ATE220657T1 - Verfahren zum herstellen mit grosser ausbeute von methylmethacrylat oder methacrylsäure - Google Patents

Verfahren zum herstellen mit grosser ausbeute von methylmethacrylat oder methacrylsäure

Info

Publication number
ATE220657T1
ATE220657T1 AT99308376T AT99308376T ATE220657T1 AT E220657 T1 ATE220657 T1 AT E220657T1 AT 99308376 T AT99308376 T AT 99308376T AT 99308376 T AT99308376 T AT 99308376T AT E220657 T1 ATE220657 T1 AT E220657T1
Authority
AT
Austria
Prior art keywords
methacrylic acid
methyl methacrylate
high yield
producing high
yield methyl
Prior art date
Application number
AT99308376T
Other languages
English (en)
Inventor
Chorng-Shyuan Tsay
Makarand Dattatraya Phadke
Soc
Michael Stanley Decourcy
Abraham Benderly
I-Hwa Midey Chang-Mateu
Nicole Rendon Koegel
Heather Granzin Thompson
Diana Elaine Chase
Original Assignee
Rohm & Haas
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Rohm & Haas filed Critical Rohm & Haas
Application granted granted Critical
Publication of ATE220657T1 publication Critical patent/ATE220657T1/de

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C69/00—Esters of carboxylic acids; Esters of carbonic or haloformic acids
    • C07C69/52—Esters of acyclic unsaturated carboxylic acids having the esterified carboxyl group bound to an acyclic carbon atom
    • C07C69/533—Monocarboxylic acid esters having only one carbon-to-carbon double bond
    • C07C69/54—Acrylic acid esters; Methacrylic acid esters
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C231/00—Preparation of carboxylic acid amides
    • C07C231/06—Preparation of carboxylic acid amides from nitriles by transformation of cyano groups into carboxamide groups
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/02—Apparatus characterised by being constructed of material selected for its chemically-resistant properties
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/24—Stationary reactors without moving elements inside
    • B01J19/2415—Tubular reactors
    • B01J19/242—Tubular reactors in series
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/24—Stationary reactors without moving elements inside
    • B01J19/2415—Tubular reactors
    • B01J19/243—Tubular reactors spirally, concentrically or zigzag wound
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/08—Preparation of carboxylic acids or their salts, halides or anhydrides from nitriles
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C67/00—Preparation of carboxylic acid esters
    • C07C67/18—Preparation of carboxylic acid esters by conversion of a group containing nitrogen into an ester group
    • C07C67/20—Preparation of carboxylic acid esters by conversion of a group containing nitrogen into an ester group from amides or lactams
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049—Controlling or regulating processes
    • B01J2219/00051—Controlling the temperature
    • B01J2219/00074—Controlling the temperature by indirect heating or cooling employing heat exchange fluids
    • B01J2219/00087—Controlling the temperature by indirect heating or cooling employing heat exchange fluids with heat exchange elements outside the reactor
    • B01J2219/00094—Jackets
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049—Controlling or regulating processes
    • B01J2219/00164—Controlling or regulating processes controlling the flow
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/02—Apparatus characterised by their chemically-resistant properties
    • B01J2219/025—Apparatus characterised by their chemically-resistant properties characterised by the construction materials of the reactor vessel proper
    • B01J2219/0277—Metal based
    • B01J2219/029—Non-ferrous metals
AT99308376T 1998-11-04 1999-10-22 Verfahren zum herstellen mit grosser ausbeute von methylmethacrylat oder methacrylsäure ATE220657T1 (de)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
US10694798P 1998-11-04 1998-11-04

Publications (1)

Publication Number Publication Date
ATE220657T1 true ATE220657T1 (de) 2002-08-15

Family

ID=22314086

Family Applications (1)

Application Number Title Priority Date Filing Date
AT99308376T ATE220657T1 (de) 1998-11-04 1999-10-22 Verfahren zum herstellen mit grosser ausbeute von methylmethacrylat oder methacrylsäure

Country Status (10)

Country Link
US (2) US6545176B1 (de)
EP (1) EP0999200B1 (de)
JP (2) JP4553425B2 (de)
KR (1) KR100691647B1 (de)
CN (1) CN1173921C (de)
AT (1) ATE220657T1 (de)
BR (1) BR9904993B1 (de)
DE (1) DE69902137T2 (de)
ES (1) ES2179599T3 (de)
TW (1) TW505629B (de)

Families Citing this family (76)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP4736165B2 (ja) * 2000-08-23 2011-07-27 住友化学株式会社 トリエチルアミンの回収方法およびエマルジョン層の削減方法
US6906164B2 (en) * 2000-12-07 2005-06-14 Eastman Chemical Company Polyester process using a pipe reactor
FR2827279B1 (fr) * 2001-07-13 2004-06-18 Atofina Procede de preparation de methacrylamide sulfurique et dispositif pour sa mise en oeuvre
ZA200303241B (en) * 2002-05-01 2003-11-04 Rohm & Haas Improved process for methacrylic acid and methcrylic acid ester production.
US7128813B2 (en) 2002-05-01 2006-10-31 Rohm And Haas Company Process for manufacturing high purity methacrylic acid
BRPI0503134B1 (pt) * 2004-08-02 2018-03-20 Rohm And Haas Company Método de formação de uma chapa de tubo laminada
US7931725B2 (en) 2004-11-02 2011-04-26 Baldwin Filters, Inc. Fluted filter apparatus
US20060091084A1 (en) * 2004-11-02 2006-05-04 Baldwin Filters, Inc. Fluted filter media with intermediate flow restriction and method of making same
US20060090431A1 (en) * 2004-11-02 2006-05-04 Baldwin Filters, Inc. Filter assembly with combination filter element
US20110197556A1 (en) 2004-11-02 2011-08-18 Baldwin Filters, Inc. Filter element
US7318851B2 (en) * 2004-11-02 2008-01-15 Baldwin Filters, Inc. Filter element
US8042694B2 (en) * 2004-11-02 2011-10-25 Baldwin Filters, Inc. Gathered filter media for an air filter and method of making same
US7255300B2 (en) 2004-11-03 2007-08-14 Baldwin Filters, Inc. Method and apparatus for winding a filter media pack
US7909954B2 (en) 2004-11-03 2011-03-22 Baldwin Filters, Inc. Method and apparatus for winding a filter media pack
US7753982B2 (en) * 2006-02-17 2010-07-13 Baldwin Filters, Inc. Filter with drained jacket, seal indicator/lock means, and seal baffle
US9757676B2 (en) 2006-12-06 2017-09-12 Baldwin Filters, Inc. Method and apparatus for winding a filter element
US10040020B2 (en) 2006-12-06 2018-08-07 Baldwin Filters, Inc. Fluid filter apparatus having filter media wound about a winding frame
US7649109B2 (en) 2006-12-07 2010-01-19 Eastman Chemical Company Polyester production system employing recirculation of hot alcohol to esterification zone
US7943094B2 (en) 2006-12-07 2011-05-17 Grupo Petrotemex, S.A. De C.V. Polyester production system employing horizontally elongated esterification vessel
DE102006058251A1 (de) * 2006-12-08 2008-06-12 Evonik Röhm Gmbh Verfahren und Vorrichtung zur Herstellung von Methacrylsäurealkylestern
US7892498B2 (en) * 2007-03-08 2011-02-22 Eastman Chemical Company Polyester production system employing an unagitated esterification reactor
US7863477B2 (en) 2007-03-08 2011-01-04 Eastman Chemical Company Polyester production system employing hot paste to esterification zone
US7858730B2 (en) * 2007-07-12 2010-12-28 Eastman Chemical Company Multi-level tubular reactor with dual headers
US7868129B2 (en) * 2007-07-12 2011-01-11 Eastman Chemical Company Sloped tubular reactor with spaced sequential trays
US7872089B2 (en) 2007-07-12 2011-01-18 Eastman Chemical Company Multi-level tubular reactor with internal tray
US7847053B2 (en) * 2007-07-12 2010-12-07 Eastman Chemical Company Multi-level tubular reactor with oppositely extending segments
US7829653B2 (en) * 2007-07-12 2010-11-09 Eastman Chemical Company Horizontal trayed reactor
US7872090B2 (en) * 2007-07-12 2011-01-18 Eastman Chemical Company Reactor system with optimized heating and phase separation
US7842777B2 (en) * 2007-07-12 2010-11-30 Eastman Chemical Company Sloped tubular reactor with divided flow
US7868130B2 (en) * 2007-07-12 2011-01-11 Eastman Chemical Company Multi-level tubular reactor with vertically spaced segments
US9545593B2 (en) 2007-11-01 2017-01-17 Baldwin Filters, Inc. Winding core pressure relief for fluted filter
EP2085376B1 (de) 2008-01-30 2012-09-05 Evonik Röhm GmbH Verfahren zur Herstellung hochreiner Methacrylsäure
DE102008000787A1 (de) * 2008-03-20 2009-09-24 Evonik Röhm Gmbh Verfahren zur Aufreinigung von Methacrylsäure
DE102008000785A1 (de) 2008-03-20 2009-09-24 Evonik Röhm Gmbh Verfahren zur Herstellung von Methacrylsäure
US8048187B2 (en) 2008-06-30 2011-11-01 Baldwin Filters, Inc. Filter frame attachment and fluted filter having same
US7959703B2 (en) 2008-06-30 2011-06-14 Baldwin Filters, Inc. Fluted filter with integrated frame
CN105646136A (zh) * 2008-10-13 2016-06-08 蓝立方知识产权公司 用于生产氯化和/或氟化丙烯的方法
JP5432852B2 (ja) * 2009-09-30 2014-03-05 ローム アンド ハース カンパニー メタクリル酸メチルの精製によって生じる流れから価値のある化合物を回収する方法
CN102596387B (zh) 2009-10-09 2015-11-25 陶氏环球技术有限责任公司 生产氯化和/或氟化丙烯和高级烯烃的等温多管反应器和方法
EP2485997B1 (de) 2009-10-09 2015-09-09 Dow Global Technologies LLC Verfahren zur herstellung von chlorierten und/oder fluorierten probenen und höheren alkenen
JP5706432B2 (ja) * 2009-10-09 2015-04-22 ダウ グローバル テクノロジーズ エルエルシー 塩素化及び／又はフッ素化プロペンの製造方法
KR20120093202A (ko) * 2009-10-09 2012-08-22 다우 글로벌 테크놀로지스 엘엘씨 단열식 플러그 흐름 반응기 및 염화 및/또는 불화 프로펜 및 고급 알켄의 제조 방법
KR101174203B1 (ko) 2010-04-09 2012-08-14 박병진 폐인조 대리석으로부터 메타크릴산메틸을 회수하는 장치 및 그 방법
SG189244A1 (en) * 2010-10-07 2013-05-31 Rohm & Haas Process for production of methacrylic acid ester
EP2714630A1 (de) 2011-05-31 2014-04-09 Dow Global Technologies LLC Verfahren zur herstellung von chlorierten propenen
WO2012166394A1 (en) 2011-05-31 2012-12-06 Dow Global Technologies, Llc Process for the production of chlorinated propenes
MX336250B (es) 2011-06-08 2016-01-13 Dow Agrosciences Llc Proceso para la produccion de propenos clorados y/o fluorados.
EP2739595B1 (de) 2011-08-07 2018-12-12 Blue Cube IP LLC Verfahren zur herstellung von chlorierten propenen
CA2844319A1 (en) 2011-08-07 2013-02-14 Dow Global Technologies Llc Process for the production of chlorinated propenes
EP2782889B1 (de) 2011-11-21 2016-12-21 Blue Cube IP LLC Verfahren zur herstellung von chlorierten alkanen
US9284239B2 (en) 2011-12-02 2016-03-15 Blue Cube Ip Llc Process for the production of chlorinated alkanes
JP6059246B2 (ja) 2011-12-02 2017-01-11 ブルー キューブ アイピー エルエルシー 塩素化アルカンの製造方法
US9334205B2 (en) 2011-12-13 2016-05-10 Blue Cube Ip Llc Process for the production of chlorinated propanes and propenes
US9169177B2 (en) 2011-12-22 2015-10-27 Blue Cube Ip Llc Process for the production of tetrachloromethane
US9512049B2 (en) 2011-12-23 2016-12-06 Dow Global Technologies Llc Process for the production of alkenes and/or aromatic compounds
BR112015001748B1 (pt) 2012-07-25 2022-03-15 Baldwin Filters, Inc Conjunto de filtro
CN104755448A (zh) 2012-09-20 2015-07-01 陶氏环球技术有限公司 用于制造氯化丙烯的方法
US9321707B2 (en) 2012-09-20 2016-04-26 Blue Cube Ip Llc Process for the production of chlorinated propenes
BR112015006831B1 (pt) * 2012-09-28 2020-10-27 Rohm And Haas Company processo para a preparação de ácido metacrílico e de ésteres do mesmo
US9795941B2 (en) 2012-09-30 2017-10-24 Blue Cube Ip Llc Weir quench and processes incorporating the same
US10065157B2 (en) 2012-10-26 2018-09-04 Blue Cube Ip Llc Mixer and processes incorporating the same
EP2935165A1 (de) 2012-12-18 2015-10-28 Blue Cube IP LLC Verfahren zur herstellung von chlorierten propenen
WO2014100039A1 (en) 2012-12-19 2014-06-26 Dow Global Technologies, Llc Process for the production of chlorinated propenes
CN104981449B (zh) 2013-02-27 2016-12-28 蓝立方知识产权有限责任公司 用于生产氯化丙烯的方法
CN105026348A (zh) 2013-03-09 2015-11-04 蓝立方知识产权有限责任公司 用于生产氯化烷烃的方法
CN103254091B (zh) * 2013-05-21 2015-04-08 重庆紫光化工股份有限公司 一种甲基丙烯酰胺、甲基丙烯酸甲酯和甲基丙烯酸的联合生产方法
FR3008692B1 (fr) * 2013-07-19 2016-12-23 Arkema France Installation et procede pour la preparation de cyanure d'hydrogene
FR3008627B1 (fr) * 2013-07-19 2017-02-24 Arkema France Cuve de conversion thermique utilisee dans un procede d'amidification de cyanohydrine d'acetone
FR3012143B1 (fr) * 2013-10-18 2016-08-26 Arkema France Cuve d'hydrolyse dans un procede d'amidification de cyanohydrine d'acetone
CN106795091B (zh) * 2014-10-27 2020-11-03 罗门哈斯公司 用于生产甲基丙烯酸甲酯的减少积垢的方法
EP3212603B1 (de) * 2014-10-27 2020-11-25 Rohm and Haas Company Verfahren mit reduzierter fäulnisbildung zur herstellung von methylmethacrylat
US10682597B2 (en) 2016-04-14 2020-06-16 Baldwin Filters, Inc. Filter system
CN110394143A (zh) * 2019-08-21 2019-11-01 兖州煤业股份有限公司 一种煤消解管式反应装置
JP2023550265A (ja) 2020-10-23 2023-12-01 レーム・ゲーエムベーハー 転化時の逆混合の低減によるメチルメタクリレートおよび／またはメタクリル酸の改良された製造方法
CN113121343A (zh) * 2021-03-15 2021-07-16 江苏新东风化工科技有限公司 一种丙烯酸正丁酯的中和生产工艺
WO2023169863A1 (en) 2022-03-08 2023-09-14 Röhm Gmbh Process for preparing high purity (meth)acrylates

Family Cites Families (14)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2416756A (en) * 1941-10-23 1947-03-04 Du Pont Continuous production of esters of methacrylic acid
US2373464A (en) * 1942-05-22 1945-04-10 Du Pont Process for inhibiting polymerization
US2786739A (en) * 1954-05-10 1957-03-26 Allied Chem & Dye Corp Continuous process for the production of methacrylic acid esters and ammonium sulphate
US3027328A (en) * 1958-12-09 1962-03-27 Degussa Process for the preparation of acetonecyanohydrin/sulfuric acid mixtures
JPS49135917A (de) * 1973-05-15 1974-12-27
PL84285B1 (de) * 1973-07-12 1976-03-31
JPS5767534A (en) * 1980-10-16 1982-04-24 Mitsui Toatsu Chem Inc Preparation of alpha,beta-unsaturated carboxylic ester and alpha,beta-unsaturated carboxylic acid
US4529816A (en) * 1984-02-13 1985-07-16 E. I. Du Pont De Nemours And Company Process for producing alkyl methacrylates
JPS61261391A (ja) * 1985-05-13 1986-11-19 東洋エンジニアリング株式会社 熱分解改質油の製法
US4748268A (en) 1986-07-31 1988-05-31 Amoco Corporation Continuous process for production of methacrylic acid ester of C1 to C4 aliphatic alcohol
JP2778131B2 (ja) * 1989-07-14 1998-07-23 三菱瓦斯化学株式会社 メタクリル酸メチルの製造方法
US5393918A (en) 1993-12-02 1995-02-28 Rohm And Haas Company High yield process for the production of methacrylic acid esters
KR960000850A (ko) * 1994-06-06 1996-01-25 사토 아키오 메타크릴산메틸의 연속제조방법
JPH0853393A (ja) * 1994-06-06 1996-02-27 Mitsui Toatsu Chem Inc メタクリル酸メチルの連続製造方法

Also Published As

Publication number Publication date
KR20000035177A (ko) 2000-06-26
US20020188153A1 (en) 2002-12-12
CN1254706A (zh) 2000-05-31
TW505629B (en) 2002-10-11
BR9904993A (pt) 2000-08-08
KR100691647B1 (ko) 2007-03-09
JP2000159728A (ja) 2000-06-13
EP0999200A1 (de) 2000-05-10
DE69902137D1 (de) 2002-08-22
JP2010209087A (ja) 2010-09-24
CN1173921C (zh) 2004-11-03
JP5213901B2 (ja) 2013-06-19
US6545176B1 (en) 2003-04-08
DE69902137T2 (de) 2003-01-30
US6610177B2 (en) 2003-08-26
BR9904993B1 (pt) 2011-02-08
ES2179599T3 (es) 2003-01-16
EP0999200B1 (de) 2002-07-17
JP4553425B2 (ja) 2010-09-29

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