FR3008692B1 - Installation et procede pour la preparation de cyanure d'hydrogene - Google Patents

Installation et procede pour la preparation de cyanure d'hydrogene

Info

Publication number
FR3008692B1
FR3008692B1 FR1357132A FR1357132A FR3008692B1 FR 3008692 B1 FR3008692 B1 FR 3008692B1 FR 1357132 A FR1357132 A FR 1357132A FR 1357132 A FR1357132 A FR 1357132A FR 3008692 B1 FR3008692 B1 FR 3008692B1
Authority
FR
France
Prior art keywords
installation
preparation
hydrogen cyanide
cyanide
hydrogen
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Active
Application number
FR1357132A
Other languages
English (en)
Other versions
FR3008692A1 (fr
Inventor
Yves Bernardin
Xavier Marcarian
Romain Billon
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Trinseo Europe GmbH
Original Assignee
Arkema France SA
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Priority to FR1357132A priority Critical patent/FR3008692B1/fr
Application filed by Arkema France SA filed Critical Arkema France SA
Priority to PCT/EP2014/065567 priority patent/WO2015007907A1/fr
Priority to CN202010600694.8A priority patent/CN111704147A/zh
Priority to CN201480041110.0A priority patent/CN105636906A/zh
Priority to MX2016000636A priority patent/MX2016000636A/es
Priority to EP14739858.0A priority patent/EP3022153B1/fr
Priority to US14/905,435 priority patent/US9944533B2/en
Publication of FR3008692A1 publication Critical patent/FR3008692A1/fr
Application granted granted Critical
Publication of FR3008692B1 publication Critical patent/FR3008692B1/fr
Priority to US15/938,606 priority patent/US10865118B2/en
Active legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01C—AMMONIA; CYANOGEN; COMPOUNDS THEREOF
    • C01C3/00—Cyanogen; Compounds thereof
    • C01C3/02—Preparation, separation or purification of hydrogen cyanide
    • C01C3/0208—Preparation in gaseous phase
    • C01C3/0212—Preparation in gaseous phase from hydrocarbons and ammonia in the presence of oxygen, e.g. the Andrussow-process
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J12/00—Chemical processes in general for reacting gaseous media with gaseous media; Apparatus specially adapted therefor
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0006—Controlling or regulating processes
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J4/00—Feed or outlet devices; Feed or outlet control devices
    • B01J4/008—Feed or outlet control devices
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J4/00—Feed or outlet devices; Feed or outlet control devices
    • B01J4/02—Feed or outlet devices; Feed or outlet control devices for feeding measured, i.e. prescribed quantities of reagents
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01C—AMMONIA; CYANOGEN; COMPOUNDS THEREOF
    • C01C3/00—Cyanogen; Compounds thereof
    • C01C3/02—Preparation, separation or purification of hydrogen cyanide
    • C01C3/0208—Preparation in gaseous phase
    • C01C3/0212—Preparation in gaseous phase from hydrocarbons and ammonia in the presence of oxygen, e.g. the Andrussow-process
    • C01C3/022—Apparatus therefor
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C231/00—Preparation of carboxylic acid amides
    • C07C231/06—Preparation of carboxylic acid amides from nitriles by transformation of cyano groups into carboxamide groups
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C231/00—Preparation of carboxylic acid amides
    • C07C231/12—Preparation of carboxylic acid amides by reactions not involving the formation of carboxamide groups
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C253/00—Preparation of carboxylic acid nitriles
    • C07C253/04—Preparation of carboxylic acid nitriles by reaction of cyanogen halides, e.g. ClCN, with organic compounds
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/06—Preparation of carboxylic acids or their salts, halides or anhydrides from carboxylic acid amides
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C67/00—Preparation of carboxylic acid esters
    • C07C67/18—Preparation of carboxylic acid esters by conversion of a group containing nitrogen into an ester group
    • C07C67/20—Preparation of carboxylic acid esters by conversion of a group containing nitrogen into an ester group from amides or lactams
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049—Controlling or regulating processes
    • B01J2219/00186—Controlling or regulating processes controlling the composition of the reactive mixture
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049—Controlling or regulating processes
    • B01J2219/00191—Control algorithm
    • B01J2219/00211—Control algorithm comparing a sensed parameter with a pre-set value
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049—Controlling or regulating processes
    • B01J2219/00191—Control algorithm
    • B01J2219/00222—Control algorithm taking actions
    • B01J2219/00225—Control algorithm taking actions stopping the system or generating an alarm
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00—Technologies relating to chemical industry
    • Y02P20/10—Process efficiency
    • Y02P20/129—Energy recovery, e.g. by cogeneration, H2recovery or pressure recovery turbines
FR1357132A 2013-07-19 2013-07-19 Installation et procede pour la preparation de cyanure d'hydrogene Active FR3008692B1 (fr)

Priority Applications (8)

Application Number Priority Date Filing Date Title
FR1357132A FR3008692B1 (fr) 2013-07-19 2013-07-19 Installation et procede pour la preparation de cyanure d'hydrogene
CN202010600694.8A CN111704147A (zh) 2013-07-19 2014-07-18 用于制备氰化氢的装置和方法
CN201480041110.0A CN105636906A (zh) 2013-07-19 2014-07-18 用于制备氰化氢的装置和方法
MX2016000636A MX2016000636A (es) 2013-07-19 2014-07-18 Instalacion y proceso para la preparacion de cianuro de hidrogeno.
PCT/EP2014/065567 WO2015007907A1 (fr) 2013-07-19 2014-07-18 Installation et procédé pour la préparation de cyanure d'hydrogène
EP14739858.0A EP3022153B1 (fr) 2013-07-19 2014-07-18 Installation et procédé pour la préparation de cyanure d'hydrogène
US14/905,435 US9944533B2 (en) 2013-07-19 2014-07-18 Installation and process for the preparation of hydrogen cyanide
US15/938,606 US10865118B2 (en) 2013-07-19 2018-03-28 Installation and process for the preparation of hydrogen cyanide

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
FR1357132A FR3008692B1 (fr) 2013-07-19 2013-07-19 Installation et procede pour la preparation de cyanure d'hydrogene

Publications (2)

Publication Number Publication Date
FR3008692A1 FR3008692A1 (fr) 2015-01-23
FR3008692B1 true FR3008692B1 (fr) 2016-12-23

Family

ID=49620060

Family Applications (1)

Application Number Title Priority Date Filing Date
FR1357132A Active FR3008692B1 (fr) 2013-07-19 2013-07-19 Installation et procede pour la preparation de cyanure d'hydrogene

Country Status (6)

Country Link
US (2) US9944533B2 (fr)
EP (1) EP3022153B1 (fr)
CN (2) CN111704147A (fr)
FR (1) FR3008692B1 (fr)
MX (1) MX2016000636A (fr)
WO (1) WO2015007907A1 (fr)

Families Citing this family (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
TW201437146A (zh) * 2012-12-18 2014-10-01 Invista Tech Sarl 使用靜式混合器製造氰化氫之方法
CN107434253B (zh) * 2017-08-06 2019-12-17 河北诚信集团有限公司 一种高品质氰化物溶液的连续化生产工艺及其生产系统
CN110963915A (zh) * 2019-11-13 2020-04-07 上海星酶生物科技有限公司 一种2-乙酰氧基异丁酰溴制备工艺
CN112777610A (zh) * 2021-03-01 2021-05-11 广东广大新能源科技有限公司 一种使用液化天然气冷能制备氢氰酸的方法及装置
CN113277532B (zh) * 2021-06-04 2023-11-21 四川能投建工集团设计研究院有限公司 一种氢氰酸的制备方法

Family Cites Families (22)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2803522A (en) * 1953-04-15 1957-08-20 Du Pont Manufacture of hydrogen cyanide
NL284848A (fr) * 1961-10-31
US3215495A (en) * 1962-01-23 1965-11-02 Du Pont Apparatus and process for preparing hydrogen cyanide
US3667907A (en) * 1970-05-04 1972-06-06 Du Pont Manufacture of hydrogen cyanide
US3762426A (en) 1972-04-26 1973-10-02 Ibm Semiconductor chip separation apparatus
GB1426254A (en) * 1972-10-06 1976-02-25 Sumitomo Chemical Co Process for preparing hydrogen cyanide
DE2831856B2 (de) * 1978-07-20 1981-07-02 Drägerwerk AG, 2400 Lübeck Anordnung zum elektrisch gesteuerten Dosieren und Mischen von Gasen
DE3515072A1 (de) * 1985-04-26 1986-11-06 Gesellschaft für Strahlen- und Umweltforschung mbH, München, 8042 Neuherberg Anlage fuer die schadgaszufuhr zu einer expositions-kammer
JP3889442B2 (ja) * 1995-09-01 2007-03-07 ルーサイト インターナショナル ユーケー リミティド シアン化水素の製造方法及びそのための装置
JPH11255710A (ja) * 1998-03-11 1999-09-21 Mitsubishi Gas Chem Co Inc メタクリル酸メチルの製造方法
US6238634B1 (en) * 1998-05-06 2001-05-29 E.I. Du Pont De Nemours And Company Process for the nondestructive heating and supply of hot ammonia or hot ammonia containing feed gas
US6221327B1 (en) * 1998-05-15 2001-04-24 Rohm And Haas Company Catalyst system using flow-through radiation shielding and a process for producing hydrogen cyanide using the same
DE69902137T2 (de) * 1998-11-04 2003-01-30 Rohm & Haas Verfahren zum Herstellen mit grosser Ausbeute von Methylmethacrylat oder Methacrylsäure
US20020071798A1 (en) * 2000-07-12 2002-06-13 Decourcy Michael Stanley Laboratory Scale reaction systems
DE10034193A1 (de) * 2000-07-13 2002-03-28 Roehm Gmbh Verfahren zur Herstellung von Cyanwasserstoff
DE102007014586A1 (de) * 2007-03-23 2008-09-25 Evonik Röhm Gmbh Verfahren zur Herstellung von Cyanwasserstoff (HCN)
DE102007026712A1 (de) * 2007-06-06 2008-12-11 Uhde Gmbh Vorrichtung und Verfahren für katalytische Gasphasenreaktionen sowie deren Verwendung
DE102007034715A1 (de) * 2007-07-23 2009-01-29 Evonik Röhm Gmbh Reaktor zur Herstellung von Cyanwasserstoff nach dem Andrussow-Verfahren
FR2928910B1 (fr) * 2008-03-20 2010-03-12 Arkema France Procede ameliore de production d'acide cyanhydrique
DE102011076642A1 (de) * 2011-05-27 2012-11-29 Evonik Röhm Gmbh Verfahren zur Herstellung von Methacrylsäure
CN202508885U (zh) * 2012-04-23 2012-10-31 山西阳煤丰喜肥业(集团)有限责任公司 一种用于富氧制氢氰酸的装置
US20150360965A1 (en) * 2012-12-18 2015-12-17 Invista Technologies S.A.R.L. Apparatus and method for decreasing humidity during an andrussow process

Also Published As

Publication number Publication date
CN111704147A (zh) 2020-09-25
EP3022153B1 (fr) 2023-09-06
MX2016000636A (es) 2016-05-26
US20180215626A1 (en) 2018-08-02
US10865118B2 (en) 2020-12-15
EP3022153A1 (fr) 2016-05-25
FR3008692A1 (fr) 2015-01-23
CN105636906A (zh) 2016-06-01
US9944533B2 (en) 2018-04-17
US20160194212A1 (en) 2016-07-07
WO2015007907A1 (fr) 2015-01-22

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