JP6059246B2 - 塩素化アルカンの製造方法 - Google Patents
塩素化アルカンの製造方法 Download PDFInfo
- Publication number
- JP6059246B2 JP6059246B2 JP2014544918A JP2014544918A JP6059246B2 JP 6059246 B2 JP6059246 B2 JP 6059246B2 JP 2014544918 A JP2014544918 A JP 2014544918A JP 2014544918 A JP2014544918 A JP 2014544918A JP 6059246 B2 JP6059246 B2 JP 6059246B2
- Authority
- JP
- Japan
- Prior art keywords
- ppm
- pentachloropropane
- alkane
- trichloropropane
- chlorine
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C17/00—Preparation of halogenated hydrocarbons
- C07C17/013—Preparation of halogenated hydrocarbons by addition of halogens
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C17/00—Preparation of halogenated hydrocarbons
- C07C17/093—Preparation of halogenated hydrocarbons by replacement by halogens
- C07C17/10—Preparation of halogenated hydrocarbons by replacement by halogens of hydrogen atoms
Description
[1]
1つ又は複数の非金属ヨウ化物及び/又は10,000ppm未満の元素状ヨウ素並びに少なくとも1つのルイス酸を含む触媒システムで、少なくとも2個の塩素原子のアルカン及び/又はアルケンへの付加を触媒することを含む、塩素化アルカンの製造方法。
[2]
塩素原子の源が、塩素ガス、塩化スルフリル又はそれらの組み合わせを含む、項目1に記載の方法。
[3]
該ルイス酸が塩化アルミニウムを含む、項目1に記載の方法。
[4]
該元素状ヨウ素が、1ppm〜5000ppmの量で用いられる、項目1に記載の方法。
[5]
クロロカーボン溶媒の存在下で実施される、項目1に記載の方法。
[6]
該クロロカーボン溶媒が塩化メチレン又は1,2,3−トリクロロプロパンを含む、項目5に記載の方法。
[7]
該アルカン及び/又はアルケンが0〜4個の塩素原子を含む、項目1に記載の方法。
[8]
該アルカン及び/又はアルケンがトリクロロアルカン又はトリクロロアルケンである、項目7に記載の方法。
[9]
該アルカン又はアルケンが2〜6個の炭素原子を含む、項目1又は7に記載の方法。
[10]
該アルカン又はアルケンがプロパン又はプロペンを含む、項目9に記載の方法。
[11]
該塩素化アルカンが2〜6個の塩素原子を含む、項目1、5、又は7に記載の方法。
[12]
該塩素化アルカンがペンタクロロプロパンを含む、項目11に記載の方法。
[13]
該塩素化アルカンが1,1,2,2,3−ペンタクロロプロパンを含む、項目12に記載の方法。
[14]
該非金属ヨウ化物が、ヨードベンゼン、ペンタクロロヨードベンゼン、塩素化ヨードベンゼン、及びそれらの誘導体、塩化フェニルクロロヨードニウム及びその誘導体、ヨウ素化ポリマー、三ハロゲン化ヨウ素、又は任意の数のそれらの組み合わせを含む、項目1に記載の方法。
[15]
該非金属ヨウ化物がヨードベンゼンを含む、項目14に記載の方法。
Claims (4)
- 少なくとも1つのルイス酸並びに1つ又は複数の非金属ヨウ化物及び/又は10,000ppm未満の量の元素状ヨウ素を含む触媒システムで、少なくとも2個の塩素原子のプロパンへの付加を触媒することを含み、該非金属ヨウ化物が、ヨードベンゼン又は2,3,5,6−テトラメチル−1−ヨードベンゼンである、塩素化アルカンの製造方法。
- 該ルイス酸が塩化アルミニウムを含む、請求項1に記載の方法。
- 該元素状ヨウ素が、1ppm〜5000ppmの量で用いられる、請求項1に記載の方法。
- 該塩素化アルカンが1,1,2,2,3−ペンタクロロプロパンを含む、請求項1に記載の方法。
Applications Claiming Priority (3)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US201161566202P | 2011-12-02 | 2011-12-02 | |
US61/566,202 | 2011-12-02 | ||
PCT/US2012/067261 WO2013082404A1 (en) | 2011-12-02 | 2012-11-30 | Process for the production of chlorinated alkanes |
Publications (2)
Publication Number | Publication Date |
---|---|
JP2015500807A JP2015500807A (ja) | 2015-01-08 |
JP6059246B2 true JP6059246B2 (ja) | 2017-01-11 |
Family
ID=47324472
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
JP2014544918A Expired - Fee Related JP6059246B2 (ja) | 2011-12-02 | 2012-11-30 | 塩素化アルカンの製造方法 |
Country Status (6)
Country | Link |
---|---|
US (1) | US9199899B2 (ja) |
EP (1) | EP2785670B1 (ja) |
JP (1) | JP6059246B2 (ja) |
CN (1) | CN104024186B (ja) |
CA (1) | CA2856545A1 (ja) |
WO (1) | WO2013082404A1 (ja) |
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CA2903760C (en) | 2013-03-09 | 2018-02-20 | Blue Cube Ip Llc | Process for the production of chlorinated alkanes |
US8969259B2 (en) * | 2013-04-05 | 2015-03-03 | Reg Synthetic Fuels, Llc | Bio-based synthetic fluids |
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2012
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JP2015500807A (ja) | 2015-01-08 |
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US9199899B2 (en) | 2015-12-01 |
WO2013082404A1 (en) | 2013-06-06 |
CN104024186A (zh) | 2014-09-03 |
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CA2856545A1 (en) | 2013-06-06 |
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