JP2010057938A - 噴射用流体の調製方法及び調製装置 - Google Patents
噴射用流体の調製方法及び調製装置 Download PDFInfo
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Abstract
【解決手段】微粉砕した薬剤および/またはバイオポリマーの微粒子をガスで流動化し、細管103内をガス流体により搬送し、該細管103の先端から微細薬剤粉体を目的部位へ噴射する。さらに、細管103内にさらに同軸状にキャピラリーチューブを設け、キャピラリーチューブから薬剤および/またはバイオポリマーの水溶液をチューブ内のガス流に注入し、ガス流動中の他の薬剤および/またはバイオポリマーの微粒子と混合して噴射する。
【選択図】図1
Description
本発明は、細管(マイクロチューブ)を使用してガスによる流動化および噴射を利用することにより、目的部位、特に体腔内の目的部位に、薬剤微細粉末を的確に投与し得る投与装置等に関する。より詳細には、本発明は、薬剤単体もしくはバイオポリマー自体、さらには当該バイオポリマーをキャリヤとして用いて薬剤を噴霧するか、あるいは複数の薬剤の微細粉体、溶液またはその組合せにより噴霧する薬剤ならびにバイオポリマーの投与装置等に関する。
本発明で使用するバイオポリマーとは、ひとつには、いわゆる生体適合性を有する高分子をいい、そのようなバイオポリマーとしては、止血、癒着防止、ケロイド防止、創傷治癒、傷口の接着、シーリング等の作用を有するポリマーである限り特に限定されるものではない。具体的にはカルボキシメチルセルロース、カルボキシエチルセルロース、酸化セルロース、アガロース、キチン、キトサン、ヒアルロン酸、デンプン、グリコーゲン、アルギネート、ペクチン、デキストラン、コンドロイチン硫酸、ゼラチン、コラーゲン等を挙げることができ、これらのバイオポリマーは一種または二種以上のものを使用することができる。
第4図に本実施例1に使用した粉体ガスジェット噴霧装置の模式図を示した。
本装置は、例えば、炭酸ガスボンベあるいは病院内の炭酸ガス配管等のガス供給源(1)から炭酸ガスを圧力調整弁(2)により圧力調整した後、装置(110)内でガス流量弁(3)および流量計(4)によりガスの流量調整を行い、バクテリアフィルター(5)によりガスに含まれている細菌を除去する。ガスと薬剤および/またはバイオポリマーの粉体を、振盪器(6)を有する定量混合器(7)にて粉体を流動化させ、次いでマイクロチューブ(8)内をガスにより搬送し、マイクロチューブ先端から噴霧できるようにしてある。
第5図に本実施例2に使用した粉体ガスジェット噴霧装置の模式図を示した。なお図中の符号は、第4図と同一の意味を有する。
第6図に本実施例3に使用した粉体ガスジェット噴霧装置の模式図を示した。なお図中の符号は、第4図および第5図と同一の意味を有する。
第7図に、本実施例に使用した2本のエアゾールを用いた、ガスジェット噴霧装置の模式的な正面図を示した。本実施例では、流動ガスの供給源に複数(本実施例では2本)の小型ボンベであるエアゾール(20a,20b)を使用し、2個のエアゾール容器にマイクロチューブ(21a,21b)を接続させ、当該マイクロチューブ連結させ、1本になったマイクロチューブ(22)の先端から薬剤および/またはバイオポリマーを噴霧するようにしてある。なお、エアゾールへのマイクロチューブの接続は、好ましくは、プッシュダウンバルブのついた2本のエアゾール容器を、熱収縮性チューブを連結一体化させた2連アクチュエーターを取り付けることにより行うのがよい。
Claims (18)
- 平均粒子径100μm以下の粉体を,ガスで流動性をもたせる流動化工程と,
前記流動化工程による流動化で得られた前記粉体の流動体を,細管であるマイクロチューブで搬送する搬送工程と,
前記マイクロチューブに,流体を注入することにより,当該流体を前記粉体の流動体に混合する混合工程と,
を含み,
これにより,噴射用流体が調製される,
噴射用流体の調製方法。 - 前記マイクロチューブ内には,当該マイクロチューブよりも小径のキャピラリーチューブが設けられており,
前記搬送工程では,
前記粉体の流動体を,前記マイクロチューブの内周面と前記キャピラリーチューブの外周面の間を流れるように搬送し,
前記混合工程では,
前記キャピラリーチューブの排出口から前記流体を流すことにより,前記マイクロチューブ内で前記粉体の流動体に前記流体を混合する,
請求項1に記載の噴射用流体の調製方法。 - 前記流体は,水分を含み,
前記粉体は,水分により粘稠性を示すか又は凝固性を呈するものであり,
前記混合工程では,
前記液体により,前記粉体の流動体中の前記粉体の少なくとも一部がゲル化する,
請求項1又は2に記載の噴射用流体の調製方法。 - 前記粉体は,薬剤を微粉砕することによって得られた微細薬剤粉末であり,
前記流体は,生体適合性又は生体吸収性を有するバイオポリマーの溶液である,
請求項1〜3のいずれか1項に記載の噴射用流体の調製方法。 - 前記粉体は,生体適合性又は生体吸収性を有するバイオポリマーであり,
前記流体は,水,生理食塩水,又は輸液である,
請求項1〜3のいずれか1項に記載の噴射用流体の調製方法。 - 前記粉体は,薬剤を微粉砕することによって得られた微細薬剤粉末であり,
前記流体は,水,生理食塩水,又は輸液である,
請求項1〜3のいずれか1項に記載の噴射用流体の調製方法。 - 前記粉体は,薬剤を微粉砕することによって得られた微細薬剤粉末と,生体適合性又は生体吸収性を有するバイオポリマーの混合物であり,
前記流体は,水,生理食塩水,又は輸液である,
請求項1〜3のいずれか1項に記載の噴射用流体の調製方法。 - 前記マイクロチューブ内には,当該マイクロチューブよりも小径の第1キャピラリーチューブが設けられているとともに,
前記マイクロチューブの内周面と前記第1キャピラリーチューブの外周面の間の空間には,当該マイクロチューブよりも小径の第2キャピラリーチューブが設けられており,
前記調製方法は,さらに,
前記粉体とは別の,平均粒子径100μm以下の第2粉体を,ガスで流動性をもたせる第2流動化工程と,
前記第2流動化工程による流動化で得られた前記第2粉体の流動体を,前記第1キャピラリーチューブで搬送する第2搬送工程と,
を含み,
前記混合工程では,
前記第1キャピラリーチューブの排出口から前記第2粉体の流動体を流すことにより,前記マイクロチューブ内で前記粉体の流動体に前記第2粉体の流動体を混合し,
前記第2キャピラリーチューブの排出口から前記マイクロチューブに前記流体を注入することにより,前記マイクロチューブ内で前記粉体の流動体及び前記第2粉体の流動体の混合物に,前記流体を混合する,
請求項1に記載の噴射用流体の調製方法。 - 前記粉体の流動体の搬送方向において,前記第1キャピラリーチューブの排出口は,前記第2キャピラリーチューブの排出口よりも上流にある,
請求項8に記載の噴射用流体の調製方法。 - 前記粉体が,生体適合性又は生体吸収性を有するバイオポリマーであり,かつ,前記第2粉体は,薬剤を微粉砕することによって得られた微細薬剤粉末であるか,
又は,
前記粉体が,薬剤を微粉砕することによって得られた微細薬剤粉末であり,かつ,前記第2粉体が,生体適合性又は生体吸収性を有するバイオポリマーである,
請求項6又は7に記載の噴射用流体の調製方法。 - 前記流体は,水分を含み,
前記粉体は,水分により粘稠性を示すか又は凝固性を呈するものであり,
前記混合工程では,
前記流体により,前記粉体の流動体中の前記粉体の少なくとも一部又は前記第2粉体の流動体中の前記第2粉体がゲル化する,
請求項6〜8のいずれか1項に記載の噴射用流体の調製方法。 - 前記調製方法は,さらに,
前記混合工程において互いに混合される粉体及び流体の相対的な混合比を変更する変更工程を含み,
これにより,前記マイクロチューブ内を移動する前記噴射用流体に濃度勾配をもたせる,
請求項1〜11のいずれか1項に記載の噴射用流体の調製方法。 - 平均粒子径100μm以下の粉体を溶液にした粉体溶液を,ガスで流動性をもたせる流動化工程と,
前記流動化工程による流動化で得られた前記粉体溶液の流動体を,細管であるマイクロチューブで搬送する搬送工程と,
を含み,
これにより,噴射用流体を調製する,
噴射用流体の調製方法。 - 前記マイクロチューブ内には,当該マイクロチューブよりも小径のキャピラリーチューブが設けられており,
前記搬送工程では,
前記粉体溶液の流動体を,前記マイクロチューブの内周面と前記キャピラリーチューブの外周面の間を流れるように搬送し,
前記調製方法は,さらに,
前記粉体とは別の,平均粒子径100μm以下の第2粉体を溶液にした第2粉体溶液を,前記キャピラリーチューブの排出口から注入することにより,前記マイクロチューブ内で前記粉体溶液の流動体と前記第2粉体溶液とを互いに混合する混合工程を含む,
請求項13に記載の噴射用流体の調製方法。 - 前記粉体が,生体適合性又は生体吸収性を有するバイオポリマーであり,かつ,前記第2粉体が,薬剤を微粉砕することによって得られた微細薬剤粉末であるか,
又は,
前記粉体が,薬剤を微粉砕することによって得られた微細薬剤粉末であり,かつ,前記第2粉体が,生体適合性又は生体吸収性を有するバイオポリマーである,
請求項14に記載の噴射用流体の調製方法。 - 前記粉体と前記第2粉体とは溶液中において互いに逆の電荷をもち,
前記混合工程では,
前記粉体溶液の流動体と前記第2粉体溶液の流動体とを互いに混合することで,前記粉体と前記第2粉体とを互いに結合させる,
請求項14又は15に記載の噴射用流体の調製方法。 - 平均粒子径100μm以下の粉体又はその溶液を,ガスで搬送するための,細管であるマイクロチューブを含む,噴射用流体の調製装置。
- 前記マイクロチューブよりも小径のキャピラリーチューブを含み,当該キャピラリーチューブの排出口が前記マイクロチューブ内に設けられており,
これにより,前記キャピラリーチューブの排出口から,前記粉体とは別の第2粉体若しくはその溶液,又は流体を前記マイクロチューブに注入することが可能である,
請求項17に記載の噴射用流体の調製装置。
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- 2003-02-18 US US10/505,205 patent/US7427607B2/en not_active Expired - Lifetime
- 2003-02-18 AU AU2003211376A patent/AU2003211376A1/en not_active Abandoned
- 2003-02-18 CN CN03804368.8A patent/CN1635853B/zh not_active Expired - Fee Related
- 2003-02-18 JP JP2003569073A patent/JP4474165B2/ja not_active Expired - Lifetime
- 2003-02-18 EP EP03705264A patent/EP1477119A4/en not_active Withdrawn
- 2003-02-18 WO PCT/JP2003/001693 patent/WO2003070110A1/ja active Application Filing
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Also Published As
Publication number | Publication date |
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JPWO2003070110A1 (ja) | 2005-06-09 |
AU2003211376A1 (en) | 2003-09-09 |
JP4474165B2 (ja) | 2010-06-02 |
US20050123485A1 (en) | 2005-06-09 |
CN1635853B (zh) | 2010-05-12 |
CN1635853A (zh) | 2005-07-06 |
JP4461200B2 (ja) | 2010-05-12 |
CN101898004A (zh) | 2010-12-01 |
US7427607B2 (en) | 2008-09-23 |
EP1477119A4 (en) | 2009-06-10 |
EP1477119A1 (en) | 2004-11-17 |
WO2003070110A1 (fr) | 2003-08-28 |
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