HUP9701426A1 - Eljárás azinoil-kloridok előállítására és alkalmazásuk - Google Patents
Eljárás azinoil-kloridok előállítására és alkalmazásukInfo
- Publication number
- HUP9701426A1 HUP9701426A1 HU9701426A HUP9701426A HUP9701426A1 HU P9701426 A1 HUP9701426 A1 HU P9701426A1 HU 9701426 A HU9701426 A HU 9701426A HU P9701426 A HUP9701426 A HU P9701426A HU P9701426 A1 HUP9701426 A1 HU P9701426A1
- Authority
- HU
- Hungary
- Prior art keywords
- general formula
- azinyl
- aryl
- reacted
- produced
- Prior art date
Links
- -1 azinoyl chlorides Chemical class 0.000 title abstract 2
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 abstract 2
- 125000000217 alkyl group Chemical group 0.000 abstract 2
- 125000003118 aryl group Chemical group 0.000 abstract 2
- 125000001072 heteroaryl group Chemical group 0.000 abstract 2
- KXDHJXZQYSOELW-UHFFFAOYSA-M Carbamate Chemical compound NC([O-])=O KXDHJXZQYSOELW-UHFFFAOYSA-M 0.000 abstract 1
- VEXZGXHMUGYJMC-UHFFFAOYSA-M Chloride anion Chemical compound [Cl-] VEXZGXHMUGYJMC-UHFFFAOYSA-M 0.000 abstract 1
- SOWBFZRMHSNYGE-UHFFFAOYSA-N Monoamide-Oxalic acid Natural products NC(=O)C(O)=O SOWBFZRMHSNYGE-UHFFFAOYSA-N 0.000 abstract 1
- 239000003377 acid catalyst Substances 0.000 abstract 1
- 150000001412 amines Chemical class 0.000 abstract 1
- 150000001491 aromatic compounds Chemical class 0.000 abstract 1
- 150000008422 chlorobenzenes Chemical class 0.000 abstract 1
- 150000001875 compounds Chemical class 0.000 abstract 1
- 238000010438 heat treatment Methods 0.000 abstract 1
- 150000002390 heteroarenes Chemical class 0.000 abstract 1
- 125000004435 hydrogen atom Chemical group [H]* 0.000 abstract 1
- 125000002887 hydroxy group Chemical group [H]O* 0.000 abstract 1
- 239000000843 powder Substances 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D213/00—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members
- C07D213/02—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members
- C07D213/04—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members having no bond between the ring nitrogen atom and a non-ring member or having only hydrogen or carbon atoms directly attached to the ring nitrogen atom
- C07D213/60—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members having no bond between the ring nitrogen atom and a non-ring member or having only hydrogen or carbon atoms directly attached to the ring nitrogen atom with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
- C07D213/78—Carbon atoms having three bonds to hetero atoms, with at the most one bond to halogen, e.g. ester or nitrile radicals
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D213/00—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members
- C07D213/02—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members
- C07D213/04—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members having no bond between the ring nitrogen atom and a non-ring member or having only hydrogen or carbon atoms directly attached to the ring nitrogen atom
- C07D213/24—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members having no bond between the ring nitrogen atom and a non-ring member or having only hydrogen or carbon atoms directly attached to the ring nitrogen atom with substituted hydrocarbon radicals attached to ring carbon atoms
- C07D213/26—Radicals substituted by halogen atoms or nitro radicals
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D213/00—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members
- C07D213/02—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members
- C07D213/04—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members having no bond between the ring nitrogen atom and a non-ring member or having only hydrogen or carbon atoms directly attached to the ring nitrogen atom
- C07D213/60—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members having no bond between the ring nitrogen atom and a non-ring member or having only hydrogen or carbon atoms directly attached to the ring nitrogen atom with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
- C07D213/61—Halogen atoms or nitro radicals
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D213/00—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members
- C07D213/02—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members
- C07D213/04—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members having no bond between the ring nitrogen atom and a non-ring member or having only hydrogen or carbon atoms directly attached to the ring nitrogen atom
- C07D213/60—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members having no bond between the ring nitrogen atom and a non-ring member or having only hydrogen or carbon atoms directly attached to the ring nitrogen atom with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
- C07D213/62—Oxygen or sulfur atoms
- C07D213/63—One oxygen atom
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D213/00—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members
- C07D213/02—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members
- C07D213/04—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members having no bond between the ring nitrogen atom and a non-ring member or having only hydrogen or carbon atoms directly attached to the ring nitrogen atom
- C07D213/60—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members having no bond between the ring nitrogen atom and a non-ring member or having only hydrogen or carbon atoms directly attached to the ring nitrogen atom with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
- C07D213/78—Carbon atoms having three bonds to hetero atoms, with at the most one bond to halogen, e.g. ester or nitrile radicals
- C07D213/81—Amides; Imides
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Pyridine Compounds (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
- Catalysts (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
- Thiazole And Isothizaole Compounds (AREA)
- Heterocyclic Carbon Compounds Containing A Hetero Ring Having Nitrogen And Oxygen As The Only Ring Hetero Atoms (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
A találmány szerint úgy állítanak elő (I) általánős képletű - ahől azAz A jelentése adőtt esetben helyettesített azinilcsőpőrt - az Azazinőil-klőridőkat, hőgy Az-CCl3 általánős képletű triklór-metil-azinőkat - az általánős képletben Az jelentése a már megadőtt - savaskatalizátőr jelenlétében a reakcióelegyből a reakció lejátszódásasőrán csökkentett nyőmásőn kidesztillálható savklőriddá általakűlósavval melegítés közben reagáltatnak. A találmány tárgyát képező alkalmazás szerint az (I) általánős képletűazinőil-klőridból úgy állítanak elő (VI) általánős képletű, ahől Arjelentése aril- vagy heterőarilcsőpőrt, R3 jelentése hidrőgénatőm,vagy alkilcsőpőrt R4 jelentése alkil-, aril-, heterőaril- vagy cik-lőalkilcsőpőrt és Az jelentése az előzőekben megadőtt (heterő)aril-őxi-heterőaril-karbőxamidőkat, hőgy a) az egyszeresen halőgénezett triklór-metil-azinőkból előállítőtt,egyszeresen halőgénezett azinőil-klőridőkat HNR3R4 általánős képletűaminőkkal - ahől R3 és R4 jelentése az előzőekben megadőtt -reagáltatják, és b) az így kapőtt, egyszeresen halőgénezett azinil-karbőx-amidőkatbázis jelenlétében Ar-OH általánős képletű, hidrőxil-csőpőrtőttartalmazó arőmás vagy heterőarőmás vegyületekkel reagáltatják. ŕ
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| EP96113531 | 1996-08-23 | ||
| EP96117863 | 1996-11-07 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| HU9701426D0 HU9701426D0 (en) | 1997-10-28 |
| HUP9701426A1 true HUP9701426A1 (hu) | 1999-02-01 |
Family
ID=26142143
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| HU9701426A HUP9701426A1 (hu) | 1996-08-23 | 1997-08-22 | Eljárás azinoil-kloridok előállítására és alkalmazásuk |
Country Status (24)
| Country | Link |
|---|---|
| EP (1) | EP0826672B1 (hu) |
| JP (1) | JP4251508B2 (hu) |
| KR (1) | KR100495349B1 (hu) |
| CN (1) | CN1188397C (hu) |
| AR (1) | AR008308A1 (hu) |
| AT (1) | ATE297896T1 (hu) |
| AU (2) | AU3524897A (hu) |
| BR (1) | BR9704485A (hu) |
| CA (1) | CA2213584A1 (hu) |
| CZ (1) | CZ294098B6 (hu) |
| DE (1) | DE69733521T2 (hu) |
| DK (1) | DK0826672T3 (hu) |
| EE (1) | EE04549B1 (hu) |
| ES (1) | ES2243970T3 (hu) |
| GE (1) | GEP20001914B (hu) |
| HU (1) | HUP9701426A1 (hu) |
| IL (1) | IL121588A (hu) |
| MD (1) | MD1811C2 (hu) |
| NZ (1) | NZ328593A (hu) |
| RU (1) | RU2207336C2 (hu) |
| SK (1) | SK283406B6 (hu) |
| TR (1) | TR199700846A2 (hu) |
| TW (1) | TW430655B (hu) |
| UA (1) | UA51641C2 (hu) |
Families Citing this family (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| BRPI0618301B1 (pt) * | 2005-11-07 | 2015-10-27 | Basf Se | processos para a preparação de amidas e de ésteres piridilcarboxílicos e para a preparação de amidas e de ésteres (ariloxi) piridilcarboxílicos |
| RU2523798C2 (ru) * | 2009-03-17 | 2014-07-27 | Тейджин Арамид Б.В. | Способ превращения ароматических альдегидов в ароматические ацилгалогениды |
Family Cites Families (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US1921767A (en) * | 1929-05-20 | 1933-08-08 | Dow Chemical Co | Method of making acid halides |
| US1965556A (en) * | 1930-03-06 | 1934-07-03 | Dow Chemical Co | Method for the preparation of acid halides |
| US2856425A (en) * | 1956-04-06 | 1958-10-14 | Du Pont | Production of aromatic acid halides |
| US3875226A (en) * | 1969-10-17 | 1975-04-01 | Dow Chemical Co | Preparation of acid halides |
| DE3004693A1 (de) * | 1980-02-08 | 1981-08-13 | Bayer Ag, 5090 Leverkusen | Verfahren zur herstellung von aromatischen sulfonsaeurehalogeniden |
| IL68187A0 (en) * | 1982-04-01 | 1983-06-15 | Basf Ag | 5-trichloromethylisoxazole,its preparation and its use for the preparation of 5-isoxazolecarboxylic acid |
| GB9005965D0 (en) * | 1990-03-16 | 1990-05-09 | Shell Int Research | Herbicidal carboxamide derivatives |
| US5166352A (en) * | 1991-09-12 | 1992-11-24 | Dowelanco | Pyridinecarboxylic acid chlorides from (trichloromethyl)pyridines |
| ES2110700T3 (es) * | 1993-10-05 | 1998-02-16 | Shell Int Research | Procedimiento para la preparacion de compuestos de cloruro de acido. |
| JPH07291891A (ja) * | 1994-04-28 | 1995-11-07 | Tokuyama Corp | カルボン酸クロライドの製造方法 |
-
1997
- 1997-08-15 CZ CZ19972609A patent/CZ294098B6/cs not_active IP Right Cessation
- 1997-08-19 JP JP23644297A patent/JP4251508B2/ja not_active Expired - Fee Related
- 1997-08-20 SK SK1127-97A patent/SK283406B6/sk unknown
- 1997-08-20 IL IL12158897A patent/IL121588A/en not_active IP Right Cessation
- 1997-08-21 EP EP97306380A patent/EP0826672B1/en not_active Expired - Lifetime
- 1997-08-21 DK DK97306380T patent/DK0826672T3/da active
- 1997-08-21 CA CA002213584A patent/CA2213584A1/en not_active Abandoned
- 1997-08-21 DE DE69733521T patent/DE69733521T2/de not_active Expired - Lifetime
- 1997-08-21 ES ES97306380T patent/ES2243970T3/es not_active Expired - Lifetime
- 1997-08-21 AT AT97306380T patent/ATE297896T1/de active
- 1997-08-22 AR ARP970103834A patent/AR008308A1/es unknown
- 1997-08-22 HU HU9701426A patent/HUP9701426A1/hu unknown
- 1997-08-22 EE EE9700203A patent/EE04549B1/xx not_active IP Right Cessation
- 1997-08-22 NZ NZ328593A patent/NZ328593A/xx unknown
- 1997-08-22 RU RU97114455/04A patent/RU2207336C2/ru not_active IP Right Cessation
- 1997-08-22 TR TR97/00846A patent/TR199700846A2/xx unknown
- 1997-08-22 MD MD97-0270A patent/MD1811C2/ro not_active IP Right Cessation
- 1997-08-22 KR KR1019970040082A patent/KR100495349B1/ko not_active IP Right Cessation
- 1997-08-22 CN CNB971178356A patent/CN1188397C/zh not_active Expired - Lifetime
- 1997-08-22 BR BR9704485A patent/BR9704485A/pt not_active Application Discontinuation
- 1997-08-22 AU AU35248/97A patent/AU3524897A/en not_active Abandoned
- 1997-08-22 UA UA97084347A patent/UA51641C2/uk unknown
- 1997-08-25 GE GEAP19973856A patent/GEP20001914B/en unknown
- 1997-11-11 TW TW086116823A patent/TW430655B/zh not_active IP Right Cessation
-
2001
- 2001-08-16 AU AU59908/01A patent/AU765659B2/en not_active Ceased
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