JP2010511650A5 - - Google Patents
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- Publication number
- JP2010511650A5 JP2010511650A5 JP2009539671A JP2009539671A JP2010511650A5 JP 2010511650 A5 JP2010511650 A5 JP 2010511650A5 JP 2009539671 A JP2009539671 A JP 2009539671A JP 2009539671 A JP2009539671 A JP 2009539671A JP 2010511650 A5 JP2010511650 A5 JP 2010511650A5
- Authority
- JP
- Japan
- Prior art keywords
- reaction
- producing
- subjected
- water
- alkyl methacrylate
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 238000000926 separation method Methods 0.000 claims 4
- -1 alkyl methacrylate ester Chemical class 0.000 claims 3
- 238000006243 chemical reaction Methods 0.000 claims 3
- 238000000034 method Methods 0.000 claims 3
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims 3
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 claims 2
- 239000008346 aqueous phase Substances 0.000 claims 2
- 239000007795 chemical reaction product Substances 0.000 claims 2
- 239000012074 organic phase Substances 0.000 claims 2
- 238000005886 esterification reaction Methods 0.000 claims 1
- FQPSGWSUVKBHSU-UHFFFAOYSA-N methacrylamide Chemical compound CC(=C)C(N)=O FQPSGWSUVKBHSU-UHFFFAOYSA-N 0.000 claims 1
- 229920000642 polymer Polymers 0.000 claims 1
- 230000000379 polymerizing effect Effects 0.000 claims 1
- 239000011541 reaction mixture Substances 0.000 claims 1
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE102006058251A DE102006058251A1 (de) | 2006-12-08 | 2006-12-08 | Verfahren und Vorrichtung zur Herstellung von Methacrylsäurealkylestern |
| DE102006058251.9 | 2006-12-08 | ||
| PCT/EP2007/059107 WO2008068063A1 (de) | 2006-12-08 | 2007-08-31 | Verfahren und vorrichtung zur herstellung von methacrylsäurealkylestern |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| JP2010511650A JP2010511650A (ja) | 2010-04-15 |
| JP2010511650A5 true JP2010511650A5 (https=) | 2011-10-13 |
| JP5757684B2 JP5757684B2 (ja) | 2015-07-29 |
Family
ID=38786597
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2009539671A Expired - Fee Related JP5757684B2 (ja) | 2006-12-08 | 2007-08-31 | メタクリル酸アルキルエステルの製造のための方法及び装置 |
Country Status (15)
| Country | Link |
|---|---|
| US (1) | US9637574B2 (https=) |
| EP (1) | EP2054369B9 (https=) |
| JP (1) | JP5757684B2 (https=) |
| KR (1) | KR101497719B1 (https=) |
| CN (1) | CN101195576B (https=) |
| AU (1) | AU2007327787B2 (https=) |
| BR (1) | BRPI0720245B1 (https=) |
| DE (1) | DE102006058251A1 (https=) |
| ES (1) | ES2531086T3 (https=) |
| MX (1) | MX2009005896A (https=) |
| MY (1) | MY157939A (https=) |
| RU (1) | RU2486173C2 (https=) |
| TW (1) | TWI371443B (https=) |
| WO (1) | WO2008068063A1 (https=) |
| ZA (1) | ZA200903945B (https=) |
Families Citing this family (12)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE102008000785A1 (de) * | 2008-03-20 | 2009-09-24 | Evonik Röhm Gmbh | Verfahren zur Herstellung von Methacrylsäure |
| DE102008000787A1 (de) | 2008-03-20 | 2009-09-24 | Evonik Röhm Gmbh | Verfahren zur Aufreinigung von Methacrylsäure |
| JP5432852B2 (ja) * | 2009-09-30 | 2014-03-05 | ローム アンド ハース カンパニー | メタクリル酸メチルの精製によって生じる流れから価値のある化合物を回収する方法 |
| KR101144306B1 (ko) * | 2010-08-26 | 2012-05-11 | 주식회사 엘지화학 | 알킬(메트)아크릴레이트의 제조 방법 |
| DE102011076642A1 (de) | 2011-05-27 | 2012-11-29 | Evonik Röhm Gmbh | Verfahren zur Herstellung von Methacrylsäure |
| CN103145576B (zh) * | 2013-03-28 | 2015-06-17 | 重庆紫光化工股份有限公司 | 一种环境友好的甲基丙烯酰胺的制备和提纯方法 |
| BR112020001740A2 (pt) * | 2017-07-28 | 2020-07-21 | Rohm And Haas Company | método para preparar metil metacrilato de metacroleína e metanol. |
| CN107862974B (zh) * | 2017-11-22 | 2023-11-24 | 河南莱帕克化工设备制造有限公司 | 苯甲酰胺生产线教学装置 |
| CN113467550B (zh) * | 2020-03-30 | 2022-10-04 | 中石油吉林化工工程有限公司 | 用于mma生产装置中酰化反应的温控系统及温控方法 |
| KR102860381B1 (ko) * | 2020-07-10 | 2025-09-15 | 주식회사 엘지화학 | 페놀계 부산물 분해방법 |
| CN115925738A (zh) * | 2022-12-13 | 2023-04-07 | 南通紫琅生物医药科技有限公司 | 一种磷脂酰丝氨酸浓缩生产制备方法 |
| CN119662299B (zh) * | 2025-01-14 | 2025-12-09 | 中国神华煤制油化工有限公司 | 一种煤直接液化装置停工退碱液的方法 |
Family Cites Families (42)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2101821A (en) * | 1934-11-07 | 1937-12-07 | Ici Ltd | Manufacture of unsaturated or ganic compounds |
| US2416756A (en) * | 1941-10-23 | 1947-03-04 | Du Pont | Continuous production of esters of methacrylic acid |
| US2786739A (en) * | 1954-05-10 | 1957-03-26 | Allied Chem & Dye Corp | Continuous process for the production of methacrylic acid esters and ammonium sulphate |
| GB905510A (en) * | 1958-03-11 | 1962-09-12 | Electro Chimie Metal | Improvements in the manufacture of methyl methacrylate |
| LU38226A1 (https=) | 1959-03-16 | |||
| NL252505A (https=) * | 1959-07-31 | |||
| US3062739A (en) * | 1960-10-25 | 1962-11-06 | Crane Co | Treatment of chemical wastes |
| BE636522A (https=) * | 1962-08-24 | |||
| US3480521A (en) * | 1964-11-13 | 1969-11-25 | Nippon Kokan Kk | Process for the electrolytic formation of aluminum coatings on metallic surfaces in molten salt bath |
| US3332984A (en) * | 1964-12-10 | 1967-07-25 | Eastman Kodak Co | Prevention of methacrylate and acrylate ester polymerization in production thereof |
| US3377378A (en) * | 1965-05-10 | 1968-04-09 | Standard Oil Co | Manufacture of esters from carboxylic acid nitriles |
| DE1468939A1 (de) * | 1965-10-23 | 1968-12-19 | Roehm & Haas Gmbh | Verfahren zur Herstellung von Methacrylsaeuremethylester |
| JPS4940689B1 (https=) | 1966-06-29 | 1974-11-05 | ||
| US3649345A (en) * | 1969-04-01 | 1972-03-14 | Roberto Tolosa | Method of coating dentures to provide a polished surface |
| US3894946A (en) * | 1973-04-02 | 1975-07-15 | American Cyanamid Co | Process for treating industrial wastes |
| US4161609A (en) * | 1977-09-14 | 1979-07-17 | E. I. Du Pont De Nemours And Company | Synthesis of carboxylic acid esters |
| US4230529A (en) * | 1978-11-16 | 1980-10-28 | Li Yao T | Distillation apparatus |
| JPS579740A (en) * | 1980-06-20 | 1982-01-19 | Asahi Chem Ind Co Ltd | Purification of methyl methacrylate |
| JPS57130964A (en) * | 1981-02-05 | 1982-08-13 | Asahi Chem Ind Co Ltd | Purification of acetone cyanohydrin |
| US4668818A (en) * | 1985-06-18 | 1987-05-26 | E. I. Du Pont De Nemours And Company | Methyl methacrylate production |
| CA2012935A1 (en) * | 1989-03-31 | 1990-09-30 | Hirozo Segawa | Purification and preparation processes for methyl methacrylate |
| IT1257282B (it) * | 1992-03-16 | 1996-01-12 | Processo migliorato per la produzione di metilmetacrilato monomero da acetoncianidrina | |
| US5393918A (en) * | 1993-12-02 | 1995-02-28 | Rohm And Haas Company | High yield process for the production of methacrylic acid esters |
| KR960000850A (ko) * | 1994-06-06 | 1996-01-25 | 사토 아키오 | 메타크릴산메틸의 연속제조방법 |
| FR2721923B1 (fr) * | 1994-06-30 | 1996-08-14 | Atochem Elf Sa | Procede de fabrication de methacrylate de methyle sans diacetyle |
| EP0999200B1 (en) * | 1998-11-04 | 2002-07-17 | Rohm And Haas Company | Process for the high yield production of methyl methacrylate or methacrylic acid |
| DE19852104A1 (de) * | 1998-11-12 | 2000-05-18 | Degussa | Verfahren zur Herstellung von ß-Hydroxyaldehyden |
| DE10034193A1 (de) * | 2000-07-13 | 2002-03-28 | Roehm Gmbh | Verfahren zur Herstellung von Cyanwasserstoff |
| DE10034194A1 (de) * | 2000-07-13 | 2003-09-11 | Roehm Gmbh | Verfahren zur Herstellung von Cyanwasserstoff |
| DE10040060A1 (de) * | 2000-08-11 | 2002-02-28 | Roehm Gmbh | Verbessertes Solarienliegematerial |
| WO2003045894A1 (fr) * | 2001-11-27 | 2003-06-05 | Mitsubishi Chemical Corporation | Procede de production d'ester (meth)acrylique |
| DE10200171A1 (de) * | 2002-01-04 | 2003-07-10 | Roehm Gmbh | Verfahren zur kontinuierlichen Herstellung von Alkyl(meth)acrylaten |
| ZA200303241B (en) * | 2002-05-01 | 2003-11-04 | Rohm & Haas | Improved process for methacrylic acid and methcrylic acid ester production. |
| DE10309209A1 (de) * | 2003-02-28 | 2004-09-09 | Degussa Ag | Verfahren zur Herstellung von Cyanwasserstoff nach dem BMA-Verfahren und Katalysator zu seiner Durchführung |
| DE10323699A1 (de) * | 2003-05-22 | 2004-12-09 | Röhm GmbH & Co. KG | Verfahren zur kontinuierlichen Herstellung von Alkylamino(meth)acrylamiden |
| MY145338A (en) * | 2003-12-04 | 2012-01-31 | Dow Global Technologies Inc | Stabilized polyethylene material |
| DE102004006826A1 (de) | 2004-02-11 | 2005-08-25 | Röhm GmbH & Co. KG | Verfahren zur Herstellung von alpha-Hydroxy-carbonsäuren und deren Ester |
| JP4654584B2 (ja) * | 2004-03-01 | 2011-03-23 | 三菱化学株式会社 | (メタ)アクリル酸エステル含有液の取り扱い方法 |
| JP4573325B2 (ja) | 2004-07-01 | 2010-11-04 | 三菱レイヨン株式会社 | メタクリル酸メチルの製造方法 |
| CA2581312C (en) * | 2004-11-23 | 2013-07-16 | Roehm Gmbh | Method for the continuous production of alkyl amino acryl amides |
| DE102005023976A1 (de) * | 2005-05-20 | 2006-11-23 | Röhm Gmbh | Verfahren zur Umesterung |
| DE102005023975A1 (de) * | 2005-05-20 | 2006-11-23 | Röhm Gmbh | Verfahren zur Herstellung von Alkyl(meth)acrylaten |
-
2006
- 2006-12-08 DE DE102006058251A patent/DE102006058251A1/de not_active Withdrawn
-
2007
- 2007-02-28 CN CN2007100843892A patent/CN101195576B/zh not_active Expired - Fee Related
- 2007-08-31 BR BRPI0720245A patent/BRPI0720245B1/pt not_active IP Right Cessation
- 2007-08-31 KR KR1020097011718A patent/KR101497719B1/ko not_active Expired - Fee Related
- 2007-08-31 MX MX2009005896A patent/MX2009005896A/es active IP Right Grant
- 2007-08-31 US US12/515,964 patent/US9637574B2/en not_active Expired - Fee Related
- 2007-08-31 JP JP2009539671A patent/JP5757684B2/ja not_active Expired - Fee Related
- 2007-08-31 RU RU2009125685/04A patent/RU2486173C2/ru not_active IP Right Cessation
- 2007-08-31 WO PCT/EP2007/059107 patent/WO2008068063A1/de not_active Ceased
- 2007-08-31 EP EP07803107.7A patent/EP2054369B9/de not_active Not-in-force
- 2007-08-31 AU AU2007327787A patent/AU2007327787B2/en not_active Ceased
- 2007-08-31 MY MYPI20091806A patent/MY157939A/en unknown
- 2007-08-31 ES ES07803107T patent/ES2531086T3/es active Active
- 2007-12-04 TW TW096146122A patent/TWI371443B/zh not_active IP Right Cessation
-
2009
- 2009-06-05 ZA ZA200903945A patent/ZA200903945B/xx unknown
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