JP2009506121A5 - - Google Patents
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- Publication number
- JP2009506121A5 JP2009506121A5 JP2008529178A JP2008529178A JP2009506121A5 JP 2009506121 A5 JP2009506121 A5 JP 2009506121A5 JP 2008529178 A JP2008529178 A JP 2008529178A JP 2008529178 A JP2008529178 A JP 2008529178A JP 2009506121 A5 JP2009506121 A5 JP 2009506121A5
- Authority
- JP
- Japan
- Prior art keywords
- alkali metal
- alkaline earth
- metal
- earth metal
- hydroxide
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- -1 alkali metal amide Chemical class 0.000 claims description 10
- 229910052783 alkali metal Inorganic materials 0.000 claims description 8
- 229910052784 alkaline earth metal Inorganic materials 0.000 claims description 7
- 150000001342 alkaline earth metals Chemical class 0.000 claims description 3
- 239000002585 base Substances 0.000 claims description 3
- 229910000288 alkali metal carbonate Inorganic materials 0.000 claims description 2
- 150000008041 alkali metal carbonates Chemical class 0.000 claims description 2
- 150000008044 alkali metal hydroxides Chemical class 0.000 claims description 2
- 229910000272 alkali metal oxide Inorganic materials 0.000 claims description 2
- 229910001860 alkaline earth metal hydroxide Inorganic materials 0.000 claims description 2
- 229910000287 alkaline earth metal oxide Inorganic materials 0.000 claims description 2
- 150000004791 alkyl magnesium halides Chemical class 0.000 claims description 2
- 229910001038 basic metal oxide Inorganic materials 0.000 claims description 2
- 150000004679 hydroxides Chemical class 0.000 claims description 2
- 150000002902 organometallic compounds Chemical class 0.000 claims description 2
- 229910000102 alkali metal hydride Inorganic materials 0.000 claims 1
- 150000008046 alkali metal hydrides Chemical class 0.000 claims 1
- 150000001340 alkali metals Chemical class 0.000 claims 1
- WMFOQBRAJBCJND-UHFFFAOYSA-M Lithium hydroxide Chemical compound [Li+].[OH-] WMFOQBRAJBCJND-UHFFFAOYSA-M 0.000 description 3
- KWYUFKZDYYNOTN-UHFFFAOYSA-M Potassium hydroxide Chemical compound [OH-].[K+] KWYUFKZDYYNOTN-UHFFFAOYSA-M 0.000 description 3
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 3
- VTYYLEPIZMXCLO-UHFFFAOYSA-L Calcium carbonate Chemical compound [Ca+2].[O-]C([O-])=O VTYYLEPIZMXCLO-UHFFFAOYSA-L 0.000 description 2
- MZRVEZGGRBJDDB-UHFFFAOYSA-N N-Butyllithium Chemical compound [Li]CCCC MZRVEZGGRBJDDB-UHFFFAOYSA-N 0.000 description 2
- UIIMBOGNXHQVGW-UHFFFAOYSA-M Sodium bicarbonate Chemical compound [Na+].OC([O-])=O UIIMBOGNXHQVGW-UHFFFAOYSA-M 0.000 description 2
- XLOMVQKBTHCTTD-UHFFFAOYSA-N Zinc monoxide Chemical compound [Zn]=O XLOMVQKBTHCTTD-UHFFFAOYSA-N 0.000 description 2
- NTTOTNSKUYCDAV-UHFFFAOYSA-N potassium hydride Chemical compound [KH] NTTOTNSKUYCDAV-UHFFFAOYSA-N 0.000 description 2
- 229910000105 potassium hydride Inorganic materials 0.000 description 2
- ZFFBIQMNKOJDJE-UHFFFAOYSA-N 2-bromo-1,2-diphenylethanone Chemical compound C=1C=CC=CC=1C(Br)C(=O)C1=CC=CC=C1 ZFFBIQMNKOJDJE-UHFFFAOYSA-N 0.000 description 1
- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 description 1
- KEAYESYHFKHZAL-UHFFFAOYSA-N Sodium Chemical compound [Na] KEAYESYHFKHZAL-UHFFFAOYSA-N 0.000 description 1
- QCWXUUIWCKQGHC-UHFFFAOYSA-N Zirconium Chemical compound [Zr] QCWXUUIWCKQGHC-UHFFFAOYSA-N 0.000 description 1
- PVOXCLVRHYZZEP-UHFFFAOYSA-M [OH-].[O-2].[Ti+3] Chemical compound [OH-].[O-2].[Ti+3] PVOXCLVRHYZZEP-UHFFFAOYSA-M 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 239000003513 alkali Substances 0.000 description 1
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 description 1
- 229910000019 calcium carbonate Inorganic materials 0.000 description 1
- AXCZMVOFGPJBDE-UHFFFAOYSA-L calcium dihydroxide Chemical compound [OH-].[OH-].[Ca+2] AXCZMVOFGPJBDE-UHFFFAOYSA-L 0.000 description 1
- 239000000920 calcium hydroxide Substances 0.000 description 1
- 229910001861 calcium hydroxide Inorganic materials 0.000 description 1
- 239000000292 calcium oxide Substances 0.000 description 1
- ODINCKMPIJJUCX-UHFFFAOYSA-N calcium oxide Inorganic materials [Ca]=O ODINCKMPIJJUCX-UHFFFAOYSA-N 0.000 description 1
- 150000002484 inorganic compounds Chemical class 0.000 description 1
- 229910010272 inorganic material Inorganic materials 0.000 description 1
- 150000002500 ions Chemical class 0.000 description 1
- AFRJJFRNGGLMDW-UHFFFAOYSA-N lithium amide Chemical compound [Li+].[NH2-] AFRJJFRNGGLMDW-UHFFFAOYSA-N 0.000 description 1
- XGZVUEUWXADBQD-UHFFFAOYSA-L lithium carbonate Chemical compound [Li+].[Li+].[O-]C([O-])=O XGZVUEUWXADBQD-UHFFFAOYSA-L 0.000 description 1
- 229910052808 lithium carbonate Inorganic materials 0.000 description 1
- SIAPCJWMELPYOE-UHFFFAOYSA-N lithium hydride Chemical compound [LiH] SIAPCJWMELPYOE-UHFFFAOYSA-N 0.000 description 1
- 229910000103 lithium hydride Inorganic materials 0.000 description 1
- FUJCRWPEOMXPAD-UHFFFAOYSA-N lithium oxide Chemical compound [Li+].[Li+].[O-2] FUJCRWPEOMXPAD-UHFFFAOYSA-N 0.000 description 1
- 229910001947 lithium oxide Inorganic materials 0.000 description 1
- 239000000395 magnesium oxide Substances 0.000 description 1
- CPLXHLVBOLITMK-UHFFFAOYSA-N magnesium oxide Inorganic materials [Mg]=O CPLXHLVBOLITMK-UHFFFAOYSA-N 0.000 description 1
- CCERQOYLJJULMD-UHFFFAOYSA-M magnesium;carbanide;chloride Chemical compound [CH3-].[Mg+2].[Cl-] CCERQOYLJJULMD-UHFFFAOYSA-M 0.000 description 1
- CRGZYKWWYNQGEC-UHFFFAOYSA-N magnesium;methanolate Chemical compound [Mg+2].[O-]C.[O-]C CRGZYKWWYNQGEC-UHFFFAOYSA-N 0.000 description 1
- AXZKOIWUVFPNLO-UHFFFAOYSA-N magnesium;oxygen(2-) Chemical compound [O-2].[Mg+2] AXZKOIWUVFPNLO-UHFFFAOYSA-N 0.000 description 1
- 229910052987 metal hydride Inorganic materials 0.000 description 1
- 150000004681 metal hydrides Chemical class 0.000 description 1
- 229910000000 metal hydroxide Inorganic materials 0.000 description 1
- 229910021645 metal ion Inorganic materials 0.000 description 1
- DVSDBMFJEQPWNO-UHFFFAOYSA-N methyllithium Chemical compound C[Li] DVSDBMFJEQPWNO-UHFFFAOYSA-N 0.000 description 1
- 230000003647 oxidation Effects 0.000 description 1
- 238000007254 oxidation reaction Methods 0.000 description 1
- NHKJPPKXDNZFBJ-UHFFFAOYSA-N phenyllithium Chemical compound [Li]C1=CC=CC=C1 NHKJPPKXDNZFBJ-UHFFFAOYSA-N 0.000 description 1
- RPDAUEIUDPHABB-UHFFFAOYSA-N potassium ethoxide Chemical compound [K+].CC[O-] RPDAUEIUDPHABB-UHFFFAOYSA-N 0.000 description 1
- LPNYRYFBWFDTMA-UHFFFAOYSA-N potassium tert-butoxide Chemical compound [K+].CC(C)(C)[O-] LPNYRYFBWFDTMA-UHFFFAOYSA-N 0.000 description 1
- 238000000746 purification Methods 0.000 description 1
- 229910052708 sodium Inorganic materials 0.000 description 1
- 239000011734 sodium Substances 0.000 description 1
- ODZPKZBBUMBTMG-UHFFFAOYSA-N sodium amide Chemical compound [NH2-].[Na+] ODZPKZBBUMBTMG-UHFFFAOYSA-N 0.000 description 1
- 229910000030 sodium bicarbonate Inorganic materials 0.000 description 1
- 235000017557 sodium bicarbonate Nutrition 0.000 description 1
- QDRKDTQENPPHOJ-UHFFFAOYSA-N sodium ethoxide Chemical compound [Na+].CC[O-] QDRKDTQENPPHOJ-UHFFFAOYSA-N 0.000 description 1
- 239000012312 sodium hydride Substances 0.000 description 1
- 229910000104 sodium hydride Inorganic materials 0.000 description 1
- KKCBUQHMOMHUOY-UHFFFAOYSA-N sodium oxide Chemical compound [O-2].[Na+].[Na+] KKCBUQHMOMHUOY-UHFFFAOYSA-N 0.000 description 1
- 229910001948 sodium oxide Inorganic materials 0.000 description 1
- XOLBLPGZBRYERU-UHFFFAOYSA-N tin dioxide Chemical compound O=[Sn]=O XOLBLPGZBRYERU-UHFFFAOYSA-N 0.000 description 1
- 229910001887 tin oxide Inorganic materials 0.000 description 1
- 239000011787 zinc oxide Substances 0.000 description 1
- 229910001928 zirconium oxide Inorganic materials 0.000 description 1
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US71231205P | 2005-08-30 | 2005-08-30 | |
| US60/712,312 | 2005-08-30 | ||
| PCT/US2006/033618 WO2007027649A1 (en) | 2005-08-30 | 2006-08-28 | Method for synthesizing spiro quaternary ammonium systems |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| JP2009506121A JP2009506121A (ja) | 2009-02-12 |
| JP2009506121A5 true JP2009506121A5 (enExample) | 2009-05-14 |
| JP5264488B2 JP5264488B2 (ja) | 2013-08-14 |
Family
ID=37574897
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2008529178A Expired - Fee Related JP5264488B2 (ja) | 2005-08-30 | 2006-08-28 | スピロ四級アンモニウム系の合成方法 |
Country Status (9)
| Country | Link |
|---|---|
| US (2) | US8426593B2 (enExample) |
| EP (1) | EP1919922B1 (enExample) |
| JP (1) | JP5264488B2 (enExample) |
| KR (1) | KR101388915B1 (enExample) |
| CN (1) | CN101300260B (enExample) |
| AT (1) | ATE506366T1 (enExample) |
| DE (2) | DE602006021437D1 (enExample) |
| TW (1) | TW200745129A (enExample) |
| WO (1) | WO2007027649A1 (enExample) |
Families Citing this family (42)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE602006021437D1 (de) * | 2005-08-30 | 2011-06-01 | Honeywell Int Inc | Verfahren zur synthese von quaternären ammonium-spirosystemen |
| JP2007077046A (ja) * | 2005-09-12 | 2007-03-29 | Tomiyama Pure Chemical Industries Ltd | スピロ化合物類の製造方法。 |
| US20110070486A1 (en) * | 2008-09-10 | 2011-03-24 | National Institute Of Advanced Industrial Science And Technology | Ionic liquid |
| WO2011113111A1 (en) * | 2010-03-18 | 2011-09-22 | Commonwealth Scientific And Industrial Research Organisation | Ionic liquids for batteries |
| WO2011136383A1 (en) | 2010-04-26 | 2011-11-03 | Dainippon Sumitomo Pharma Co., Ltd. | A process of a quaternary ammonium salt |
| ES2527545T3 (es) * | 2010-04-26 | 2015-01-26 | Sumitomo Dainippon Pharma Co., Ltd. | Un procedimiento de preparación de una sal de amonio cuaternario utilizando fosfato |
| TW201218480A (en) * | 2010-09-30 | 2012-05-01 | Basf Se | Additive for electrolytes |
| CN102070651B (zh) * | 2010-12-18 | 2012-11-07 | 渤海大学 | 一种超级电容器有机电解质氧杂螺环季铵盐的制备方法 |
| CN102093367B (zh) * | 2010-12-18 | 2013-02-27 | 渤海大学 | 一种超级电容器有机电解质螺环季铵盐的制备方法 |
| CN102074366B (zh) * | 2010-12-30 | 2012-07-04 | 苏州方昇光电装备技术有限公司 | 一种混合型离子液体电解质及其制备方法和应用 |
| US8961809B2 (en) * | 2011-01-21 | 2015-02-24 | Corning Incorporated | Electrolyte synthesis for ultracapacitors |
| CN102496469A (zh) * | 2011-12-05 | 2012-06-13 | 上海奥威科技开发有限公司 | 高功率双电层电容器 |
| JP5780484B2 (ja) * | 2012-02-28 | 2015-09-16 | 国立研究開発法人産業技術総合研究所 | イオン液体 |
| JP2014088361A (ja) | 2012-04-27 | 2014-05-15 | Semiconductor Energy Lab Co Ltd | 環状４級アンモニウム塩、非水溶媒、非水電解質及び蓄電装置 |
| JP6370449B2 (ja) * | 2012-04-27 | 2018-08-08 | 株式会社半導体エネルギー研究所 | 非水溶媒、蓄電装置 |
| JP2016500200A (ja) * | 2012-11-20 | 2016-01-07 | コーニング インコーポレイテッド | ウルトラキャパシタのための電解質合成 |
| CN103050292A (zh) * | 2012-12-20 | 2013-04-17 | 上海奥威科技开发有限公司 | 一种高功率双电层电容器 |
| JP5572844B1 (ja) * | 2013-09-05 | 2014-08-20 | 新シコー科技株式会社 | 振動装置、振動装置を用いた電子機器及び身体装着品 |
| CN104576081B (zh) * | 2013-10-24 | 2017-11-14 | 中国科学院长春应用化学研究所 | 防凝固型电解液及超级电容器 |
| US20150158020A1 (en) * | 2013-12-11 | 2015-06-11 | Uop Llc | Synthesis of zeolites using an organoammonium compound |
| WO2015124504A1 (de) * | 2014-02-18 | 2015-08-27 | Bayer Materialscience Ag | Verfahren zur isocyanatmodifizierung unter verwendung von spirocyclischen ammoniumsalzen als katalysator |
| CN104059076B (zh) * | 2014-04-29 | 2016-11-02 | 宁波中车新能源科技有限公司 | 一种电容器电解质螺环季铵盐的制备方法 |
| CN104387386B (zh) * | 2014-10-29 | 2016-08-24 | 江苏国泰超威新材料有限公司 | 一种对称螺环季铵盐电解质的制备方法 |
| CN104387397B (zh) * | 2014-10-29 | 2016-08-17 | 江苏国泰超威新材料有限公司 | 一种螺环季铵盐电解质的制备方法 |
| CN104505264B (zh) * | 2014-12-06 | 2017-10-20 | 中国铝业股份有限公司 | 一种无卤素螺环季铵盐的合成方法 |
| CN105732645B (zh) * | 2014-12-11 | 2018-11-09 | 华东理工常熟研究院有限公司 | 一种螺环季铵盐的制备方法 |
| CN104650095B (zh) * | 2015-02-16 | 2017-06-06 | 衢州康鹏化学有限公司 | 一种四氟硼酸螺环季铵盐的制备方法 |
| CN104779075A (zh) * | 2015-03-26 | 2015-07-15 | 珠海市赛纬电子材料有限公司 | 一种超级电容器高电压非水电解液 |
| WO2017137343A1 (en) | 2016-02-11 | 2017-08-17 | Covestro Deutschland Ag | Sustainable synthesis of carbamate compounds |
| CN106117218B (zh) * | 2016-06-23 | 2018-09-14 | 东莞东阳光科研发有限公司 | 一种四氟硼酸螺环季铵盐的制备方法 |
| CN106316862B (zh) * | 2016-08-19 | 2019-01-08 | 上海康鹏科技有限公司 | 一种四氟硼酸季铵盐的制备方法 |
| CN106674232A (zh) * | 2017-01-04 | 2017-05-17 | 湖南省正源储能材料与器件研究所 | 一种用离子交换净化法制备高纯螺环季铵盐的方法 |
| KR101830636B1 (ko) * | 2017-01-04 | 2018-02-21 | 삼화페인트공업주식회사 | 스피로 4차 암모늄 염의 제조 방법 |
| ES2917404T3 (es) | 2017-02-22 | 2022-07-08 | Covestro Intellectual Property Gmbh & Co Kg | Procedimiento para la modificación de al menos diisocianato de pentametileno usando sales de amonio espirocíclicas como catalizador |
| EP3444288A1 (de) | 2017-08-15 | 2019-02-20 | Covestro Deutschland AG | Verfahren zur herstellung iminooxadiazindiongruppen enthaltender polyisocyanate unter verwendung von katalysatorenmischungen |
| CN109020973B (zh) * | 2018-09-06 | 2019-10-29 | 天津工业大学 | 一种含氟磺酰亚胺螺环季铵盐电解质、其制备方法及用途 |
| CN113045512B (zh) * | 2021-03-17 | 2023-03-21 | 重庆中科超容科技有限公司 | 一种n,n-二甲基吡咯烷鎓盐的一步制备方法 |
| CN115124454A (zh) * | 2022-07-14 | 2022-09-30 | 山东氟能化工材料有限公司 | 一种复杂结构的螺环季铵盐的合成方法及其产品和应用 |
| KR102774514B1 (ko) * | 2022-08-12 | 2025-03-04 | 삼화페인트공업주식회사 | 고순도 4차 암모늄염의 제조방법 |
| CN115246839B (zh) * | 2022-09-22 | 2023-05-05 | 江苏国泰超威新材料有限公司 | 一种四氟硼酸螺环季铵盐的制备方法 |
| CN116621751A (zh) * | 2023-02-22 | 2023-08-22 | 广东利尔化学有限公司 | 一种酸性镀铜盲孔填充用整平剂的制备方法及电镀铜液 |
| EP4663638A1 (de) | 2024-06-14 | 2025-12-17 | Covestro Deutschland AG | Spirozyklisches ammoniumsalz und verfahren zu seiner herstellung |
Family Cites Families (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4351939A (en) * | 1980-10-16 | 1982-09-28 | Mead Johnson & Company | Spiro-quaternary ammonium halides and N-(2-pyrimidinyl)piperazinylalkylazaspiroalkanedione process |
| US5086178A (en) * | 1990-09-20 | 1992-02-04 | Air Products And Chemicals, Inc. | Fluorinated diazabicycloalkane derivatives |
| US6469888B1 (en) | 1999-11-25 | 2002-10-22 | Bridgestone Corporation | Non-aqueous electrolyte electric double-layer capacitor |
| US6489888B1 (en) * | 2001-06-29 | 2002-12-03 | Johnson Controls Technology Company | Using signal strength to identify tire position |
| CA2428237C (en) * | 2003-05-08 | 2010-07-20 | Delmar Chemicals Inc. | Process for the preparation of carbostyril derivatives |
| US7411777B2 (en) | 2003-08-29 | 2008-08-12 | Japan Carlit Co., Ltd. | Electrolytic solution for electric double layer capacitor and electric double layer capacitor |
| DE602006021437D1 (de) * | 2005-08-30 | 2011-06-01 | Honeywell Int Inc | Verfahren zur synthese von quaternären ammonium-spirosystemen |
-
2006
- 2006-08-28 DE DE602006021437T patent/DE602006021437D1/de active Active
- 2006-08-28 EP EP06790055A patent/EP1919922B1/en not_active Not-in-force
- 2006-08-28 AT AT06790055T patent/ATE506366T1/de not_active IP Right Cessation
- 2006-08-28 WO PCT/US2006/033618 patent/WO2007027649A1/en not_active Ceased
- 2006-08-28 DE DE06790055T patent/DE06790055T1/de active Pending
- 2006-08-28 JP JP2008529178A patent/JP5264488B2/ja not_active Expired - Fee Related
- 2006-08-28 US US11/511,938 patent/US8426593B2/en not_active Expired - Fee Related
- 2006-08-28 CN CN2006800405552A patent/CN101300260B/zh not_active Expired - Fee Related
- 2006-08-28 KR KR1020087007841A patent/KR101388915B1/ko not_active Expired - Fee Related
- 2006-08-30 TW TW095132012A patent/TW200745129A/zh unknown
-
2013
- 2013-03-18 US US13/846,805 patent/US9064633B2/en not_active Expired - Fee Related