |
Families Citing this family (20)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| KR101063214B1 (ko) * | 2008-11-28 | 2011-09-07 | 전자부품연구원 | 리튬이차전지용 구형 양극 활물질 제조방법 |
| TWI474970B (zh) | 2008-12-29 | 2015-03-01 | Basf Se | 於水熱條件下合成鋰－金屬－磷酸鹽 |
| TW201038469A (en) | 2009-03-17 | 2010-11-01 | Basf Se | Synthesis of lithium-iron-phosphates |
| KR101718972B1 (ko) | 2009-06-24 | 2017-03-23 | 바스프 에스이 | ＬｉＦｅＰＯ4-탄소 복합재의 제조 방법 |
| JP5729802B2 (ja) * | 2009-12-25 | 2015-06-03 | 三菱マテリアル株式会社 | Ｌｉイオン電池用正極活物質、およびその製造方法 |
| CN101989653B (zh) * | 2010-05-06 | 2012-10-31 | 黄兵 | 超微球颗粒连接的锂离子电池用球形正极材料及其制备方法 |
| FR2978137A1 (fr) * | 2011-07-21 | 2013-01-25 | Saint Gobain Ct Recherches | Produit fondu a base de lithium |
| FR2989378B1 (fr) | 2012-04-16 | 2015-10-02 | Commissariat Energie Atomique | Polymere comme materiau d'electrode pour des batteries secondaires au lithium. |
| WO2013185837A1 (en) * | 2012-06-15 | 2013-12-19 | MAX-PLANCK-Gesellschaft zur Förderung der Wissenschaften e.V. | Method of manufacture of an electrode material and an electrode material |
| US20140328729A1 (en) | 2013-05-06 | 2014-11-06 | Liang-Yuh Chen | Apparatus for Preparing a Material of a Battery Cell |
| WO2015030401A1 (ko) | 2013-08-28 | 2015-03-05 | 주식회사 엘지화학 | 리튬 전이금속 인산화물 입자를 포함하는 양극 활물질, 이의 제조방법, 및 이를 포함하는 리튬 이차전지 |
| FR3012450B1 (fr) | 2013-10-30 | 2017-10-13 | Commissariat Energie Atomique | Materiau d'electrode pour batterie organique |
| CN103647080A (zh) * | 2013-11-15 | 2014-03-19 | 成都兴能新材料有限公司 | 金属离子-LiFePO4-C复合材料的制备方法 |
| CN106684379B (zh) * | 2015-11-11 | 2019-05-10 | 中国科学院金属研究所 | 合成具有超高大倍率充放电性能的超薄纳米片状LiFePO4的方法 |
| JP7280722B2 (ja) * | 2019-03-15 | 2023-05-24 | 積水化学工業株式会社 | 非水電解質二次電池用正極及びリチウムイオン二次電池 |
| US11376559B2 (en) | 2019-06-28 | 2022-07-05 | eJoule, Inc. | Processing system and method for producing a particulate material |
| US11673112B2 (en) | 2020-06-28 | 2023-06-13 | eJoule, Inc. | System and process with assisted gas flow inside a reaction chamber |
| TWI785881B (zh) | 2019-06-28 | 2022-12-01 | 美商壹久公司 | 具有輔助氣體流的處理系統與方法及所製成用於電池的材料 |
| US11121354B2 (en) | 2019-06-28 | 2021-09-14 | eJoule, Inc. | System with power jet modules and method thereof |
| WO2024038136A1 (en) | 2022-08-18 | 2024-02-22 | Integrals Power | Improved cathode material for secondary lithium batteries |
Family Cites Families (34)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5910382A (en) * | 1996-04-23 | 1999-06-08 | Board Of Regents, University Of Texas Systems | Cathode materials for secondary (rechargeable) lithium batteries |
| US6514640B1 (en) * | 1996-04-23 | 2003-02-04 | Board Of Regents, The University Of Texas System | Cathode materials for secondary (rechargeable) lithium batteries |
| US20020192137A1 (en) * | 2001-04-30 | 2002-12-19 | Benjamin Chaloner-Gill | Phosphate powder compositions and methods for forming particles with complex anions |
| CA2270771A1 (fr) * | 1999-04-30 | 2000-10-30 | Hydro-Quebec | Nouveaux materiaux d'electrode presentant une conductivite de surface elevee |
| US6528033B1 (en) * | 2000-01-18 | 2003-03-04 | Valence Technology, Inc. | Method of making lithium-containing materials |
| CA2320661A1 (fr) * | 2000-09-26 | 2002-03-26 | Hydro-Quebec | Nouveau procede de synthese de materiaux limpo4 a structure olivine |
| EP1261050A1 (en) * | 2001-05-23 | 2002-11-27 | n.v. Umicore s.a. | Lithium transition-metal phosphate powder for rechargeable batteries |
| US6913855B2 (en) * | 2002-07-22 | 2005-07-05 | Valence Technology, Inc. | Method of synthesizing electrochemically active materials from a slurry of precursors |
| FR2848205B1 (fr) * | 2002-12-05 | 2006-03-24 | Commissariat Energie Atomique | Composes d'insertion du lithium substitues au bore, materiaux actifs d'electrodes, accumulateurs et dispositifs electrochromes |
| FR2852148B1 (fr) | 2003-03-07 | 2014-04-11 | Batscap Sa | Materiau pour electrode composite, procede pour sa preparation |
| JP4483253B2 (ja) | 2003-09-30 | 2010-06-16 | 三菱化学株式会社 | リチウム二次電池用正極材料、リチウム二次電池用正極及びリチウム二次電池 |
| JP4522682B2 (ja) * | 2003-10-09 | 2010-08-11 | 住友大阪セメント株式会社 | 電極材料粉体の製造方法と電極材料粉体及び電極並びにリチウム電池 |
| CN1233054C (zh) | 2003-12-17 | 2005-12-21 | 北京科技大学 | 一种采用微波法制备LiFePO4材料的方法 |
| JP2007230784A (ja) | 2004-03-30 | 2007-09-13 | Agc Seimi Chemical Co Ltd | リチウム鉄複合酸化物の製造方法 |
| JP2006155941A (ja) * | 2004-11-25 | 2006-06-15 | Kyushu Univ | 電極活物質の製造方法 |
| DE102005012640B4 (de) | 2005-03-18 | 2015-02-05 | Süd-Chemie Ip Gmbh & Co. Kg | Kreisprozess zur nasschemischen Herstellung von Lithiummetallphosphaten |
| EP1875542B1 (en) | 2005-04-05 | 2010-05-19 | Byd Company Limited | Flow-field plate and fuel cell stack using the same |
| DE102005015613A1 (de) | 2005-04-05 | 2006-10-12 | Süd-Chemie AG | Kristallines Ionenleitendes Nanomaterial und Verfahren zu seiner Herstellung |
| US8062792B2 (en) * | 2005-04-26 | 2011-11-22 | Uchicago Argonne Llc | Processes for making dense, spherical active materials for lithium-ion cells |
| JP4869629B2 (ja) * | 2005-05-30 | 2012-02-08 | 住友大阪セメント株式会社 | リチウム電池用正極活物質の製造方法及びリチウム電池用正極活物質並びにリチウム電池 |
| JP4804045B2 (ja) * | 2005-06-15 | 2011-10-26 | Ａｇｃセイミケミカル株式会社 | リチウム鉄複合酸化物の製造方法 |
| CN100420076C (zh) * | 2005-12-19 | 2008-09-17 | 南开大学 | 溶胶凝胶法合成锂离子电池正极材料磷酸钒锂的方法 |
| KR100940979B1 (ko) * | 2006-05-08 | 2010-02-05 | 주식회사 엘지화학 | ＬｉＦｅＰ０４의 제조방법 |
| JP5216960B2 (ja) * | 2006-12-26 | 2013-06-19 | 日立マクセル株式会社 | リチウムイオン二次電池用正極活物質 |
| CA2684119A1 (en) * | 2007-04-16 | 2008-10-23 | Basf Se | Process for preparing lithium-rich metal oxides |
| JP5293936B2 (ja) * | 2007-05-21 | 2013-09-18 | 戸田工業株式会社 | 非水電解質二次電池用オリビン型複合酸化物及びその製造方法、並びに二次電池 |
| CN102123943B (zh) * | 2007-10-01 | 2013-07-10 | 巴斯夫欧洲公司 | 制备包含锂、钒和磷酸根的多孔材料的方法 |
| KR101519686B1 (ko) * | 2007-10-01 | 2015-05-12 | 바스프 에스이 | 결정질 리튬, 바나듐 및 포스페이트 함유 물질의 제조 방법 |
| WO2009122686A1 (ja) * | 2008-03-31 | 2009-10-08 | 戸田工業株式会社 | リン酸鉄リチウム粒子粉末の製造方法、オリビン型構造のリン酸鉄リチウム粒子粉末、該リン酸鉄リチウム粒子粉末を用いた正極材シート及び非水溶媒系二次電池 |
| JP5517032B2 (ja) * | 2008-03-31 | 2014-06-11 | 戸田工業株式会社 | 非水電解質二次電池用オリビン型複合酸化物粒子粉末及びその製造方法、並びに二次電池 |
| TW200951066A (en) * | 2008-04-17 | 2009-12-16 | Basf Se | Process for the preparation of crystalline lithium-, iron-and phosphate-comprising materials |
| TWI440597B (zh) * | 2008-08-26 | 2014-06-11 | Basf Se | 於水熱條件下合成ＬｉＦｅＰＯ4 |
| TWI474970B (zh) * | 2008-12-29 | 2015-03-01 | Basf Se | 於水熱條件下合成鋰－金屬－磷酸鹽 |
| TW201038469A (en) | 2009-03-17 | 2010-11-01 | Basf Se | Synthesis of lithium-iron-phosphates |
-
2009
- 2009-04-14 TW TW098112365A patent/TW201010944A/zh unknown
- 2009-04-16 WO PCT/EP2009/054488 patent/WO2009127674A1/en not_active Ceased
- 2009-04-16 CA CA2721029A patent/CA2721029A1/en not_active Abandoned
- 2009-04-16 US US12/988,418 patent/US20110049443A1/en not_active Abandoned
- 2009-04-16 JP JP2011504454A patent/JP2011519806A/ja active Pending
- 2009-04-16 EP EP09732251.5A patent/EP2285740B1/en active Active
- 2009-04-16 KR KR1020107025278A patent/KR101592049B1/ko active Active
- 2009-04-16 CN CN200980122733XA patent/CN102066241B/zh active Active
-
2014
- 2014-12-08 US US14/563,290 patent/US9147877B2/en active Active
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