JP2001509530A - カップリング剤として多官能化されたポリオルガノシロキサン（白色フィラー／エラストマー）を含む、白色フィラーで強化されたジエンゴム組成物 - Google Patents

カップリング剤として多官能化されたポリオルガノシロキサン（白色フィラー／エラストマー）を含む、白色フィラーで強化されたジエンゴム組成物

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Publication number
JP2001509530A
JP2001509530A JP2000502111A JP2000502111A JP2001509530A JP 2001509530 A JP2001509530 A JP 2001509530A JP 2000502111 A JP2000502111 A JP 2000502111A JP 2000502111 A JP2000502111 A JP 2000502111A JP 2001509530 A JP2001509530 A JP 2001509530A
Authority
JP
Japan
Prior art keywords
group
pos
white filler
elastomer
composition
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Ceased
Application number
JP2000502111A
Other languages
English (en)
Japanese (ja)
Other versions
JP2001509530A5 (enExample
Inventor
フレデリック シロン
クロード ラフォール
ジャン ルーク マンジェール
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Compagnie Generale des Etablissements Michelin SCA
Original Assignee
Compagnie Generale des Etablissements Michelin SCA
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Compagnie Generale des Etablissements Michelin SCA filed Critical Compagnie Generale des Etablissements Michelin SCA
Publication of JP2001509530A publication Critical patent/JP2001509530A/ja
Publication of JP2001509530A5 publication Critical patent/JP2001509530A5/ja
Ceased legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K3/00—Use of inorganic substances as compounding ingredients
    • C08K3/34—Silicon-containing compounds
    • C08K3/36—Silica
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B60—VEHICLES IN GENERAL
    • B60C—VEHICLE TYRES; TYRE INFLATION; TYRE CHANGING; CONNECTING VALVES TO INFLATABLE ELASTIC BODIES IN GENERAL; DEVICES OR ARRANGEMENTS RELATED TO TYRES
    • B60C1/00—Tyres characterised by the chemical composition or the physical arrangement or mixture of the composition
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B60—VEHICLES IN GENERAL
    • B60C—VEHICLE TYRES; TYRE INFLATION; TYRE CHANGING; CONNECTING VALVES TO INFLATABLE ELASTIC BODIES IN GENERAL; DEVICES OR ARRANGEMENTS RELATED TO TYRES
    • B60C1/00—Tyres characterised by the chemical composition or the physical arrangement or mixture of the composition
    • B60C1/0008—Compositions of the inner liner
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B60—VEHICLES IN GENERAL
    • B60C—VEHICLE TYRES; TYRE INFLATION; TYRE CHANGING; CONNECTING VALVES TO INFLATABLE ELASTIC BODIES IN GENERAL; DEVICES OR ARRANGEMENTS RELATED TO TYRES
    • B60C1/00—Tyres characterised by the chemical composition or the physical arrangement or mixture of the composition
    • B60C1/0016—Compositions of the tread
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B60—VEHICLES IN GENERAL
    • B60C—VEHICLE TYRES; TYRE INFLATION; TYRE CHANGING; CONNECTING VALVES TO INFLATABLE ELASTIC BODIES IN GENERAL; DEVICES OR ARRANGEMENTS RELATED TO TYRES
    • B60C1/00—Tyres characterised by the chemical composition or the physical arrangement or mixture of the composition
    • B60C1/0025—Compositions of the sidewalls
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G77/00—Macromolecular compounds obtained by reactions forming a linkage containing silicon with or without sulfur, nitrogen, oxygen or carbon in the main chain of the macromolecule
    • C08G77/04—Polysiloxanes
    • C08G77/38—Polysiloxanes modified by chemical after-treatment
    • C08G77/382—Polysiloxanes modified by chemical after-treatment containing atoms other than carbon, hydrogen, oxygen or silicon
    • C08G77/392—Polysiloxanes modified by chemical after-treatment containing atoms other than carbon, hydrogen, oxygen or silicon containing sulfur
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K3/00—Use of inorganic substances as compounding ingredients
    • C08K3/01—Use of inorganic substances as compounding ingredients characterized by their specific function
    • C08K3/013—Fillers, pigments or reinforcing additives
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K5/00—Use of organic ingredients
    • C08K5/54—Silicon-containing compounds
    • C08K5/5403—Silicon-containing compounds containing no other elements than carbon or hydrogen
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L21/00—Compositions of unspecified rubbers
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L23/00—Compositions of homopolymers or copolymers of unsaturated aliphatic hydrocarbons having only one carbon-to-carbon double bond; Compositions of derivatives of such polymers
    • C08L23/02—Compositions of homopolymers or copolymers of unsaturated aliphatic hydrocarbons having only one carbon-to-carbon double bond; Compositions of derivatives of such polymers not modified by chemical after-treatment
    • C08L23/18—Homopolymers or copolymers of hydrocarbons having four or more carbon atoms
    • C08L23/20—Homopolymers or copolymers of hydrocarbons having four or more carbon atoms having four to nine carbon atoms
    • C08L23/22—Copolymers of isobutene; Butyl rubber; Homopolymers or copolymers of other iso-olefins
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L25/00—Compositions of, homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by an aromatic carbocyclic ring; Compositions of derivatives of such polymers
    • C08L25/02—Homopolymers or copolymers of hydrocarbons
    • C08L25/04—Homopolymers or copolymers of styrene
    • C08L25/08—Copolymers of styrene
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L7/00—Compositions of natural rubber
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L83/00—Compositions of macromolecular compounds obtained by reactions forming in the main chain of the macromolecule a linkage containing silicon with or without sulfur, nitrogen, oxygen or carbon only; Compositions of derivatives of such polymers
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L9/00—Compositions of homopolymers or copolymers of conjugated diene hydrocarbons
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L9/00—Compositions of homopolymers or copolymers of conjugated diene hydrocarbons
    • C08L9/06—Copolymers with styrene

Landscapes

  • Chemical & Material Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Mechanical Engineering (AREA)
  • General Chemical & Material Sciences (AREA)
  • Compositions Of Macromolecular Compounds (AREA)
JP2000502111A 1997-07-11 1998-07-10 カップリング剤として多官能化されたポリオルガノシロキサン（白色フィラー／エラストマー）を含む、白色フィラーで強化されたジエンゴム組成物 Ceased JP2001509530A (ja)

Applications Claiming Priority (5)

Application Number Priority Date Filing Date Title
FR97/09047 1997-07-11
FR9709047 1997-07-11
FR98/01452 1998-02-04
FR9801452 1998-02-04
PCT/EP1998/004308 WO1999002602A1 (fr) 1997-07-11 1998-07-10 Composition de caoutchouc dienique renforcee d'une charge blanche, comportant a titre d'agent de couplage (charge blanche/elastomere) un polyorganosiloxane multifonctionnalise

Publications (2)

Publication Number Publication Date
JP2001509530A true JP2001509530A (ja) 2001-07-24
JP2001509530A5 JP2001509530A5 (enExample) 2008-06-26

Family

ID=26233680

Family Applications (1)

Application Number Title Priority Date Filing Date
JP2000502111A Ceased JP2001509530A (ja) 1997-07-11 1998-07-10 カップリング剤として多官能化されたポリオルガノシロキサン（白色フィラー／エラストマー）を含む、白色フィラーで強化されたジエンゴム組成物

Country Status (12)

Country Link
US (1) US6313205B1 (enExample)
EP (1) EP0996676B1 (enExample)
JP (1) JP2001509530A (enExample)
KR (1) KR100511701B1 (enExample)
CN (1) CN1214069C (enExample)
AU (1) AU8807198A (enExample)
BR (1) BR9811001A (enExample)
CA (1) CA2296010A1 (enExample)
DE (1) DE69806008T2 (enExample)
ES (1) ES2177038T3 (enExample)
PL (1) PL338041A1 (enExample)
WO (1) WO1999002602A1 (enExample)

Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2003020539A1 (en) * 2001-09-04 2003-03-13 The Yokohama Rubber Co., Ltd. Pneumatic tire and method of producing the same
WO2004076207A1 (ja) * 2003-02-27 2004-09-10 The Yokohama Rubber Co., Ltd. 空気入りタイヤ及びその製造方法
JP2007509209A (ja) * 2003-10-24 2007-04-12 ランクセス・インク． シリカ充填エラストマーコンパウンド
JP2015214620A (ja) * 2014-05-08 2015-12-03 株式会社ブリヂストン ゴム組成物、インナーライナー、シーラントおよび空気入りタイヤ
JP2017502149A (ja) * 2013-12-27 2017-01-19 株式会社ブリヂストン メルカプト官能性シロキサンを含む組成物から調製した加硫ゴム及びタイヤ部品

Families Citing this family (52)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE19905820A1 (de) * 1998-10-27 2000-05-04 Degussa Schwefelfunktionelle Polyorganosilane
CN100334135C (zh) * 2000-06-16 2007-08-29 米其林技术公司 含有多官能聚有机硅氧烷作为偶联剂的轮胎橡胶组合物
EP1311600A2 (fr) 2000-07-31 2003-05-21 Société de Technologie Michelin Bande de roulement pour pneumatique
DE10044989A1 (de) * 2000-09-11 2002-03-21 Bayer Ag Flüssige schwefelhaltige Oligosiloxane und ihre Verwendung in Kautschukmischungen
EP1258373B1 (en) * 2001-05-15 2007-07-18 Sumitomo Rubber Industries Limited Rubber composition for tire tread and pneumatic tire using the same
JP4536375B2 (ja) 2001-06-28 2010-09-01 ソシエテ ド テクノロジー ミシュラン 極めて低い比表面積のシリカで強化されたタイヤトレッド
WO2003002648A1 (fr) 2001-06-28 2003-01-09 Societe De Technologie Michelin Bande de roulement pour pneumatique renforcee d'une silice a basse surface specifique
FR2849045B1 (fr) * 2002-12-19 2005-01-21 Rhodia Chimie Sa Oligomeres polyorganosiloxane portant des fonctions thiols ou episulfures et leurs procedes de preparation
EP1576044A1 (fr) * 2002-12-19 2005-09-21 Société de Technologie Michelin COMPOSITION DE CAOUTCHOUC POUR PNEUMATIQUE COMPORTANT UN OLIGOMERE POLYORGANOSILOXANE A TITRE D’AGENT DE COUPLAGE
MY164448A (en) 2003-12-15 2017-12-15 Ciba Holding Inc Coupling agents between filler and elastomer
WO2006102518A1 (en) 2005-03-24 2006-09-28 Bridgestone Corporation Compounding silica-reinforced rubber with low volatile organic compound (voc) emission
FR2886303B1 (fr) * 2005-05-26 2007-07-20 Rhodia Chimie Sa Utilisation d'une combinaison particuliere d'un agent de couplage et d'un agent de recouvrement, comme systeme de couplage(charge blanche-elastomere) dans les compositions de caoutchouc comprenant une charge inorganique
US8119710B2 (en) * 2005-09-21 2012-02-21 Basf Se Filled rubber compounds with improved processability
US7915368B2 (en) 2007-05-23 2011-03-29 Bridgestone Corporation Method for making alkoxy-modified silsesquioxanes
US8501895B2 (en) 2007-05-23 2013-08-06 Bridgestone Corporation Method for making alkoxy-modified silsesquioxanes and amino alkoxy-modified silsesquioxanes
US8962746B2 (en) 2007-12-27 2015-02-24 Bridgestone Corporation Methods of making blocked-mercapto alkoxy-modified silsesquioxane compounds
US8794282B2 (en) 2007-12-31 2014-08-05 Bridgestone Corporation Amino alkoxy-modified silsesquioxane adhesives for improved metal adhesion and metal adhesion retention to cured rubber
US8513371B2 (en) 2007-12-31 2013-08-20 Bridgestone Corporation Amino alkoxy-modified silsesquioxanes and method of preparation
DE102008001007A1 (de) * 2008-04-04 2009-10-08 Robert Bosch Gmbh Silikon-Polymer modifizierte Gummi-Zusammensetzungen, Verfahren zu ihrer Herstellung sowie dieses Material umfassende Scheibenwischer
CN101260190B (zh) * 2008-04-28 2011-04-27 华南理工大学 多官能度聚硅氧烷偶联剂及其制备方法
FR2940290B1 (fr) 2008-12-22 2010-12-31 Michelin Soc Tech Agent de couplage mercaptosilane bloque
FR2945815B1 (fr) 2009-05-20 2011-07-01 Michelin Soc Tech Composition de caoutchouc comportant un agent de couplage organosilane
FR2947552B1 (fr) 2009-05-20 2011-08-26 Michelin Soc Tech Agent de couplage organosilane
FR2954774B1 (fr) 2009-10-30 2012-01-06 Michelin Soc Tech Methode de preparation d'un melange maitre de caoutchouc naturel et de silice
FR2952064B1 (fr) 2009-10-30 2012-08-31 Michelin Soc Tech Methode de preparation d'un melange maitre d'elastomere dienique et de silice
FR2954775B1 (fr) 2009-10-30 2012-03-30 Michelin Soc Tech Methode de preparation d'un melange maitre d'elastomere dienique synthetique et de silice
US8642691B2 (en) 2009-12-28 2014-02-04 Bridgestone Corporation Amino alkoxy-modified silsesquioxane adhesives for improved metal adhesion and metal adhesion retention to cured rubber
FR2962440B1 (fr) * 2010-07-12 2012-08-03 Total Raffinage Marketing Procede de preparation de polymeres greffes sans amorceur et sans solvant et compositions bitume/polymere comprenant lesdits polymeres greffes
FR2974093B1 (fr) 2011-04-15 2015-05-08 Michelin Soc Tech Procede de preparation d'un melange maitre d'elastomere et d'une charge inorganique renforcante
FR2981078B1 (fr) 2011-10-11 2013-11-01 Michelin Soc Tech Methode pour preparer un melange maitre d'elastomere dienique et de silice
FR2981077B1 (fr) 2011-10-11 2013-11-01 Michelin Soc Tech Methode pour preparer un melange maitre d'elastomere dienique et de silice
FR2981081B1 (fr) 2011-10-11 2013-11-01 Michelin Soc Tech Methode de preparation d'un melange maitre de caoutchouc naturel et de silice
FR2981076B1 (fr) 2011-10-11 2013-11-01 Michelin Soc Tech Methode pour preparer un melange maitre d'elastomere dienique et de silice
FR2981080B1 (fr) 2011-10-11 2013-11-01 Michelin Soc Tech Methode de preparation d'un melange maitre de caoutchouc naturel et de silice dopee magnesium
FR2981079B1 (fr) 2011-10-11 2013-11-01 Michelin Soc Tech Methode pour preparer un melange maitre d'elastomere dienique et de silice
FR2984326B1 (fr) 2011-12-16 2014-01-10 Michelin Soc Tech Agent de couplage mercaptosilane bloque
EP2960286B1 (en) * 2013-02-25 2019-10-30 The Yokohama Rubber Co., Ltd. Rubber composition for tire tread, and pneumatic tire using same
KR101625032B1 (ko) * 2013-02-25 2016-05-27 요코하마 고무 가부시키가이샤 타이어용 고무 조성물 및 이것을 이용하는 공기입 타이어
KR101686611B1 (ko) * 2013-02-25 2016-12-14 요코하마 고무 가부시키가이샤 타이어 트레드용 고무 조성물 및 이것을 이용하는 공기입 타이어
CN114016318A (zh) 2014-12-31 2022-02-08 株式会社普利司通 用于将钢合金粘附到橡胶的氨基烷氧基改性倍半硅氧烷粘合剂
FR3038320A1 (fr) 2015-07-02 2017-01-06 Michelin & Cie Composition de caoutchouc comprenant une silice de tres haute surface specifique et une resine hydrocarbonee de faible temperature de transition vitreuse
EP3263359A1 (en) * 2016-06-28 2018-01-03 Sumitomo Rubber Industries, Ltd. Rubber composition for sealants
FR3053345B1 (fr) 2016-06-30 2018-07-06 Compagnie Generale Des Etablissements Michelin Composition de caoutchouc comprenant un agent de couplage polysulfure de monohydroxysilane
FR3053337B1 (fr) 2016-06-30 2018-07-06 Compagnie Generale Des Etablissements Michelin Polysulfure de monohydroxysilane
WO2018045291A1 (en) 2016-09-02 2018-03-08 Bridgestone Corporation Production of cis-1,4-polydienes with multiple silane functional groups prepared by in-situ hydrosilylation of polymer cement
FR3060565A1 (fr) 2016-12-16 2018-06-22 Michelin & Cie Polysulfure d'alcoxysilane
FR3065960B1 (fr) 2017-05-05 2019-06-28 Compagnie Generale Des Etablissements Michelin Composition de caoutchouc comprenant au moins une silice en tant que charge renforcante inorganique
FR3079842B1 (fr) 2018-04-06 2020-10-09 Michelin & Cie Pneumatique comportant une composition de caoutchouc comprenant un nouvel agent de couplage polysulfure porteur de groupes associatifs azotes
FR3079841B1 (fr) 2018-04-06 2020-10-09 Michelin & Cie Pneumatique comportant une composition de caoutchouc comprenant un nouvel agent de couplage polysulfure porteur de groupes associatifs azotes
FR3113906B1 (fr) 2020-09-04 2022-08-05 Michelin & Cie Composition de caoutchouc a base d’elastomere dienique fortement sature
FR3113905B1 (fr) 2020-09-04 2022-08-05 Michelin & Cie Composition de caoutchouc a base d’elastomere dienique fortement sature
CN116082641B (zh) * 2021-11-08 2024-07-09 中蓝晨光化工有限公司 一种t型对称结构的大分子烷氧基硅烷处理剂及其制备方法与应用

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GB1310379A (en) * 1970-12-10 1973-03-21 Ppg Industries Inc Tire tread
JPS6248743A (ja) * 1985-08-28 1987-03-03 Shin Etsu Chem Co Ltd ゴム組成物
US4725630A (en) * 1987-06-01 1988-02-16 Wacker Silicones Corporation α, β-unsaturated carbonyl-functional silicone compositions
US6191247B1 (en) * 1996-04-10 2001-02-20 The Yokohama Rubber Co., Ltd. Polysiloxane composition having superior storage stability and rubber composition containing same

Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2003020539A1 (en) * 2001-09-04 2003-03-13 The Yokohama Rubber Co., Ltd. Pneumatic tire and method of producing the same
WO2004076207A1 (ja) * 2003-02-27 2004-09-10 The Yokohama Rubber Co., Ltd. 空気入りタイヤ及びその製造方法
JP2004262274A (ja) * 2003-02-27 2004-09-24 Yokohama Rubber Co Ltd:The 空気入りタイヤ及びその製造方法
JP2007509209A (ja) * 2003-10-24 2007-04-12 ランクセス・インク． シリカ充填エラストマーコンパウンド
JP2017502149A (ja) * 2013-12-27 2017-01-19 株式会社ブリヂストン メルカプト官能性シロキサンを含む組成物から調製した加硫ゴム及びタイヤ部品
JP2015214620A (ja) * 2014-05-08 2015-12-03 株式会社ブリヂストン ゴム組成物、インナーライナー、シーラントおよび空気入りタイヤ

Also Published As

Publication number Publication date
EP0996676A1 (fr) 2000-05-03
CN1265126A (zh) 2000-08-30
AU8807198A (en) 1999-02-08
WO1999002602A1 (fr) 1999-01-21
DE69806008T2 (de) 2002-11-28
KR20010021698A (ko) 2001-03-15
BR9811001A (pt) 2000-11-07
EP0996676B1 (fr) 2002-06-12
ES2177038T3 (es) 2002-12-01
US6313205B1 (en) 2001-11-06
KR100511701B1 (ko) 2005-09-02
PL338041A1 (en) 2000-09-25
DE69806008D1 (de) 2002-07-18
CA2296010A1 (fr) 1999-01-21
CN1214069C (zh) 2005-08-10

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