GB614354A - Manufacture of water-soluble dyestuffs - Google Patents

Manufacture of water-soluble dyestuffs

Info

Publication number
GB614354A
GB614354A GB2077746A GB2077746A GB614354A GB 614354 A GB614354 A GB 614354A GB 2077746 A GB2077746 A GB 2077746A GB 2077746 A GB2077746 A GB 2077746A GB 614354 A GB614354 A GB 614354A
Authority
GB
United Kingdom
Prior art keywords
water
dyestuffs
soluble
salts
aliphatic
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
GB2077746A
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Imperial Chemical Industries Ltd
Original Assignee
Imperial Chemical Industries Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Imperial Chemical Industries Ltd filed Critical Imperial Chemical Industries Ltd
Priority to GB2077746A priority Critical patent/GB614354A/en
Publication of GB614354A publication Critical patent/GB614354A/en
Expired legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
    • C09B67/00—Influencing the physical, e.g. the dyeing or printing properties of dyestuffs without chemical reactions, e.g. by treating with solvents grinding or grinding assistants, coating of pigments or dyes; Process features in the making of dyestuff preparations; Dyestuff preparations of a special physical nature, e.g. tablets, films
    • C09B67/0001—Post-treatment of organic pigments or dyes
    • C09B67/0003—Drying, e.g. sprax drying; Sublimation of the solvent
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
    • D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
    • D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
    • D06P1/655—Compounds containing ammonium groups
    • D06P1/66—Compounds containing ammonium groups containing quaternary ammonium groups

Abstract

Water-soluble dyestuffs, especially direct cotton dyestuffs of the azo and stilbene-azo series, are obtained in pulverulent form by drying the water-soluble dyestuffs, or mixtures of the water-soluble dyestuffs in water-soluble form with other coloured or colourless water-soluble compounds, in the presence of one or more surface-active agents selected from the following classes: (1) aliphatic alcohols containing at least 12 carbon atoms and obtainable from natural oils and fats (e.g. cetyl or oleyl alcohol), and their sulphates and salts thereof (e.g. the sodium salt of sulphated sperm oil alcohols); (2) aliphatic acids containing at least 12 carbon atoms and obtainable from natural oils and fats, and their salts and esters (e.g. oleic acid and its sodium and diphenylguanidine salts); (3) aliphatic or aromatic amines, amides and quaternary ammonium salts with at least one aliphatic radical containing at least 12 carbon atoms attached to the nitrogen atom (e.g. cetyltrimethylammonium bromide or sodium 4 - oleylamino - 1 - methoxybenzene - 2 - sulphonate); (4) condensation products of ethylene oxide with alcohols, phenols, carboxylic acids, amines or amides (e.g. cetyl alcohol condensed with 4, 17 or 30 molecular proportions of ethylene oxide or sperm oil alcohols condensed with 2.5 molecular proportions of ethylene oxide). The surface-active agent may be added at any stage in the manufacture of the dyestuff paste, conveniently to the solution or suspension of the dyestuff immediately before or during salting out, or (in solution) to the dyestuff immediately before the final drying operation, which may be carried out in any known type of dryer or by admixture with a water absorbing salt (e.g. sodium sulphate). Examples describe the application of the process to the following dyestuffs: (1), (4), (6) and (7) the product obtained by condensing 4 : 41 - dinitrodibenzyl - 2 - sulphonic acid with 2 - methyl - 5 - methoxy - 4 - aminoazobenzene - 41 - sulphonic acid in the presence of caustic soda; (2) Rhodamine B base; (3) and (5) the product obtained by condensing 4 : 41-dinitrodibenzyl-2 : 21-disulphonic acid with 4-aminoazobenzene-41-sulphonic acid in the presence of caustic soda. Specifications 17677/07, [Class 2], 491,793 and 526,760 are referred to.
GB2077746A 1946-07-11 1946-07-11 Manufacture of water-soluble dyestuffs Expired GB614354A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
GB2077746A GB614354A (en) 1946-07-11 1946-07-11 Manufacture of water-soluble dyestuffs

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
GB2077746A GB614354A (en) 1946-07-11 1946-07-11 Manufacture of water-soluble dyestuffs

Publications (1)

Publication Number Publication Date
GB614354A true GB614354A (en) 1948-12-14

Family

ID=10151509

Family Applications (1)

Application Number Title Priority Date Filing Date
GB2077746A Expired GB614354A (en) 1946-07-11 1946-07-11 Manufacture of water-soluble dyestuffs

Country Status (1)

Country Link
GB (1) GB614354A (en)

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3003844A (en) * 1957-06-10 1961-10-10 Gen Aniline & Film Corp Stable solution for producing ice colors
US4425134A (en) 1979-10-02 1984-01-10 Ciba-Geigy Corporation Process for producing agglomerates of water-soluble dyes

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3003844A (en) * 1957-06-10 1961-10-10 Gen Aniline & Film Corp Stable solution for producing ice colors
US4425134A (en) 1979-10-02 1984-01-10 Ciba-Geigy Corporation Process for producing agglomerates of water-soluble dyes

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