JP2007521140A - 高い完全度のスパッタリングターゲット材料及びそれを大量に製造する方法 - Google Patents
高い完全度のスパッタリングターゲット材料及びそれを大量に製造する方法 Download PDFInfo
- Publication number
- JP2007521140A JP2007521140A JP2006547211A JP2006547211A JP2007521140A JP 2007521140 A JP2007521140 A JP 2007521140A JP 2006547211 A JP2006547211 A JP 2006547211A JP 2006547211 A JP2006547211 A JP 2006547211A JP 2007521140 A JP2007521140 A JP 2007521140A
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- JP
- Japan
- Prior art keywords
- metal plate
- rolling
- less
- thickness
- plate according
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 238000005477 sputtering target Methods 0.000 title claims abstract description 25
- 238000004519 manufacturing process Methods 0.000 title abstract description 22
- 239000013077 target material Substances 0.000 title description 5
- 229910052751 metal Inorganic materials 0.000 claims abstract description 82
- 239000002184 metal Substances 0.000 claims abstract description 82
- 238000000034 method Methods 0.000 claims abstract description 74
- 239000004579 marble Substances 0.000 claims abstract description 34
- 238000005096 rolling process Methods 0.000 claims description 140
- GUVRBAGPIYLISA-UHFFFAOYSA-N tantalum atom Chemical compound [Ta] GUVRBAGPIYLISA-UHFFFAOYSA-N 0.000 claims description 65
- 229910052715 tantalum Inorganic materials 0.000 claims description 62
- 230000009467 reduction Effects 0.000 claims description 39
- 238000004544 sputter deposition Methods 0.000 claims description 25
- 239000002245 particle Substances 0.000 claims description 14
- 238000000137 annealing Methods 0.000 claims description 12
- 239000000126 substance Substances 0.000 claims description 12
- 230000008859 change Effects 0.000 claims description 9
- 230000003628 erosive effect Effects 0.000 claims description 8
- 238000005452 bending Methods 0.000 claims description 5
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 claims description 3
- 229910045601 alloy Inorganic materials 0.000 claims description 3
- 239000000956 alloy Substances 0.000 claims description 3
- 229910052802 copper Inorganic materials 0.000 claims description 3
- 239000010949 copper Substances 0.000 claims description 3
- 239000013078 crystal Substances 0.000 claims description 3
- RTAQQCXQSZGOHL-UHFFFAOYSA-N Titanium Chemical compound [Ti] RTAQQCXQSZGOHL-UHFFFAOYSA-N 0.000 claims description 2
- 238000005266 casting Methods 0.000 claims description 2
- 238000005242 forging Methods 0.000 claims description 2
- 229910052758 niobium Inorganic materials 0.000 claims description 2
- 239000010955 niobium Substances 0.000 claims description 2
- GUCVJGMIXFAOAE-UHFFFAOYSA-N niobium atom Chemical compound [Nb] GUCVJGMIXFAOAE-UHFFFAOYSA-N 0.000 claims description 2
- 239000010936 titanium Substances 0.000 claims description 2
- 229910052719 titanium Inorganic materials 0.000 claims description 2
- 238000010894 electron beam technology Methods 0.000 claims 1
- 238000002844 melting Methods 0.000 claims 1
- 230000008018 melting Effects 0.000 claims 1
- 230000017105 transposition Effects 0.000 claims 1
- 230000008569 process Effects 0.000 abstract description 32
- 239000000463 material Substances 0.000 description 23
- 239000000047 product Substances 0.000 description 17
- 238000012545 processing Methods 0.000 description 12
- 238000005097 cold rolling Methods 0.000 description 10
- 238000001953 recrystallisation Methods 0.000 description 8
- 239000007769 metal material Substances 0.000 description 7
- 150000002739 metals Chemical class 0.000 description 7
- 238000005098 hot rolling Methods 0.000 description 6
- 230000004044 response Effects 0.000 description 6
- KRHYYFGTRYWZRS-UHFFFAOYSA-N Fluorane Chemical compound F KRHYYFGTRYWZRS-UHFFFAOYSA-N 0.000 description 4
- 230000015572 biosynthetic process Effects 0.000 description 3
- 230000007423 decrease Effects 0.000 description 3
- 239000000203 mixture Substances 0.000 description 3
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 2
- 239000002253 acid Substances 0.000 description 2
- 238000004458 analytical method Methods 0.000 description 2
- 238000013459 approach Methods 0.000 description 2
- 230000004888 barrier function Effects 0.000 description 2
- 239000003990 capacitor Substances 0.000 description 2
- 238000004140 cleaning Methods 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 238000005530 etching Methods 0.000 description 2
- 238000002474 experimental method Methods 0.000 description 2
- 239000010408 film Substances 0.000 description 2
- 239000012467 final product Substances 0.000 description 2
- 238000005259 measurement Methods 0.000 description 2
- 238000004377 microelectronic Methods 0.000 description 2
- 238000005240 physical vapour deposition Methods 0.000 description 2
- 239000010409 thin film Substances 0.000 description 2
- GRYLNZFGIOXLOG-UHFFFAOYSA-N Nitric acid Chemical compound O[N+]([O-])=O GRYLNZFGIOXLOG-UHFFFAOYSA-N 0.000 description 1
- BQCADISMDOOEFD-UHFFFAOYSA-N Silver Chemical compound [Ag] BQCADISMDOOEFD-UHFFFAOYSA-N 0.000 description 1
- 238000010923 batch production Methods 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 238000003486 chemical etching Methods 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 229910017052 cobalt Inorganic materials 0.000 description 1
- 239000010941 cobalt Substances 0.000 description 1
- GUTLYIVDDKVIGB-UHFFFAOYSA-N cobalt atom Chemical compound [Co] GUTLYIVDDKVIGB-UHFFFAOYSA-N 0.000 description 1
- 239000000356 contaminant Substances 0.000 description 1
- 238000005520 cutting process Methods 0.000 description 1
- 239000008367 deionised water Substances 0.000 description 1
- 229910021641 deionized water Inorganic materials 0.000 description 1
- 230000001627 detrimental effect Effects 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 238000009792 diffusion process Methods 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 230000001747 exhibiting effect Effects 0.000 description 1
- PCHJSUWPFVWCPO-UHFFFAOYSA-N gold Chemical compound [Au] PCHJSUWPFVWCPO-UHFFFAOYSA-N 0.000 description 1
- 239000010931 gold Substances 0.000 description 1
- 229910052737 gold Inorganic materials 0.000 description 1
- 238000000227 grinding Methods 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 238000003754 machining Methods 0.000 description 1
- 239000011159 matrix material Substances 0.000 description 1
- 238000005555 metalworking Methods 0.000 description 1
- 238000001000 micrograph Methods 0.000 description 1
- 238000003801 milling Methods 0.000 description 1
- 238000000465 moulding Methods 0.000 description 1
- 229910017604 nitric acid Inorganic materials 0.000 description 1
- 238000009659 non-destructive testing Methods 0.000 description 1
- 238000000879 optical micrograph Methods 0.000 description 1
- 230000008520 organization Effects 0.000 description 1
- 238000005554 pickling Methods 0.000 description 1
- 230000001681 protective effect Effects 0.000 description 1
- 239000003870 refractory metal Substances 0.000 description 1
- 238000011160 research Methods 0.000 description 1
- 230000004043 responsiveness Effects 0.000 description 1
- 239000004065 semiconductor Substances 0.000 description 1
- 238000000926 separation method Methods 0.000 description 1
- 229910052709 silver Inorganic materials 0.000 description 1
- 239000004332 silver Substances 0.000 description 1
- 238000004513 sizing Methods 0.000 description 1
- 238000003892 spreading Methods 0.000 description 1
- 230000007480 spreading Effects 0.000 description 1
- 238000005482 strain hardening Methods 0.000 description 1
- 239000000758 substrate Substances 0.000 description 1
- HIFJUMGIHIZEPX-UHFFFAOYSA-N sulfuric acid;sulfur trioxide Chemical compound O=S(=O)=O.OS(O)(=O)=O HIFJUMGIHIZEPX-UHFFFAOYSA-N 0.000 description 1
- MZLGASXMSKOWSE-UHFFFAOYSA-N tantalum nitride Chemical compound [Ta]#N MZLGASXMSKOWSE-UHFFFAOYSA-N 0.000 description 1
- 238000011282 treatment Methods 0.000 description 1
- 239000002699 waste material Substances 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
Images
Classifications
-
- C—CHEMISTRY; METALLURGY
- C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
- C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
- C23C14/00—Coating by vacuum evaporation, by sputtering or by ion implantation of the coating forming material
- C23C14/22—Coating by vacuum evaporation, by sputtering or by ion implantation of the coating forming material characterised by the process of coating
- C23C14/34—Sputtering
- C23C14/3407—Cathode assembly for sputtering apparatus, e.g. Target
- C23C14/3414—Metallurgical or chemical aspects of target preparation, e.g. casting, powder metallurgy
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22F—CHANGING THE PHYSICAL STRUCTURE OF NON-FERROUS METALS AND NON-FERROUS ALLOYS
- C22F1/00—Changing the physical structure of non-ferrous metals or alloys by heat treatment or by hot or cold working
- C22F1/16—Changing the physical structure of non-ferrous metals or alloys by heat treatment or by hot or cold working of other metals or alloys based thereon
- C22F1/18—High-melting or refractory metals or alloys based thereon
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22F—CHANGING THE PHYSICAL STRUCTURE OF NON-FERROUS METALS AND NON-FERROUS ALLOYS
- C22F1/00—Changing the physical structure of non-ferrous metals or alloys by heat treatment or by hot or cold working
- C22F1/16—Changing the physical structure of non-ferrous metals or alloys by heat treatment or by hot or cold working of other metals or alloys based thereon
- C22F1/18—High-melting or refractory metals or alloys based thereon
- C22F1/183—High-melting or refractory metals or alloys based thereon of titanium or alloys based thereon
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Mechanical Engineering (AREA)
- Metallurgy (AREA)
- Organic Chemistry (AREA)
- Physics & Mathematics (AREA)
- Thermal Sciences (AREA)
- Crystallography & Structural Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Physical Vapour Deposition (AREA)
- Metal Rolling (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US53181303P | 2003-12-22 | 2003-12-22 | |
| PCT/US2004/042734 WO2005064037A2 (en) | 2003-12-22 | 2004-12-20 | High integrity sputtering target material and method for producing bulk quantities of same |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JP2007521140A true JP2007521140A (ja) | 2007-08-02 |
| JP2007521140A5 JP2007521140A5 (enExample) | 2008-02-14 |
Family
ID=34738707
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2006547211A Pending JP2007521140A (ja) | 2003-12-22 | 2004-12-20 | 高い完全度のスパッタリングターゲット材料及びそれを大量に製造する方法 |
Country Status (6)
| Country | Link |
|---|---|
| US (1) | US20050236076A1 (enExample) |
| EP (1) | EP1704266A2 (enExample) |
| JP (1) | JP2007521140A (enExample) |
| CN (1) | CN1985021A (enExample) |
| TW (1) | TW200523375A (enExample) |
| WO (1) | WO2005064037A2 (enExample) |
Families Citing this family (12)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US20050252268A1 (en) * | 2003-12-22 | 2005-11-17 | Michaluk Christopher A | High integrity sputtering target material and method for producing bulk quantities of same |
| DE112007000440B4 (de) * | 2006-03-07 | 2021-01-07 | Global Advanced Metals, Usa, Inc. | Verfahren zum Erzeugen von verformten Metallartikeln |
| CN102091733B (zh) * | 2009-12-09 | 2013-02-13 | 宁波江丰电子材料有限公司 | 高纯度铜靶材的制作方法 |
| CN102489951B (zh) * | 2011-12-03 | 2013-11-27 | 西北有色金属研究院 | 一种溅射用铌管状靶材的制备方法 |
| CN102873093B (zh) * | 2012-10-31 | 2014-12-03 | 西安诺博尔稀贵金属材料有限公司 | 一种大尺寸钽板材的制备方法 |
| CN104419901B (zh) * | 2013-08-27 | 2017-06-30 | 宁波江丰电子材料股份有限公司 | 一种钽靶材的制造方法 |
| JP6553813B2 (ja) * | 2017-03-30 | 2019-07-31 | Jx金属株式会社 | タンタルスパッタリングターゲット |
| US11062889B2 (en) | 2017-06-26 | 2021-07-13 | Tosoh Smd, Inc. | Method of production of uniform metal plates and sputtering targets made thereby |
| CN107584251B (zh) * | 2017-09-08 | 2019-04-16 | 西北有色金属研究院 | 一种钽合金异形件的成形方法 |
| CN110394603B (zh) * | 2019-07-29 | 2023-05-09 | 福建阿石创新材料股份有限公司 | 一种金属旋转靶材及其制备方法和应用 |
| CN111440938B (zh) * | 2020-04-21 | 2022-01-28 | 合肥工业大学 | 一种轧制纯钽箔的退火强化工艺方法 |
| CN115518981A (zh) * | 2022-10-11 | 2022-12-27 | 西南铝业(集团)有限责任公司 | 一种2xxx系铝锂合金薄宽板的轧制工艺 |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2001504898A (ja) * | 1996-12-04 | 2001-04-10 | アルミニウム ペシネイ | アルミニウム合金製陰極スパッタリング標的 |
| JP2002518593A (ja) * | 1998-06-17 | 2002-06-25 | ジヨンソン マテイ エレクトロニクス,インコーポレーテツド | 微細で一様な構造とテキスチュアを有する金属製品及びその製造方法 |
| JP2002530534A (ja) * | 1998-11-25 | 2002-09-17 | キャボット コーポレイション | 高純度タンタルおよびそれを含む、スパッタターゲットのような製品 |
| JP2004536958A (ja) * | 2000-11-27 | 2004-12-09 | キャボット コーポレイション | 中空カソードターゲットおよびその製造方法 |
Family Cites Families (26)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US1370328A (en) * | 1921-03-01 | Method of making tubes | ||
| DE2037542A1 (de) * | 1970-07-29 | 1972-02-10 | Deutsche Edelstahlwerke AG, 4150Krefeld | Verfahren zur Verminderung der Langs streifigkeit kaltgewalzter Bander aus rost und säurebeständigem Chromstahl |
| US3954514A (en) * | 1975-04-02 | 1976-05-04 | Lockheed Missiles & Space Company, Inc. | Textureless forging of beryllium |
| US4092181A (en) * | 1977-04-25 | 1978-05-30 | Rockwell International Corporation | Method of imparting a fine grain structure to aluminum alloys having precipitating constituents |
| FR2475426A1 (fr) * | 1980-02-12 | 1981-08-14 | Secim | Procede de realisation de fils metalliques |
| FR2529578B1 (fr) * | 1982-07-02 | 1986-04-11 | Cegedur | Procede pour ameliorer a la fois la resistance a la fatigue et la tenacite des alliages d'al a haute resistance |
| JPS61210158A (ja) * | 1985-03-15 | 1986-09-18 | Sumitomo Metal Ind Ltd | 超塑性2相ステンレス鋼およびその熱間加工法 |
| US4721537A (en) * | 1985-10-15 | 1988-01-26 | Rockwell International Corporation | Method of producing a fine grain aluminum alloy using three axes deformation |
| US4722754A (en) * | 1986-09-10 | 1988-02-02 | Rockwell International Corporation | Superplastically formable aluminum alloy and composite material |
| CH682326A5 (enExample) * | 1990-06-11 | 1993-08-31 | Alusuisse Lonza Services Ag | |
| FR2664618B1 (fr) * | 1990-07-10 | 1993-10-08 | Pechiney Aluminium | Procede de fabrication de cathodes pour pulverisation cathodique a base d'aluminium de tres haute purete. |
| US5087297A (en) * | 1991-01-17 | 1992-02-11 | Johnson Matthey Inc. | Aluminum target for magnetron sputtering and method of making same |
| US5370839A (en) * | 1991-07-05 | 1994-12-06 | Nippon Steel Corporation | Tial-based intermetallic compound alloys having superplasticity |
| DE69420124T2 (de) * | 1993-01-15 | 2000-03-02 | Abbott Laboratories, Abbott Park | Strukturierte lipide |
| JP2600065B2 (ja) * | 1994-03-08 | 1997-04-16 | 協和メデックス株式会社 | 高密度リポ蛋白中のコレステロールの定量法 |
| US5850755A (en) * | 1995-02-08 | 1998-12-22 | Segal; Vladimir M. | Method and apparatus for intensive plastic deformation of flat billets |
| US6569270B2 (en) * | 1997-07-11 | 2003-05-27 | Honeywell International Inc. | Process for producing a metal article |
| US6323055B1 (en) * | 1998-05-27 | 2001-11-27 | The Alta Group, Inc. | Tantalum sputtering target and method of manufacture |
| US6193821B1 (en) * | 1998-08-19 | 2001-02-27 | Tosoh Smd, Inc. | Fine grain tantalum sputtering target and fabrication process |
| US6463339B1 (en) * | 1999-09-27 | 2002-10-08 | Rockwell Automation Technologies, Inc. | High reliability industrial controller using tandem independent programmable gate-arrays |
| US20040072009A1 (en) * | 1999-12-16 | 2004-04-15 | Segal Vladimir M. | Copper sputtering targets and methods of forming copper sputtering targets |
| US6331233B1 (en) * | 2000-02-02 | 2001-12-18 | Honeywell International Inc. | Tantalum sputtering target with fine grains and uniform texture and method of manufacture |
| IL156802A0 (en) * | 2001-01-11 | 2004-02-08 | Cabot Corp | Tantalum and niobium billets and methods of producing same |
| DE60231538D1 (de) * | 2001-11-26 | 2009-04-23 | Nikko Materials Co Ltd | Sputtertarget und herstellungsverfahren dafür |
| JP4376487B2 (ja) * | 2002-01-18 | 2009-12-02 | 日鉱金属株式会社 | 高純度ニッケル合金ターゲットの製造方法 |
| US6890393B2 (en) * | 2003-02-07 | 2005-05-10 | Advanced Steel Technology, Llc | Fine-grained martensitic stainless steel and method thereof |
-
2004
- 2004-12-20 WO PCT/US2004/042734 patent/WO2005064037A2/en not_active Ceased
- 2004-12-20 US US11/017,224 patent/US20050236076A1/en not_active Abandoned
- 2004-12-20 EP EP04814868A patent/EP1704266A2/en not_active Withdrawn
- 2004-12-20 CN CNA2004800419912A patent/CN1985021A/zh active Pending
- 2004-12-20 JP JP2006547211A patent/JP2007521140A/ja active Pending
- 2004-12-22 TW TW093140138A patent/TW200523375A/zh unknown
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2001504898A (ja) * | 1996-12-04 | 2001-04-10 | アルミニウム ペシネイ | アルミニウム合金製陰極スパッタリング標的 |
| JP2002518593A (ja) * | 1998-06-17 | 2002-06-25 | ジヨンソン マテイ エレクトロニクス,インコーポレーテツド | 微細で一様な構造とテキスチュアを有する金属製品及びその製造方法 |
| JP2002530534A (ja) * | 1998-11-25 | 2002-09-17 | キャボット コーポレイション | 高純度タンタルおよびそれを含む、スパッタターゲットのような製品 |
| JP2004536958A (ja) * | 2000-11-27 | 2004-12-09 | キャボット コーポレイション | 中空カソードターゲットおよびその製造方法 |
Also Published As
| Publication number | Publication date |
|---|---|
| CN1985021A (zh) | 2007-06-20 |
| US20050236076A1 (en) | 2005-10-27 |
| WO2005064037A2 (en) | 2005-07-14 |
| TW200523375A (en) | 2005-07-16 |
| EP1704266A2 (en) | 2006-09-27 |
| WO2005064037A3 (en) | 2005-12-08 |
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