JP2003246810A5 - - Google Patents
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- Publication number
- JP2003246810A5 JP2003246810A5 JP2002366969A JP2002366969A JP2003246810A5 JP 2003246810 A5 JP2003246810 A5 JP 2003246810A5 JP 2002366969 A JP2002366969 A JP 2002366969A JP 2002366969 A JP2002366969 A JP 2002366969A JP 2003246810 A5 JP2003246810 A5 JP 2003246810A5
- Authority
- JP
- Japan
- Prior art keywords
- acrylic acid
- mass
- monomer component
- producing
- water
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- NIXOWILDQLNWCW-UHFFFAOYSA-N 2-Propenoic acid Natural products OC(=O)C=C NIXOWILDQLNWCW-UHFFFAOYSA-N 0.000 description 55
- SMZOUWXMTYCWNB-UHFFFAOYSA-N 2-(2-methoxy-5-methylphenyl)ethanamine Chemical compound COC1=CC=C(C)C=C1CCN SMZOUWXMTYCWNB-UHFFFAOYSA-N 0.000 description 54
- 239000000178 monomer Substances 0.000 description 26
- 239000011347 resin Substances 0.000 description 22
- 229920005989 resin Polymers 0.000 description 22
- ATUOYWHBWRKTHZ-UHFFFAOYSA-N Propane Chemical compound CCC ATUOYWHBWRKTHZ-UHFFFAOYSA-N 0.000 description 20
- 238000004519 manufacturing process Methods 0.000 description 18
- 239000000203 mixture Substances 0.000 description 18
- 239000002250 absorbent Substances 0.000 description 16
- LHGVFZTZFXWLCP-UHFFFAOYSA-N guaiacol Chemical compound COC1=CC=CC=C1O LHGVFZTZFXWLCP-UHFFFAOYSA-N 0.000 description 16
- 150000003839 salts Chemical class 0.000 description 12
- 230000003197 catalytic effect Effects 0.000 description 10
- 238000000034 method Methods 0.000 description 10
- 230000003647 oxidation Effects 0.000 description 10
- 238000007254 oxidation reaction Methods 0.000 description 10
- 239000001294 propane Substances 0.000 description 10
- 238000006116 polymerization reaction Methods 0.000 description 9
- 238000006386 neutralization reaction Methods 0.000 description 8
- QQONPFPTGQHPMA-UHFFFAOYSA-N propylene Natural products CC=C QQONPFPTGQHPMA-UHFFFAOYSA-N 0.000 description 8
- 125000004805 propylene group Chemical group [H]C([H])([H])C([H])([*:1])C([H])([H])[*:2] 0.000 description 8
- 230000000379 polymerizing effect Effects 0.000 description 7
- HYBBIBNJHNGZAN-UHFFFAOYSA-N furfural Chemical compound O=CC1=CC=CO1 HYBBIBNJHNGZAN-UHFFFAOYSA-N 0.000 description 6
- 238000010526 radical polymerization reaction Methods 0.000 description 5
- 238000010521 absorption reaction Methods 0.000 description 4
- 239000007789 gas Substances 0.000 description 4
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 description 3
- 238000002425 crystallisation Methods 0.000 description 3
- 230000008025 crystallization Effects 0.000 description 3
- 238000004821 distillation Methods 0.000 description 3
- 239000002245 particle Substances 0.000 description 3
- 239000002504 physiological saline solution Substances 0.000 description 3
- JLUQTCXCAFSSLD-NXEZZACHSA-N Anemonin Chemical compound C1=CC(=O)O[C@]11[C@@]2(C=CC(=O)O2)CC1 JLUQTCXCAFSSLD-NXEZZACHSA-N 0.000 description 2
- JLUQTCXCAFSSLD-UHFFFAOYSA-N Anemonin Natural products C1=CC(=O)OC11C2(C=CC(=O)O2)CC1 JLUQTCXCAFSSLD-UHFFFAOYSA-N 0.000 description 2
- MHAJPDPJQMAIIY-UHFFFAOYSA-N Hydrogen peroxide Chemical compound OO MHAJPDPJQMAIIY-UHFFFAOYSA-N 0.000 description 2
- 239000002253 acid Substances 0.000 description 2
- 239000000463 material Substances 0.000 description 2
- KJSVAZNPHAQRIM-UHFFFAOYSA-N phenol;prop-1-ene Chemical compound CC=C.OC1=CC=CC=C1 KJSVAZNPHAQRIM-UHFFFAOYSA-N 0.000 description 2
- RNYZJZKPGHQTJR-UHFFFAOYSA-N protoanemonin Chemical compound C=C1OC(=O)C=C1 RNYZJZKPGHQTJR-UHFFFAOYSA-N 0.000 description 2
- 230000002745 absorbent Effects 0.000 description 1
- 239000003463 adsorbent Substances 0.000 description 1
- 238000004132 cross linking Methods 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 229920000642 polymer Polymers 0.000 description 1
- 239000003505 polymerization initiator Substances 0.000 description 1
- 239000000843 powder Substances 0.000 description 1
- 229910001428 transition metal ion Inorganic materials 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP2002366969A JP4150253B2 (ja) | 2001-12-19 | 2002-12-18 | アクリル酸系吸水性樹脂の製造方法、この方法に用いるアクリル酸組成物とその製造方法 |
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP2001-385746 | 2001-12-19 | ||
| JP2001385746 | 2001-12-19 | ||
| JP2002366969A JP4150253B2 (ja) | 2001-12-19 | 2002-12-18 | アクリル酸系吸水性樹脂の製造方法、この方法に用いるアクリル酸組成物とその製造方法 |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| JP2003246810A JP2003246810A (ja) | 2003-09-05 |
| JP2003246810A5 true JP2003246810A5 (https=) | 2006-02-02 |
| JP4150253B2 JP4150253B2 (ja) | 2008-09-17 |
Family
ID=19187869
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2002366969A Expired - Fee Related JP4150253B2 (ja) | 2001-12-19 | 2002-12-18 | アクリル酸系吸水性樹脂の製造方法、この方法に用いるアクリル酸組成物とその製造方法 |
Country Status (9)
| Country | Link |
|---|---|
| US (1) | US7049366B2 (https=) |
| EP (1) | EP1456259B1 (https=) |
| JP (1) | JP4150253B2 (https=) |
| KR (1) | KR100549717B1 (https=) |
| CN (2) | CN1831019B (https=) |
| BR (1) | BR0206696B1 (https=) |
| DE (1) | DE60233590D1 (https=) |
| SA (1) | SA03230508B1 (https=) |
| WO (1) | WO2003051940A1 (https=) |
Families Citing this family (69)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US6927268B2 (en) * | 2000-06-21 | 2005-08-09 | Nippon Shokubai Co., Ltd. | Production process for water-absorbent resin |
| US6794473B2 (en) | 2001-05-01 | 2004-09-21 | Nippon Shokubai Co., Ltd. | Acrylic acid (salt) polymer, its production process and uses |
| JP3939988B2 (ja) * | 2002-01-16 | 2007-07-04 | 住友精化株式会社 | 吸水性樹脂の製造方法 |
| KR20070003874A (ko) * | 2004-01-28 | 2007-01-05 | 바스프 악티엔게젤샤프트 | 중합체 제조방법 |
| JP2005225921A (ja) * | 2004-02-10 | 2005-08-25 | Asahi Kasei Chemicals Corp | 吸水性樹脂及び吸水性樹脂組成物及び吸水体 |
| JP2006055833A (ja) * | 2004-03-29 | 2006-03-02 | Nippon Shokubai Co Ltd | 吸水性樹脂を主成分とする粒子状吸水剤 |
| EP1790668A4 (en) * | 2004-07-15 | 2008-11-19 | Sumitomo Seika Chemicals | PROCESS FOR PRODUCING WATER ABSORBING RESIN |
| AU2005285763A1 (en) * | 2004-09-24 | 2006-03-30 | Nippon Shokubai Co., Ltd. | Particulate water-absorbing agent containing water-absorbent resin as a main component |
| EP1799721B1 (de) * | 2004-09-28 | 2011-11-23 | Basf Se | Verfahren zur kontinuierlichen herstellung von vernetzten feinteiligen gelförmigen polymerisaten |
| DE102004055765A1 (de) | 2004-11-18 | 2006-05-24 | Basf Ag | Verfahren zur Herstellung wasserabsorbierender Polymere |
| DE102004057874A1 (de) * | 2004-11-30 | 2006-06-01 | Basf Ag | Verfahren zur Nachvernetzung wasserabsorbierender Polymerpartikel |
| TWI353360B (en) * | 2005-04-07 | 2011-12-01 | Nippon Catalytic Chem Ind | Production process of polyacrylic acid (salt) wate |
| CN101155840B (zh) * | 2005-04-07 | 2011-06-15 | 株式会社日本触媒 | 聚丙烯酸（盐）吸水树脂的生产方法 |
| JP5091477B2 (ja) * | 2005-04-12 | 2012-12-05 | 株式会社日本触媒 | ポリアクリル酸（塩）系吸水性樹脂を主成分とする粒子状吸水剤、その製造方法、この粒子状吸水剤を用いた吸収体及び吸収性物品 |
| KR100905853B1 (ko) * | 2005-08-17 | 2009-07-02 | 가부시키가이샤 닛폰 쇼쿠바이 | 흡수성 수지의 제조방법, 흡수성 수지, 및 그 용도 |
| TWI383008B (zh) * | 2005-08-17 | 2013-01-21 | Nippon Catalytic Chem Ind | 吸水性樹脂之製造方法及吸水性樹脂以及其利用 |
| JP5044555B2 (ja) * | 2005-08-24 | 2012-10-10 | ビーエーエスエフ ソシエタス・ヨーロピア | 吸水性ポリマー粒子の製造方法 |
| DE102005042608A1 (de) † | 2005-09-07 | 2007-03-08 | Basf Ag | Polymerisationsverfahren |
| DE102005042607A1 (de) | 2005-09-07 | 2007-03-08 | Basf Ag | Polymerisationsverfahren |
| TW200712114A (en) | 2005-09-30 | 2007-04-01 | Nippon Catalytic Chem Ind | Method for manufacturing particulate water-absorbing agent and particulate water-absorbing agent |
| DE102005055077A1 (de) * | 2005-11-16 | 2007-05-24 | Basf Ag | Verfahren zur Herstellung wasserabsorbierender Polymerpartikel |
| TWI394789B (zh) | 2005-12-22 | 2013-05-01 | Nippon Catalytic Chem Ind | 吸水性樹脂組成物及其製造方法、吸收性物品 |
| EP1837348B9 (en) | 2006-03-24 | 2020-01-08 | Nippon Shokubai Co.,Ltd. | Water-absorbing resin and method for manufacturing the same |
| JP5042674B2 (ja) * | 2006-03-29 | 2012-10-03 | 株式会社日本触媒 | ポリアクリル酸（塩）系吸水性樹脂の製造方法 |
| DE602007003397D1 (de) | 2006-03-29 | 2010-01-07 | Nippon Catalytic Chem Ind | Verfahren zur Herstellung von wasserabsorbierendem Polyacrylsäure (Salz)-Harz |
| US8907017B2 (en) * | 2006-04-21 | 2014-12-09 | Evonik Degussa Gmbh | Water-absorbing polymer structure having improved permeability and absorption under pressure |
| JP5306197B2 (ja) | 2006-07-19 | 2013-10-02 | ビーエーエスエフ ソシエタス・ヨーロピア | モノマー溶液の液滴の重合による、吸水性ポリマー粒子の製造方法 |
| CN101490139B (zh) * | 2006-07-31 | 2012-02-15 | 株式会社日本触媒 | 吸水树脂粉末的制备方法和吸水树脂粉末的包装 |
| US8822373B2 (en) * | 2006-08-31 | 2014-09-02 | Nippon Shokubai Co., Ltd | Particulate water absorbing agent and production method thereof |
| WO2008034786A1 (de) | 2006-09-19 | 2008-03-27 | Basf Se | Verfahren zur herstellung farbstabiler wasserabsorbierender polymerpartikel mit niedrigen neutralisationsgrad |
| CN101594889A (zh) * | 2007-01-29 | 2009-12-02 | 巴斯夫欧洲公司 | 生产具有高吸收率和高盐水导流率的白色且颜色稳定的吸水性聚合物颗粒的方法 |
| EP2115019B2 (de) † | 2007-01-29 | 2019-07-10 | Basf Se | VERFAHREN ZUR HERSTELLUNG WEIßER UND FARBSTABILER WASSERABSORBIERENDER POLYMERPARTIKEL MIT HOHEM ABSORPTIONSVERMÖGEN UND HOHER FLÜSSIGKEITSLEITFÄHIGKEIT |
| CN101600762B (zh) | 2007-02-05 | 2012-10-24 | 株式会社日本触媒 | 粒子状吸水剂及其制造方法 |
| BRPI0809157A2 (pt) * | 2007-03-23 | 2014-09-16 | Basf Se | Processos para transportar uma composição manomérica, e para preparar resinas que absorvem água. |
| US8835575B2 (en) | 2008-01-29 | 2014-09-16 | Basf Se | Method for the production of water-absorbing polymer particles |
| US8148485B2 (en) | 2008-03-13 | 2012-04-03 | Nippon Shokubai Co., Ltd. | Production method for water-absorbing resin |
| US8410223B2 (en) | 2008-03-28 | 2013-04-02 | Nippon Shokubai Co., Ltd. | Production method for water-absorbing resin |
| JP5410412B2 (ja) | 2008-03-31 | 2014-02-05 | 株式会社日本触媒 | 吸水性樹脂を主成分とする粒子状吸水剤の製造方法及びその製造装置 |
| CN101550202B (zh) * | 2008-03-31 | 2011-09-21 | 上海恒谊化工有限公司 | 一种新型反相乳液聚合物的制备方法 |
| US8546492B2 (en) | 2008-04-11 | 2013-10-01 | Nippon Shokubai, Co., Ltd. | Surface treatment method for water-absorbing resin and production method for water-absorbing resin |
| WO2009130915A1 (ja) | 2008-04-25 | 2009-10-29 | 株式会社日本触媒 | ポリアクリル酸（塩）系吸水性樹脂およびその製造方法 |
| EP2275400B1 (en) * | 2008-04-27 | 2017-01-11 | Nippon Shokubai Co., Ltd. | Process for producing acrylic acid, and process for producing hydrophilic resin and process for producing water absorptive resin using the process |
| JP5718060B2 (ja) | 2009-02-06 | 2015-05-13 | 株式会社日本触媒 | ポリアクリル酸（塩）系親水性樹脂およびその製造方法 |
| US20100285224A1 (en) * | 2009-05-11 | 2010-11-11 | Dale Fisher | Agent and method for curing pervious concrete |
| DE102009026822A1 (de) | 2009-06-08 | 2010-12-09 | Basf Se | Verfahren zur Umstabilisierung von (Meth)acrylmonomeren |
| WO2011032876A1 (de) * | 2009-09-16 | 2011-03-24 | Basf Se | Farbstabiler superabsorber |
| JP5801203B2 (ja) | 2009-09-29 | 2015-10-28 | 株式会社日本触媒 | 粒子状吸水剤及びその製造方法 |
| JP5731390B2 (ja) | 2009-09-30 | 2015-06-10 | 株式会社日本触媒 | ポリアクリル酸（塩）系吸水性樹脂およびその製造方法 |
| WO2011040530A1 (ja) * | 2009-09-30 | 2011-04-07 | 株式会社日本触媒 | 粒子状吸水剤及びその製造方法 |
| FR2957594B1 (fr) * | 2010-03-18 | 2013-04-26 | Arkema France | Procede de fabrication d'acide acrylique bio-ressource de grade polymere a partir de glycerol |
| BR112012027406B1 (pt) * | 2010-04-26 | 2021-02-09 | Nippon Shokubai Co., Ltd. | resina absorvedora de água tipo ácido poliacrílico (sal), material sanitário e método para produzir a referida resina |
| BR112012027407B1 (pt) * | 2010-04-26 | 2020-04-07 | Nippon Shokubai Co., Ltd. | resina absorvedora de água tipo ácido poliacrílico (sal), material sanitário contendo a mesma, método para produzir e identificar a mesma e método para produzir ácido poliacrílico (sal) |
| US8791230B2 (en) | 2010-06-08 | 2014-07-29 | Nippon Shokubai Co., Ltd. | Method for producing particulate water absorbent resin |
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| JP5599513B2 (ja) * | 2011-06-29 | 2014-10-01 | 株式会社日本触媒 | ポリアクリル酸（塩）系吸水性樹脂粉末及びその製造方法 |
| US9320822B2 (en) | 2012-02-17 | 2016-04-26 | Nippon Shokubai Co., Ltd. | Polyacrylic acid (salt) water-absorbing resin and manufacturing method therefor |
| EP2912110B1 (de) | 2012-10-24 | 2018-12-05 | Evonik Degussa GmbH | Geruchs- und farbstabile wasserabsorbierende zusammensetzung |
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| WO2015046604A1 (ja) | 2013-09-30 | 2015-04-02 | 株式会社日本触媒 | 粒子状吸水剤の充填方法および粒子状吸水剤充填物のサンプリング方法 |
| JP2017006808A (ja) | 2013-11-14 | 2017-01-12 | 株式会社日本触媒 | ポリアクリル酸（塩）系吸水性樹脂の製造方法 |
| US20150283284A1 (en) * | 2014-04-07 | 2015-10-08 | Evonik Corporation | Superabsorbent polymer having fast absorption |
| KR102223611B1 (ko) * | 2014-04-25 | 2021-03-11 | 송원산업 주식회사 | 흡수성 폴리머 입자를 제조하기 위한, 과-중화를 이용한 모노머 처리 방법 |
| JP5766344B1 (ja) † | 2014-07-11 | 2015-08-19 | 住友精化株式会社 | 吸水性樹脂及び吸収性物品 |
| JP5719079B1 (ja) * | 2014-07-11 | 2015-05-13 | 住友精化株式会社 | 吸水性樹脂及び吸収性物品 |
| US12600849B2 (en) | 2020-03-23 | 2026-04-14 | Lg Chem, Ltd. | Super absorbent polymer film and preparation method thereof |
| EP4074763A4 (en) * | 2020-03-23 | 2023-01-25 | Lg Chem, Ltd. | Super absorbent resin film and preparation method thereof |
| EP4074764B1 (en) | 2020-03-23 | 2025-10-15 | Lg Chem, Ltd. | Preparation method for super absorbent polymer film |
| JP7591415B2 (ja) * | 2021-01-29 | 2024-11-28 | 株式会社日本触媒 | 吸水性樹脂の製造方法 |
| CN121909219A (zh) * | 2023-09-29 | 2026-04-21 | 住友精化株式会社 | 制造吸水性树脂粒子的方法及控制吸水性树脂粒子的粒径的方法 |
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-
2002
- 2002-12-17 WO PCT/JP2002/013161 patent/WO2003051940A1/en not_active Ceased
- 2002-12-17 DE DE60233590T patent/DE60233590D1/de not_active Expired - Lifetime
- 2002-12-17 EP EP02805022A patent/EP1456259B1/en not_active Revoked
- 2002-12-17 CN CN2006100515342A patent/CN1831019B/zh not_active Expired - Fee Related
- 2002-12-17 CN CNB028055136A patent/CN1279067C/zh not_active Expired - Lifetime
- 2002-12-17 US US10/472,039 patent/US7049366B2/en not_active Expired - Lifetime
- 2002-12-17 BR BRPI0206696-3B1A patent/BR0206696B1/pt active IP Right Grant
- 2002-12-17 KR KR1020037010833A patent/KR100549717B1/ko not_active Expired - Lifetime
- 2002-12-18 JP JP2002366969A patent/JP4150253B2/ja not_active Expired - Fee Related
-
2003
- 2003-01-12 SA SA03230508A patent/SA03230508B1/ar unknown
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