JP2009527529A5 - - Google Patents
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- Publication number
- JP2009527529A5 JP2009527529A5 JP2008555774A JP2008555774A JP2009527529A5 JP 2009527529 A5 JP2009527529 A5 JP 2009527529A5 JP 2008555774 A JP2008555774 A JP 2008555774A JP 2008555774 A JP2008555774 A JP 2008555774A JP 2009527529 A5 JP2009527529 A5 JP 2009527529A5
- Authority
- JP
- Japan
- Prior art keywords
- alkanol
- stream
- rich stream
- carbonate
- dialkyl carbonate
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 claims description 21
- BVKZGUZCCUSVTD-UHFFFAOYSA-L Carbonate Chemical compound [O-]C([O-])=O BVKZGUZCCUSVTD-UHFFFAOYSA-L 0.000 claims description 13
- 150000001875 compounds Chemical class 0.000 claims description 12
- 238000009835 boiling Methods 0.000 claims description 9
- 238000000066 reactive distillation Methods 0.000 claims description 9
- 238000000034 method Methods 0.000 claims description 7
- -1 alkylene carbonate Chemical compound 0.000 claims description 5
- 238000000926 separation method Methods 0.000 claims description 5
- 238000004064 recycling Methods 0.000 claims description 2
- 238000005809 transesterification reaction Methods 0.000 claims description 2
- RUOJZAUFBMNUDX-UHFFFAOYSA-N propylene carbonate Chemical group CC1COC(=O)O1 RUOJZAUFBMNUDX-UHFFFAOYSA-N 0.000 claims 1
- 238000000746 purification Methods 0.000 claims 1
- 239000000356 contaminant Substances 0.000 description 4
- 238000004821 distillation Methods 0.000 description 4
- 238000010586 diagram Methods 0.000 description 3
- IEJIGPNLZYLLBP-UHFFFAOYSA-N dimethyl carbonate Chemical compound COC(=O)OC IEJIGPNLZYLLBP-UHFFFAOYSA-N 0.000 description 3
- 238000000895 extractive distillation Methods 0.000 description 3
- 239000007788 liquid Substances 0.000 description 3
- GOOHAUXETOMSMM-UHFFFAOYSA-N Propylene oxide Chemical compound CC1CO1 GOOHAUXETOMSMM-UHFFFAOYSA-N 0.000 description 2
- 239000006227 byproduct Substances 0.000 description 2
- 238000006243 chemical reaction Methods 0.000 description 2
- 239000000203 mixture Substances 0.000 description 2
- YSVZGWAJIHWNQK-UHFFFAOYSA-N [3-(hydroxymethyl)-2-bicyclo[2.2.1]heptanyl]methanol Chemical compound C1CC2C(CO)C(CO)C1C2 YSVZGWAJIHWNQK-UHFFFAOYSA-N 0.000 description 1
- 239000007791 liquid phase Substances 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 238000010992 reflux Methods 0.000 description 1
- 239000012808 vapor phase Substances 0.000 description 1
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US77546906P | 2006-02-22 | 2006-02-22 | |
| US60/775,469 | 2006-02-22 | ||
| PCT/EP2007/051585 WO2007096342A1 (en) | 2006-02-22 | 2007-02-20 | Process for the preparation of an alkanediol and a dialkyl carbonate |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| JP2009527529A JP2009527529A (ja) | 2009-07-30 |
| JP2009527529A5 true JP2009527529A5 (enExample) | 2013-02-07 |
| JP5322658B2 JP5322658B2 (ja) | 2013-10-23 |
Family
ID=38024231
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2008555774A Expired - Fee Related JP5322658B2 (ja) | 2006-02-22 | 2007-02-20 | アルカンジオールおよびジアルキルカーボネートの調製方法 |
Country Status (7)
| Country | Link |
|---|---|
| US (1) | US7563919B2 (enExample) |
| EP (1) | EP1986988B1 (enExample) |
| JP (1) | JP5322658B2 (enExample) |
| KR (1) | KR20080105088A (enExample) |
| CN (1) | CN101389591B (enExample) |
| TW (1) | TWI378087B (enExample) |
| WO (1) | WO2007096342A1 (enExample) |
Families Citing this family (13)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| TWI383976B (zh) * | 2006-02-22 | 2013-02-01 | Shell Int Research | 製備碳酸二烷酯及烷二醇的方法 |
| CN101605751B (zh) * | 2007-01-23 | 2013-01-02 | 国际壳牌研究有限公司 | 制备烷二醇和二甲基碳酸酯的方法 |
| RU2461541C2 (ru) * | 2007-01-23 | 2012-09-20 | Шелл Интернэшнл Рисерч Маатсхаппий Б.В. | Способ получения алкандиола и диалкилкарбоната |
| WO2008099370A2 (en) * | 2007-02-16 | 2008-08-21 | Sabic Innovative Plastics Ip Bv | Process for manufacturing dimethyl carbonate |
| CN101627003B (zh) * | 2007-02-16 | 2016-03-16 | 沙特基础全球技术有限公司 | 碳酸二甲酯的制备方法 |
| TW200906774A (en) * | 2007-04-23 | 2009-02-16 | Shell Int Research | Process for the preparation of an 1,2-alkylene diol and a dialkylcarbonate |
| US20100121078A1 (en) * | 2008-05-06 | 2010-05-13 | Cyrille Paul Allais | Process for preparing alkanediol and dialkyl carbonate |
| DE102009030680A1 (de) * | 2009-06-26 | 2010-12-30 | Bayer Materialscience Ag | Verfahren zur Herstellung von Dialkylcarbonaten aus Alkylencarbonaten und Alkoholen |
| EP2464620B1 (en) * | 2009-08-12 | 2013-10-02 | Shell Internationale Research Maatschappij B.V. | Process for removing an alkanol impurity from a dialkyl carbonate stream |
| US9475751B2 (en) * | 2012-11-21 | 2016-10-25 | Covestro Deutschland Ag | Process for producing dialkyl carbonates |
| CN105646219A (zh) * | 2016-01-24 | 2016-06-08 | 辽宁会福化工有限公司 | 一种利用强酸性阳离子树脂催化合成碳酸二乙酯的方法 |
| WO2020075152A2 (en) | 2018-10-11 | 2020-04-16 | Shell Oil Company | A composition and uses thereof |
| WO2025057960A1 (ja) * | 2023-09-15 | 2025-03-20 | 旭化成株式会社 | アリール基を有するカーボネートの製造方法 |
Family Cites Families (49)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2994705A (en) * | 1958-12-08 | 1961-08-01 | Pure Oil Co | Preparation of cyclic alkylene carbonates in the presence of organic phosphonium compounds |
| US3803201A (en) * | 1971-02-22 | 1974-04-09 | Dow Chemical Co | Synthesis of dimethyl carbonate |
| DE2740243A1 (de) | 1977-09-07 | 1979-03-15 | Bayer Ag | Verfahren zur herstellung von dialkylcarbonaten |
| DE2748718A1 (de) * | 1977-10-29 | 1979-05-03 | Bayer Ag | Verfahren zur herstellung von dialkylcarbonaten |
| US4314945A (en) * | 1977-12-22 | 1982-02-09 | Union Carbide Corporation | Alkylene carbonate process |
| JPS6022698B2 (ja) | 1978-11-08 | 1985-06-03 | 日曹油化工業株式会社 | ジアルキル炭酸エステルの製法 |
| GB8307613D0 (en) | 1983-03-18 | 1983-04-27 | Bp Chem Int Ltd | Carbonates |
| US4508927A (en) * | 1983-08-02 | 1985-04-02 | The Halcon Sd Group, Inc. | Preparation of glycols from ethylene oxide |
| US4851555A (en) | 1984-10-25 | 1989-07-25 | Scientific Design Company, Inc. | Process for preparing alkylene oxides from alkylene carbonates |
| JPS61291545A (ja) | 1985-06-18 | 1986-12-22 | Daicel Chem Ind Ltd | 炭酸エステルの製造方法 |
| US4691041A (en) * | 1986-01-03 | 1987-09-01 | Texaco Inc. | Process for production of ethylene glycol and dimethyl carbonate |
| FR2608812B1 (fr) | 1986-12-23 | 1989-04-07 | Organo Synthese Ste Fse | Procede de preparation de carbonates organiques par transesterification |
| US4877886A (en) | 1987-06-19 | 1989-10-31 | Union Carbide Chemicals And Plastics Company Inc. | Process for the production of alkylene carbonate |
| JP2557099B2 (ja) | 1989-02-13 | 1996-11-27 | ダイセル化学工業株式会社 | ジメチルカーボネートの分離方法 |
| CN1060091A (zh) | 1990-09-21 | 1992-04-08 | 北京理工大学 | 二羟乙二肟的合成 |
| DE4030283A1 (de) * | 1990-09-25 | 1992-03-26 | Ruetgerswerke Ag | Verfahren zur herstellung cyclischer carbonate |
| GB2255972A (en) * | 1991-04-12 | 1992-11-25 | Davy Res & Dev Ltd | Production of diaryl carbonates. |
| DE4129316A1 (de) * | 1991-09-03 | 1993-03-04 | Bayer Ag | Verfahren zur kontinuierlichen herstellung von dialkylcarbonaten |
| DE4216121A1 (de) * | 1992-05-15 | 1993-11-18 | Bayer Ag | Verfahren zur kontinuierlichen Herstellung von Dialkylcarbonaten |
| KR940003917A (ko) | 1992-08-20 | 1994-03-14 | 고지마 아끼로 | 반응 제어방법 |
| DE4318892A1 (de) * | 1993-06-07 | 1994-12-08 | Bayer Ag | Verfahren zur Herstellung von Propylenglykolcarbonat |
| DE4318893A1 (de) * | 1993-06-07 | 1994-12-08 | Bayer Ag | Reaktor und damit durchzuführendes kontinuierliches Verfahren zur Herstellung von Ethylenglykolcarbonat bzw. Propylenglykolcarbonat |
| DE4342713A1 (de) * | 1993-12-15 | 1995-06-22 | Bayer Ag | Verfahren zur Abtrennung von Methanol aus einem Gemisch von Dimethylcarbonat und Methanol |
| CN1049212C (zh) | 1994-06-24 | 2000-02-09 | 华东理工大学 | 一种改进的碳酸二烷基酯的合成方法 |
| JP3652035B2 (ja) | 1995-10-31 | 2005-05-25 | 旭化成ケミカルズ株式会社 | ジアルキルカーボネートおよびジオールの連続的製造法 |
| US5763691A (en) | 1995-11-30 | 1998-06-09 | Mitsubishi Chemical Corporation | Ethylene glycol process |
| DE69620470T2 (de) * | 1995-12-22 | 2002-11-21 | Asahi Kasei Kabushiki Kaisha, Osaka | Verfahren zur kontinuierlichen herstellung von dialkylcarbonaten und diolen |
| DE19819586A1 (de) | 1998-04-30 | 1999-11-04 | Basf Ag | Verfahren zur kontinuierlichen Herstellung von 1,3-Dioxolan-2-onen |
| JP2000005503A (ja) | 1998-06-24 | 2000-01-11 | Nippon Shokubai Co Ltd | 反応蒸留装置および反応蒸留方法 |
| SG77264A1 (en) * | 1998-08-10 | 2000-12-19 | Mitsubishi Chem Corp | Process for producing an alkylene glycol |
| JP2000113144A (ja) | 1998-10-06 | 2000-04-21 | Hitachi Chem Co Ltd | 非接触式icカード |
| US6156160A (en) * | 1998-10-07 | 2000-12-05 | Huntsman Petrochemical Corporation | Alkylene carbonate process |
| AU2827900A (en) * | 1999-03-03 | 2000-09-21 | Asahi Kasei Kabushiki Kaisha | Process for continuously producing dialkyl carbonate and diol |
| US6407279B1 (en) * | 1999-11-19 | 2002-06-18 | Exxonmobil Chemical Patents Inc. | Integrated process for preparing dialkyl carbonates and diols |
| US6294684B1 (en) * | 1999-12-08 | 2001-09-25 | General Electric Company | Method and apparatus for the continuous production of diaryl carbonates |
| JP3659109B2 (ja) * | 2000-01-19 | 2005-06-15 | 三菱化学株式会社 | エチレングリコールと炭酸エステルの併産方法 |
| US6392078B1 (en) * | 2000-06-12 | 2002-05-21 | Catalytic Distillation Technologies | Process and catalyst for making dialkyl carbonates |
| US6774256B2 (en) * | 2001-06-22 | 2004-08-10 | Exxonmobil Chemical Patents Inc. | Low corrosive integrated process for preparing dialkyl carbonates |
| WO2003006418A1 (en) | 2001-07-10 | 2003-01-23 | Mitsubishi Chemical Corporation | Method for producing dialkylcarbonate |
| JP2003081893A (ja) | 2001-09-10 | 2003-03-19 | Mitsui Chemicals Inc | ジアルキルカーボネートとグリコールの連続的同時製造方法 |
| US6573396B2 (en) * | 2001-10-12 | 2003-06-03 | Exxonmobil Chemical Patents Inc. | Co-production of dialkyl carbonates and diols with treatment of hydroxy alkyl carbonate |
| JP3969065B2 (ja) | 2001-11-19 | 2007-08-29 | 三菱化学株式会社 | アルキルアリールカーボネートの製造方法 |
| JP3960525B2 (ja) * | 2002-03-13 | 2007-08-15 | 三菱化学株式会社 | ジメチルカーボネート及びエチレングリコールの製造方法 |
| JP2003300936A (ja) * | 2002-04-09 | 2003-10-21 | Mitsui Chemicals Inc | ジアルキルカーボネートとグリコールの連続同時製造方法 |
| JP4000912B2 (ja) | 2002-05-30 | 2007-10-31 | 三菱化学株式会社 | ジメチルカーボネートの製造方法 |
| TW200503997A (en) | 2002-12-20 | 2005-02-01 | Shell Int Research | Process for the preparation of alkylene glycol |
| ES2293327T3 (es) | 2003-06-30 | 2008-03-16 | Shell Internationale Research Maatschappij B.V. | Procedimiento para la preparacion de carbonato de propileno. |
| CN1241900C (zh) | 2003-10-16 | 2006-02-15 | 华东理工大学 | 一种联产碳酸二烷基酯和二元醇的方法 |
| US20050148787A1 (en) | 2003-11-26 | 2005-07-07 | Beckers Johannes Gerhardus J. | Process for the preparation of propylene carbonate |
-
2007
- 2007-02-16 TW TW096106260A patent/TWI378087B/zh not_active IP Right Cessation
- 2007-02-20 CN CN2007800064459A patent/CN101389591B/zh not_active Expired - Fee Related
- 2007-02-20 JP JP2008555774A patent/JP5322658B2/ja not_active Expired - Fee Related
- 2007-02-20 KR KR1020087022816A patent/KR20080105088A/ko not_active Withdrawn
- 2007-02-20 EP EP07704658.9A patent/EP1986988B1/en not_active Not-in-force
- 2007-02-20 WO PCT/EP2007/051585 patent/WO2007096342A1/en not_active Ceased
- 2007-02-22 US US11/677,999 patent/US7563919B2/en not_active Expired - Fee Related
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