FR3012143B1 - Cuve d'hydrolyse dans un procede d'amidification de cyanohydrine d'acetone - Google Patents

Cuve d'hydrolyse dans un procede d'amidification de cyanohydrine d'acetone

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Publication number
FR3012143B1
FR3012143B1 FR1360194A FR1360194A FR3012143B1 FR 3012143 B1 FR3012143 B1 FR 3012143B1 FR 1360194 A FR1360194 A FR 1360194A FR 1360194 A FR1360194 A FR 1360194A FR 3012143 B1 FR3012143 B1 FR 3012143B1
Authority
FR
France
Prior art keywords
acetone cyanohydrin
hydrolysis tank
amidification
amidification process
hydrolysis
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Active
Application number
FR1360194A
Other languages
English (en)
Other versions
FR3012143A1 (fr
Inventor
Yves Bernardin
Xavier Marcarian
Romain Billon
Florent Vallet
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Trinseo Europe GmbH
Original Assignee
Arkema France SA
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Priority to FR1360194A priority Critical patent/FR3012143B1/fr
Application filed by Arkema France SA filed Critical Arkema France SA
Priority to US15/029,306 priority patent/US10273199B2/en
Priority to BR112016008641-4A priority patent/BR112016008641B1/pt
Priority to MX2016004483A priority patent/MX2016004483A/es
Priority to EP14786195.9A priority patent/EP3057700B1/fr
Priority to CN201480057190.9A priority patent/CN105658319B/zh
Priority to PCT/EP2014/072369 priority patent/WO2015055844A1/fr
Publication of FR3012143A1 publication Critical patent/FR3012143A1/fr
Application granted granted Critical
Publication of FR3012143B1 publication Critical patent/FR3012143B1/fr
Active legal-status Critical Current
Anticipated expiration legal-status Critical

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    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C67/00—Preparation of carboxylic acid esters
    • C07C67/18—Preparation of carboxylic acid esters by conversion of a group containing nitrogen into an ester group
    • C07C67/20—Preparation of carboxylic acid esters by conversion of a group containing nitrogen into an ester group from amides or lactams
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J14/00—Chemical processes in general for reacting liquids with liquids; Apparatus specially adapted therefor
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0006—Controlling or regulating processes
    • B01J19/0013—Controlling the temperature of the process
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0006—Controlling or regulating processes
    • B01J19/002—Avoiding undesirable reactions or side-effects, e.g. avoiding explosions, or improving the yield by suppressing side-reactions
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0053—Details of the reactor
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    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
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    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0053—Details of the reactor
    • B01J19/0066—Stirrers
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/02—Apparatus characterised by being constructed of material selected for its chemically-resistant properties
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/18—Stationary reactors having moving elements inside
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/18—Stationary reactors having moving elements inside
    • B01J19/1856—Stationary reactors having moving elements inside placed in parallel
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/18—Stationary reactors having moving elements inside
    • B01J19/1862—Stationary reactors having moving elements inside placed in series
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J4/00—Feed or outlet devices; Feed or outlet control devices
    • B01J4/001—Feed or outlet devices as such, e.g. feeding tubes
    • B01J4/002—Nozzle-type elements
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C231/00—Preparation of carboxylic acid amides
    • C07C231/06—Preparation of carboxylic acid amides from nitriles by transformation of cyano groups into carboxamide groups
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C303/00—Preparation of esters or amides of sulfuric acids; Preparation of sulfonic acids or of their esters, halides, anhydrides or amides
    • C07C303/02—Preparation of esters or amides of sulfuric acids; Preparation of sulfonic acids or of their esters, halides, anhydrides or amides of sulfonic acids or halides thereof
    • C07C303/04—Preparation of esters or amides of sulfuric acids; Preparation of sulfonic acids or of their esters, halides, anhydrides or amides of sulfonic acids or halides thereof by substitution of hydrogen atoms by sulfo or halosulfonyl groups
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/06—Preparation of carboxylic acids or their salts, halides or anhydrides from carboxylic acid amides
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
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    • B01J2219/00002—Chemical plants
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    • B01J2219/00049—Controlling or regulating processes
    • B01J2219/00051—Controlling the temperature
    • B01J2219/00054—Controlling or regulating the heat exchange system
    • B01J2219/00056—Controlling or regulating the heat exchange system involving measured parameters
    • B01J2219/00058—Temperature measurement
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
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    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049—Controlling or regulating processes
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    • B01J2219/00058—Temperature measurement
    • B01J2219/00063—Temperature measurement of the reactants
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
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    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049—Controlling or regulating processes
    • B01J2219/00051—Controlling the temperature
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    • B01J2219/00056—Controlling or regulating the heat exchange system involving measured parameters
    • B01J2219/00065—Pressure measurement
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049—Controlling or regulating processes
    • B01J2219/00051—Controlling the temperature
    • B01J2219/00074—Controlling the temperature by indirect heating or cooling employing heat exchange fluids
    • B01J2219/00076—Controlling the temperature by indirect heating or cooling employing heat exchange fluids with heat exchange elements inside the reactor
    • B01J2219/00081—Tubes
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
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    • B01J2219/00049—Controlling or regulating processes
    • B01J2219/00051—Controlling the temperature
    • B01J2219/00074—Controlling the temperature by indirect heating or cooling employing heat exchange fluids
    • B01J2219/00087—Controlling the temperature by indirect heating or cooling employing heat exchange fluids with heat exchange elements outside the reactor
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    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
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    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049—Controlling or regulating processes
    • B01J2219/00051—Controlling the temperature
    • B01J2219/00074—Controlling the temperature by indirect heating or cooling employing heat exchange fluids
    • B01J2219/00087—Controlling the temperature by indirect heating or cooling employing heat exchange fluids with heat exchange elements outside the reactor
    • B01J2219/00094—Jackets
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    • B01J2219/00761—Details of the reactor
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    • B01J2219/00765—Baffles attached to the reactor wall
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    • B—PERFORMING OPERATIONS; TRANSPORTING
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    • B01J2219/025—Apparatus characterised by their chemically-resistant properties characterised by the construction materials of the reactor vessel proper
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    • B01J2219/025—Apparatus characterised by their chemically-resistant properties characterised by the construction materials of the reactor vessel proper
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    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
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    • B01J2219/02—Apparatus characterised by their chemically-resistant properties
    • B01J2219/025—Apparatus characterised by their chemically-resistant properties characterised by the construction materials of the reactor vessel proper
    • B01J2219/0277—Metal based
    • B01J2219/029—Non-ferrous metals

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
FR1360194A 2013-10-18 2013-10-18 Cuve d'hydrolyse dans un procede d'amidification de cyanohydrine d'acetone Active FR3012143B1 (fr)

Priority Applications (7)

Application Number Priority Date Filing Date Title
FR1360194A FR3012143B1 (fr) 2013-10-18 2013-10-18 Cuve d'hydrolyse dans un procede d'amidification de cyanohydrine d'acetone
BR112016008641-4A BR112016008641B1 (pt) 2013-10-18 2014-10-17 Vaso de hidrólise utilizado em um processo para a amidificação de cianoidrina acetona
MX2016004483A MX2016004483A (es) 2013-10-18 2014-10-17 Recipiente para hidrolisis usando en un proceso para la amidificacion de cianohidrina de acetona.
EP14786195.9A EP3057700B1 (fr) 2013-10-18 2014-10-17 Cuve d'hydrolyse pour un procédé d'amidation d'acétone-cyanhydrine
US15/029,306 US10273199B2 (en) 2013-10-18 2014-10-17 Hydrolysis vessel used in a process for amidification of acetone cyanohydrin
CN201480057190.9A CN105658319B (zh) 2013-10-18 2014-10-17 用于丙酮合氰化氢的酰胺化方法中的水解容器
PCT/EP2014/072369 WO2015055844A1 (fr) 2013-10-18 2014-10-17 Cuve d'hydrolyse utilisée dans un procédé d'amidation d'acétone-cyanhydrine

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
FR1360194A FR3012143B1 (fr) 2013-10-18 2013-10-18 Cuve d'hydrolyse dans un procede d'amidification de cyanohydrine d'acetone

Publications (2)

Publication Number Publication Date
FR3012143A1 FR3012143A1 (fr) 2015-04-24
FR3012143B1 true FR3012143B1 (fr) 2016-08-26

Family

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FR1360194A Active FR3012143B1 (fr) 2013-10-18 2013-10-18 Cuve d'hydrolyse dans un procede d'amidification de cyanohydrine d'acetone

Country Status (7)

Country Link
US (1) US10273199B2 (fr)
EP (1) EP3057700B1 (fr)
CN (1) CN105658319B (fr)
BR (1) BR112016008641B1 (fr)
FR (1) FR3012143B1 (fr)
MX (1) MX2016004483A (fr)
WO (1) WO2015055844A1 (fr)

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CN106588650B (zh) * 2016-03-25 2020-04-17 中国石油集团东北炼化工程有限公司吉林设计院 甲基丙烯酸甲酯制备过程中丙酮氰醇的给料方法和系统
CN110354790B (zh) * 2019-08-15 2024-02-20 山东方明药业集团股份有限公司 一种丹皮酚磺酸的工业化生产方法
CN113467550B (zh) * 2020-03-30 2022-10-04 中石油吉林化工工程有限公司 用于mma生产装置中酰化反应的温控系统及温控方法
CN113457572A (zh) * 2020-03-30 2021-10-01 中石油吉林化工工程有限公司 一种丙酮氰醇低温反应器
CN111635332A (zh) * 2020-06-22 2020-09-08 重庆奕翔化工有限公司 一种酰胺化反应的生产工艺
CN112316855B (zh) * 2020-10-06 2021-09-24 大连理工大学 一种改进的对计量盘密封力可调的微粉计量装置及对应调节方法
JP2023550265A (ja) * 2020-10-23 2023-12-01 レーム・ゲーエムベーハー 転化時の逆混合の低減によるメチルメタクリレートおよび／またはメタクリル酸の改良された製造方法
CN112724846B (zh) * 2021-01-14 2022-08-26 中科华宇(福建)科技发展有限公司 一种标签胶及其制备设备
CN113413861B (zh) * 2021-08-25 2021-11-19 河南科隆新能源股份有限公司 一种锂离子电池正极材料前驱体反应釜
CN113967455B (zh) * 2021-09-28 2023-06-20 郯城众一科环化工有限公司 一种甲烷氢氯化反应器

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EP3057700A1 (fr) 2016-08-24
CN105658319B (zh) 2020-06-26
US10273199B2 (en) 2019-04-30
BR112016008641A2 (fr) 2017-08-01
CN105658319A (zh) 2016-06-08
BR112016008641B1 (pt) 2021-09-08
FR3012143A1 (fr) 2015-04-24
US20160251299A1 (en) 2016-09-01
WO2015055844A1 (fr) 2015-04-23
MX2016004483A (es) 2016-06-21
EP3057700B1 (fr) 2022-08-17

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