JP2006509859A5 - - Google Patents
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- Publication number
- JP2006509859A5 JP2006509859A5 JP2004559074A JP2004559074A JP2006509859A5 JP 2006509859 A5 JP2006509859 A5 JP 2006509859A5 JP 2004559074 A JP2004559074 A JP 2004559074A JP 2004559074 A JP2004559074 A JP 2004559074A JP 2006509859 A5 JP2006509859 A5 JP 2006509859A5
- Authority
- JP
- Japan
- Prior art keywords
- weight
- catalyst ink
- organic solvent
- polar aprotic
- aprotic organic
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- ZMXDDKWLCZADIW-UHFFFAOYSA-N N,N-Dimethylformamide Chemical compound CN(C)C=O ZMXDDKWLCZADIW-UHFFFAOYSA-N 0.000 claims 4
- 239000003054 catalyst Substances 0.000 claims 4
- WEVYAHXRMPXWCK-UHFFFAOYSA-N Acetonitrile Chemical compound CC#N WEVYAHXRMPXWCK-UHFFFAOYSA-N 0.000 claims 3
- IAZDPXIOMUYVGZ-UHFFFAOYSA-N dimethyl sulfoxide Natural products CS(C)=O IAZDPXIOMUYVGZ-UHFFFAOYSA-N 0.000 claims 3
- 239000003960 organic solvent Substances 0.000 claims 3
- YEJRWHAVMIAJKC-UHFFFAOYSA-N 4-Butyrolactone Chemical compound O=C1CCCO1 YEJRWHAVMIAJKC-UHFFFAOYSA-N 0.000 claims 2
- FXHOOIRPVKKKFG-UHFFFAOYSA-N N,N-Dimethylacetamide Chemical compound CN(C)C(C)=O FXHOOIRPVKKKFG-UHFFFAOYSA-N 0.000 claims 2
- 239000005518 polymer electrolyte Substances 0.000 claims 2
- CYSGHNMQYZDMIA-UHFFFAOYSA-N 1,3-Dimethyl-2-imidazolidinon Chemical compound CN1CCN(C)C1=O CYSGHNMQYZDMIA-UHFFFAOYSA-N 0.000 claims 1
- OIFBSDVPJOWBCH-UHFFFAOYSA-N Diethyl carbonate Chemical compound CCOC(=O)OCC OIFBSDVPJOWBCH-UHFFFAOYSA-N 0.000 claims 1
- KMTRUDSVKNLOMY-UHFFFAOYSA-N Ethylene carbonate Chemical compound O=C1OCCO1 KMTRUDSVKNLOMY-UHFFFAOYSA-N 0.000 claims 1
- NTIZESTWPVYFNL-UHFFFAOYSA-N Methyl isobutyl ketone Chemical compound CC(C)CC(C)=O NTIZESTWPVYFNL-UHFFFAOYSA-N 0.000 claims 1
- UIHCLUNTQKBZGK-UHFFFAOYSA-N Methyl isobutyl ketone Natural products CCC(C)C(C)=O UIHCLUNTQKBZGK-UHFFFAOYSA-N 0.000 claims 1
- 239000002253 acid Substances 0.000 claims 1
- 125000000732 arylene group Chemical group 0.000 claims 1
- 238000009835 boiling Methods 0.000 claims 1
- 229930188620 butyrolactone Natural products 0.000 claims 1
- IEJIGPNLZYLLBP-UHFFFAOYSA-N dimethyl carbonate Chemical compound COC(=O)OC IEJIGPNLZYLLBP-UHFFFAOYSA-N 0.000 claims 1
- GNOIPBMMFNIUFM-UHFFFAOYSA-N hexamethylphosphoric triamide Chemical compound CN(C)P(=O)(N(C)C)N(C)C GNOIPBMMFNIUFM-UHFFFAOYSA-N 0.000 claims 1
- 229920000642 polymer Polymers 0.000 claims 1
- RUOJZAUFBMNUDX-UHFFFAOYSA-N propylene carbonate Chemical compound CC1COC(=O)O1 RUOJZAUFBMNUDX-UHFFFAOYSA-N 0.000 claims 1
- HNJBEVLQSNELDL-UHFFFAOYSA-N pyrrolidin-2-one Chemical compound O=C1CCCN1 HNJBEVLQSNELDL-UHFFFAOYSA-N 0.000 claims 1
- 239000011949 solid catalyst Substances 0.000 claims 1
- HXJUTPCZVOIRIF-UHFFFAOYSA-N sulfolane Chemical compound O=S1(=O)CCCC1 HXJUTPCZVOIRIF-UHFFFAOYSA-N 0.000 claims 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims 1
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US10/315,589 US20040107869A1 (en) | 2002-12-10 | 2002-12-10 | Catalyst ink |
| US10/315,589 | 2002-12-10 | ||
| PCT/US2003/033133 WO2004054021A2 (en) | 2002-12-10 | 2003-10-17 | Catalyst ink |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| JP2006509859A JP2006509859A (ja) | 2006-03-23 |
| JP2006509859A5 true JP2006509859A5 (enExample) | 2006-09-28 |
| JP4690047B2 JP4690047B2 (ja) | 2011-06-01 |
Family
ID=32468741
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2004559074A Expired - Fee Related JP4690047B2 (ja) | 2002-12-10 | 2003-10-17 | 触媒インク |
Country Status (10)
| Country | Link |
|---|---|
| US (2) | US20040107869A1 (enExample) |
| EP (1) | EP1588449B1 (enExample) |
| JP (1) | JP4690047B2 (enExample) |
| KR (1) | KR20050084199A (enExample) |
| CN (1) | CN100380723C (enExample) |
| AT (1) | ATE370521T1 (enExample) |
| AU (1) | AU2003286497A1 (enExample) |
| CA (1) | CA2506657A1 (enExample) |
| DE (1) | DE60315721T2 (enExample) |
| WO (1) | WO2004054021A2 (enExample) |
Families Citing this family (48)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2004220979A (ja) * | 2003-01-16 | 2004-08-05 | Toyota Motor Corp | 触媒物質含有インクとそれを用いた電極および燃料電池 |
| JP2004311057A (ja) * | 2003-04-02 | 2004-11-04 | Dainippon Printing Co Ltd | 触媒層形成用ペースト組成物及び触媒層−電解質膜積層体製造用転写シート |
| WO2005081352A1 (en) * | 2004-02-18 | 2005-09-01 | Polyfuel, Inc. | Catalyst ink, process for making catalyst ink and for preparing catalyst coated membranes |
| US20050266980A1 (en) * | 2004-05-28 | 2005-12-01 | Mada Kannan Arunachala N | Process of producing a novel MEA with enhanced electrode/electrolyte adhesion and performancese characteristics |
| DE102004033679A1 (de) * | 2004-07-09 | 2006-02-16 | Tesa Ag | Verfahren zur Herstellung einer Membran-Elektroden-Einheit |
| US7304101B2 (en) * | 2004-07-19 | 2007-12-04 | 3M Innovative Properties Company | Method of purifying a dispersion of ionic fluoropolymer |
| US20060014887A1 (en) * | 2004-07-19 | 2006-01-19 | 3M Innovative Properties Company | Method of hydrolyzing a dispersion of ionic fluoropolymer |
| JP4552183B2 (ja) * | 2004-08-17 | 2010-09-29 | 株式会社豊田中央研究所 | ゾル状プロトン伝導性電解質及び燃料電池 |
| US7691932B2 (en) | 2004-09-27 | 2010-04-06 | 3M Innovative Properties Company | Method of making a composition and nanocomposites therefrom |
| US7862956B2 (en) * | 2004-12-29 | 2011-01-04 | 3M Innovative Properties Company | Z-axis electrically conducting flow field separator |
| US7311990B2 (en) * | 2004-12-29 | 2007-12-25 | 3M Innovative Properties Company | Form-in-place fastening for fuel cell assemblies |
| EP2273591B1 (en) | 2005-03-30 | 2017-05-31 | Umicore Ag & Co. Kg | Ink for producing catalyst layers |
| US7838138B2 (en) * | 2005-09-19 | 2010-11-23 | 3M Innovative Properties Company | Fuel cell electrolyte membrane with basic polymer |
| US7517604B2 (en) | 2005-09-19 | 2009-04-14 | 3M Innovative Properties Company | Fuel cell electrolyte membrane with acidic polymer |
| US8652705B2 (en) | 2005-09-26 | 2014-02-18 | W.L. Gore & Associates, Inc. | Solid polymer electrolyte and process for making same |
| US20070105007A1 (en) * | 2005-11-10 | 2007-05-10 | The Board Of Trustees Of The University Of Illinois | Dry impregnation of platinum on a carbon substrate |
| DE102005054149A1 (de) * | 2005-11-14 | 2007-05-16 | Basf Ag | Aminhaltige Katalysatortinte für Brennstoffzellen |
| JP2007141528A (ja) * | 2005-11-15 | 2007-06-07 | Hitachi Maxell Ltd | 燃料電池の電極用ペーストと燃料電池 |
| CN101098007A (zh) * | 2006-06-27 | 2008-01-02 | 上海攀业氢能源科技有限公司 | 用于制作燃料电池膜电极的催化剂浆料及其制备方法 |
| EP1873860A1 (en) * | 2006-06-28 | 2008-01-02 | Solvay Solexis S.p.A. | Catalyst-Polymer Liquid Dispersion for Fuel Cell Applications |
| US7696122B2 (en) * | 2006-07-05 | 2010-04-13 | Cabot Corporation | Electrocatalyst inks for fuel cell applications |
| JP5141104B2 (ja) * | 2006-11-06 | 2013-02-13 | トヨタ自動車株式会社 | 燃料電池の製造方法 |
| DE102007030566A1 (de) * | 2007-03-28 | 2008-10-02 | Man Roland Druckmaschinen Ag | Zerstörungsfreie Prüfverfahren der Aushärtungs- oder Trocknungsgrades von Farben und Lacken |
| KR100874112B1 (ko) * | 2007-06-25 | 2008-12-15 | 한화석유화학 주식회사 | 연료전지용 촉매 잉크 및 이를 이용한 막-전극 복합체의제조방법 |
| JP5242955B2 (ja) * | 2007-07-04 | 2013-07-24 | 株式会社キャタラー | スラリーの粘度調整方法およびスラリーの製造方法 |
| JP5497049B2 (ja) | 2008-10-24 | 2014-05-21 | ナノシス・インク． | 燃料電池用電気化学的触媒 |
| US20110275005A1 (en) * | 2008-10-24 | 2011-11-10 | Nanosys, Inc | Membrane Electrode Assemblies With Interfacial Layer |
| JP5293149B2 (ja) * | 2008-12-18 | 2013-09-18 | 株式会社エクォス・リサーチ | 燃料電池の電極用ペースト、膜電極接合体及び電極用ペーストの製造方法 |
| JP5245838B2 (ja) * | 2009-01-09 | 2013-07-24 | 株式会社エクォス・リサーチ | 燃料電池の電極用ペースト、膜電極接合体及び電極用ペーストの製造方法 |
| US8735023B2 (en) * | 2009-12-14 | 2014-05-27 | GM Global Technology Operations LLC | Fuel cell with layered electrode |
| JP5494585B2 (ja) * | 2011-07-27 | 2014-05-14 | トヨタ自動車株式会社 | 燃料電池電極用触媒インク、膜電極接合体、燃料電池 |
| US11155661B2 (en) | 2015-09-23 | 2021-10-26 | 3M Innovative Properties Company | Method of making a copolymer of tetrafluoroethylene having sulfonyl pendant groups |
| JP6568326B2 (ja) | 2016-04-04 | 2019-08-28 | ダイオキサイド マテリアルズ，インコーポレイティド | 触媒層及び電解槽 |
| WO2019055791A1 (en) | 2017-09-14 | 2019-03-21 | 3M Innovative Properties Company | FLUORINATED COPOLYMER HAVING SULFONYL PENDANT GROUPS AND COMPOSITIONS AND ARTICLES COMPRISING SAID FLUORINATED COPOLYMER |
| US10490829B2 (en) * | 2018-02-20 | 2019-11-26 | GM Global Technology Operations LLC | Method for manufacturing a fuel cell |
| FR3085800B1 (fr) * | 2018-09-12 | 2021-06-04 | Commissariat Energie Atomique | Procede de fabrication d’un guide d’ecoulement de reacteur electrochimique |
| WO2020183306A1 (en) | 2019-03-12 | 2020-09-17 | 3M Innovative Properties Company | Dispersible perfluorosulfonic acid ionomer compositions |
| CN113906038A (zh) | 2019-06-04 | 2022-01-07 | 3M创新有限公司 | 多官能氟化化合物、由该化合物制成的氟化聚合物以及相关方法 |
| CN114761445B (zh) | 2019-12-02 | 2024-08-30 | 3M创新有限公司 | 全氟磺酸离聚物的可分散颗粒 |
| KR20220119048A (ko) | 2019-12-20 | 2022-08-26 | 쓰리엠 이노베이티브 프로퍼티즈 컴파니 | 플루오르화 공중합체 및 이를 포함하는 조성물 및 물품 |
| US12286387B2 (en) | 2019-12-23 | 2025-04-29 | 3M Innovative Properties Company | Process of making fluoroolefins by thermal decomposition of fluorinated ionomers |
| CN115667332B (zh) | 2020-03-30 | 2024-08-16 | 3M创新有限公司 | 包含具有离子双(磺酰基)酰亚胺部分和全氟醚末端基团的侧基的含氟聚合物 |
| US20230090482A1 (en) | 2020-04-09 | 2023-03-23 | 3M Innovative Properties Company | Composite including fluorinated polymer and salt nanoparticles and articles including the same |
| US20230279192A1 (en) | 2020-06-08 | 2023-09-07 | 3M Innovative Properties Company | Process for recycling a solid article including a fluorinated polymer |
| US12341227B2 (en) | 2021-06-04 | 2025-06-24 | 3M Innovative Properties Company | Perfluorosulfonyl monomers suitable for fluoropolymers and fuel cell membrane articles |
| US20250239638A1 (en) | 2021-10-07 | 2025-07-24 | 3M Innovative Properties Company | Composite including fluorinated polymer and lithium fluoride nanoparticles and articles including the same |
| CN114540854A (zh) * | 2022-03-18 | 2022-05-27 | 中国科学院长春应用化学研究所 | 一种spewe膜电极及其制备方法 |
| JP7616138B2 (ja) * | 2022-03-31 | 2025-01-17 | トヨタ自動車株式会社 | 洗浄装置 |
Family Cites Families (30)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5211984A (en) * | 1991-02-19 | 1993-05-18 | The Regents Of The University Of California | Membrane catalyst layer for fuel cells |
| JP3422377B2 (ja) * | 1993-08-06 | 2003-06-30 | 松下電器産業株式会社 | 固体高分子型燃料電池の製造方法及びこれにより得られる固体高分子型燃料電池 |
| KR100389150B1 (ko) * | 1994-10-20 | 2003-10-10 | 훽스트 악티엔게젤샤프트 | 금속피복된양이온교환멤브레인/전극복합체및이의제조방법 |
| EP0795137B1 (en) * | 1994-11-29 | 1998-08-26 | Minnesota Mining And Manufacturing Company | Transparent decorative article having an etched appearing/prismatic image thereon |
| JP3712768B2 (ja) * | 1995-01-26 | 2005-11-02 | 松下電器産業株式会社 | 固体高分子型燃料電池の製造法 |
| GB9504713D0 (en) * | 1995-03-09 | 1995-04-26 | Johnson Matthey Plc | Improved electrocatalytic material |
| US5702755A (en) * | 1995-11-06 | 1997-12-30 | The Dow Chemical Company | Process for preparing a membrane/electrode assembly |
| JPH09223503A (ja) * | 1996-02-14 | 1997-08-26 | Tanaka Kikinzoku Kogyo Kk | 高分子固体電解質型燃料電池用電極の製造方法 |
| DE19611510A1 (de) * | 1996-03-23 | 1997-09-25 | Degussa | Gasdiffusionselektrode für Membranbrennstoffzellen und Verfahren zu ihrer Herstellung |
| TW404079B (en) | 1996-08-27 | 2000-09-01 | Univ New York State Res Found | Gas diffusion electrodes based on polyethersulfone carbon blends |
| JPH10302805A (ja) * | 1997-04-22 | 1998-11-13 | Matsushita Electric Ind Co Ltd | 固体高分子電解質膜と電極との接合体およびその製造法とそれを用いた燃料電池 |
| DE19745904A1 (de) * | 1997-10-17 | 1999-04-22 | Hoechst Ag | Polymerstabilisierte Metallkolloid-Lösungen, Verfahren zu ihrer Herstellung und ihre Verwendung als Katalysatoren für Brennstoffzellen |
| EP0955687B1 (en) | 1998-05-04 | 2006-03-15 | Samsung SDI Co., Ltd. | Method for producing a slurry for forming a catalyst layer for a proton exchange membrane fuel cell |
| TR200101135T2 (tr) * | 1998-10-26 | 2001-09-21 | Akzo Nobel N.V. | Bir poliüretan dispersiyonları karışımını içeren sulu kaplama bileşimi |
| AU759819B2 (en) * | 1999-01-22 | 2003-05-01 | University Of Southern California | Improved membrane electrode assembly for a fuel cell |
| JP2000353528A (ja) * | 1999-04-09 | 2000-12-19 | Toray Ind Inc | 電極触媒層およびその製造方法並びに電極触媒層を用いた燃料電池 |
| JP4815651B2 (ja) * | 1999-12-01 | 2011-11-16 | 株式会社Ｇｓユアサ | 固体高分子型電解質型燃料電池用ガス拡散電極 |
| JP2001160400A (ja) * | 1999-12-01 | 2001-06-12 | Asahi Glass Co Ltd | 固体高分子電解質型燃料電池用のガス拡散電極の製造方法 |
| DE10112585A1 (de) * | 2000-03-15 | 2001-10-31 | Japan Storage Battery Co Ltd | Composit-Katalysator für eine Brennstoffzelle vom festen Polymer-Elektrolyt-Typ und Verfahren zu seiner Herstellung |
| JP3614077B2 (ja) * | 2000-03-22 | 2005-01-26 | トヨタ自動車株式会社 | 燃料電池用の電極触媒溶液およびその製造方法 |
| WO2001071835A2 (en) | 2000-03-22 | 2001-09-27 | Victrex Manufacturing Limited | Membrane/electrode composite |
| JP2001273907A (ja) * | 2000-03-28 | 2001-10-05 | Japan Storage Battery Co Ltd | ガス拡散電極およびその製造方法。 |
| US20020045081A1 (en) * | 2000-07-05 | 2002-04-18 | Masaaki Nanaumi | Electrolyte membrane/electrode assembly of solid polymer electrolyte fuel cell |
| DE10037074A1 (de) * | 2000-07-29 | 2002-02-14 | Omg Ag & Co Kg | Tinte zur Herstellung von Membran-Elektroden-Einheiten für PEM-Brennstoffzellen |
| JP3579885B2 (ja) * | 2000-09-01 | 2004-10-20 | 本田技研工業株式会社 | 燃料電池用電極構造体およびその製造方法 |
| US6696382B1 (en) * | 2000-11-14 | 2004-02-24 | The Regents Of The University Of California | Catalyst inks and method of application for direct methanol fuel cells |
| AU2002242146A1 (en) * | 2001-01-29 | 2002-08-12 | 3M Innovative Properties Company | Decal method of making membrane electrode assemblies for fuel cells |
| US20040265676A1 (en) * | 2001-10-25 | 2004-12-30 | Jun Takagi | Polymer electrolyte solution for manufacturing electrode for fuel cell |
| JP2003317728A (ja) * | 2002-04-26 | 2003-11-07 | Ube Ind Ltd | 多孔質炭素フィルムを用いた燃料電池用電極、膜−電極接合体及び燃料電池 |
| DE60230979D1 (de) * | 2002-07-31 | 2009-03-12 | Umicore Ag & Co Kg | Wässrige Katalysatortinten und ihre Verwendung für die Herstellung von mit Katalysator beschichteten Substraten |
-
2002
- 2002-12-10 US US10/315,589 patent/US20040107869A1/en not_active Abandoned
-
2003
- 2003-10-17 DE DE60315721T patent/DE60315721T2/de not_active Expired - Lifetime
- 2003-10-17 EP EP03777697A patent/EP1588449B1/en not_active Expired - Lifetime
- 2003-10-17 KR KR1020057010345A patent/KR20050084199A/ko not_active Withdrawn
- 2003-10-17 CA CA002506657A patent/CA2506657A1/en not_active Abandoned
- 2003-10-17 JP JP2004559074A patent/JP4690047B2/ja not_active Expired - Fee Related
- 2003-10-17 AT AT03777697T patent/ATE370521T1/de not_active IP Right Cessation
- 2003-10-17 WO PCT/US2003/033133 patent/WO2004054021A2/en not_active Ceased
- 2003-10-17 CN CNB200380105215XA patent/CN100380723C/zh not_active Expired - Fee Related
- 2003-10-17 AU AU2003286497A patent/AU2003286497A1/en not_active Abandoned
-
2010
- 2010-07-21 US US12/840,859 patent/US7855160B2/en not_active Expired - Fee Related
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