FI110093B - Kobolthydroxid eller koboltlegeringshydroxid med hög densitet och stor partikelstorlek - Google Patents

Kobolthydroxid eller koboltlegeringshydroxid med hög densitet och stor partikelstorlek Download PDF

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Publication number
FI110093B
FI110093B FI991478A FI991478A FI110093B FI 110093 B FI110093 B FI 110093B FI 991478 A FI991478 A FI 991478A FI 991478 A FI991478 A FI 991478A FI 110093 B FI110093 B FI 110093B
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Prior art keywords
hydroxide
cobalt
metal
particle size
mixed
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FI991478A
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English (en)
Finnish (fi)
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FI991478A (sv
FI991478A0 (sv
Inventor
Mika Martikainen
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Omg Kokkola Chemicals Oy
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Publication of FI991478A0 publication Critical patent/FI991478A0/sv
Priority to FI991478A priority Critical patent/FI110093B/sv
Priority to CA2377152A priority patent/CA2377152C/en
Priority to AT00944062T priority patent/ATE286855T1/de
Priority to ES00944062T priority patent/ES2235906T3/es
Priority to EP00944062A priority patent/EP1210295B1/en
Priority to CNB008097429A priority patent/CN1164499C/zh
Priority to JP2001506951A priority patent/JP3961826B2/ja
Priority to DE60017421T priority patent/DE60017421T2/de
Priority to PCT/FI2000/000581 priority patent/WO2001000532A1/en
Priority to AU58298/00A priority patent/AU5829800A/en
Publication of FI991478A publication Critical patent/FI991478A/sv
Priority to NO20016394A priority patent/NO20016394L/no
Application granted granted Critical
Publication of FI110093B publication Critical patent/FI110093B/sv

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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B82NANOTECHNOLOGY
    • B82YSPECIFIC USES OR APPLICATIONS OF NANOSTRUCTURES; MEASUREMENT OR ANALYSIS OF NANOSTRUCTURES; MANUFACTURE OR TREATMENT OF NANOSTRUCTURES
    • B82Y30/00Nanotechnology for materials or surface science, e.g. nanocomposites
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01GCOMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G51/00Compounds of cobalt
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01GCOMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G51/00Compounds of cobalt
    • C01G51/04Oxides; Hydroxides
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01MPROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00Electrodes
    • H01M4/02Electrodes composed of, or comprising, active material
    • H01M4/36Selection of substances as active materials, active masses, active liquids
    • H01M4/48Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides
    • H01M4/52Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides of nickel, cobalt or iron
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01MPROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00Electrodes
    • H01M4/86Inert electrodes with catalytic activity, e.g. for fuel cells
    • H01M4/90Selection of catalytic material
    • H01M4/9016Oxides, hydroxides or oxygenated metallic salts
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2002/00Crystal-structural characteristics
    • C01P2002/60Compounds characterised by their crystallite size
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00Particle morphology
    • C01P2004/51Particles with a specific particle size distribution
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00Particle morphology
    • C01P2004/60Particles characterised by their size
    • C01P2004/61Micrometer sized, i.e. from 1-100 micrometer
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00Particle morphology
    • C01P2004/60Particles characterised by their size
    • C01P2004/62Submicrometer sized, i.e. from 0.1-1 micrometer
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00Particle morphology
    • C01P2004/60Particles characterised by their size
    • C01P2004/64Nanometer sized, i.e. from 1-100 nanometer
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00Physical properties of inorganic compounds
    • C01P2006/10Solid density
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00Physical properties of inorganic compounds
    • C01P2006/12Surface area
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01MPROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00Electrodes
    • H01M4/02Electrodes composed of, or comprising, active material
    • H01M4/36Selection of substances as active materials, active masses, active liquids
    • H01M4/48Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides
    • H01M4/52Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides of nickel, cobalt or iron
    • H01M4/525Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides of nickel, cobalt or iron of mixed oxides or hydroxides containing iron, cobalt or nickel for inserting or intercalating light metals, e.g. LiNiO2, LiCoO2 or LiCoOxFy
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02EREDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
    • Y02E60/00Enabling technologies; Technologies with a potential or indirect contribution to GHG emissions mitigation
    • Y02E60/10Energy storage using batteries
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02EREDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
    • Y02E60/00Enabling technologies; Technologies with a potential or indirect contribution to GHG emissions mitigation
    • Y02E60/30Hydrogen technology
    • Y02E60/50Fuel cells

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Inorganic Chemistry (AREA)
  • Nanotechnology (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Electrochemistry (AREA)
  • General Chemical & Material Sciences (AREA)
  • Materials Engineering (AREA)
  • Physics & Mathematics (AREA)
  • Condensed Matter Physics & Semiconductors (AREA)
  • General Physics & Mathematics (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Composite Materials (AREA)
  • Inorganic Compounds Of Heavy Metals (AREA)
  • Battery Electrode And Active Subsutance (AREA)
  • Catalysts (AREA)
  • Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)

Claims (8)

1. Kobolthydroxid eller en av kobolt och nickel, mangan, magnesium eller aluminium eller en blandning av dessa bildad blandhydroxid, kännetecknad av att dess volymvikt är ca 0,5-2,2 g/cm3, partikelstorlek mer än ca 1 pm, typiskt ca 1-20 pm 5 och en specifik yta ca 0,5-20 m2/g och att den är framställd genom att till en vatten-haltig kloridlösning av kobolt eller till en vattenhaltig kloridlösning av kobolt och nickel, mangan, magnesium eller aluminium eller en blandning av dessa under alka-liska betingelser tillsätta en komplexbildarsubstans och hydroxidjoner för att bilda metallhydroxid, varvid komplexbildarsubstansen väljs sä, att den bildar ett ammoni-10 umkomplex med metalljonen medan molförhällandet mellan komplexbildarsubstansen och metallen är ca 0,5-3 och pH regleras till 10-13.
2. Kobolthydroxid eller en blandhydroxid enligt patentkrav 1, kännetecknad av att pH regleras till ett pH intervall 11,2-12,0.
3. Kobolthydroxid eller en blandhydroxid enligt patentkrav 1, kännetecknad av 15 att kloridlösningens koncentration är i intervallet 10 -120 g/1 räknat med avseende pä den totala metallhalten.
4. Kobolthydroxid eller en blandhydroxid enligt patentkrav 1, kännetecknad av att komplexbildarsubstansen är ammoniumsulfat eller vattenhaltig ammoniak.
;· ’ 5. Kobolthydroxid eller en blandhydroxid enligt patentkrav 1, kännetecknad av . 20 att molförhällandet mellan komplexbildarsubstansen och metallen är ca 1,5-2.
*“·* 6. Kobolthydroxid eller en blandhydroxid enligt patentkrav 1, kännetecknad av : :: att man till regiering av pH använder NaOH.
7. Kobolthydroxid eller en blandhydroxid enligt patentkrav 1, kännetecknad av att reaktionen genomförs vid en temperatur av ca 40-90 °C. •" ’ ;25
8. Kobolthydroxid eller en blandhydroxid enligt patentkrav 7, kännetecknad av att reaktionen genomförs vid en temperatur av ca 70 °C. « · ·
FI991478A 1999-06-29 1999-06-29 Kobolthydroxid eller koboltlegeringshydroxid med hög densitet och stor partikelstorlek FI110093B (sv)

Priority Applications (11)

Application Number Priority Date Filing Date Title
FI991478A FI110093B (sv) 1999-06-29 1999-06-29 Kobolthydroxid eller koboltlegeringshydroxid med hög densitet och stor partikelstorlek
JP2001506951A JP3961826B2 (ja) 1999-06-29 2000-06-28 高密度及び大きな粒径の水酸化コバルト又はコバルト混合水酸化物の製造方法及びこの方法により製造される製造物
AT00944062T ATE286855T1 (de) 1999-06-29 2000-06-28 Verfahren zur herstellung von kobalthydroxiden oder gemischten kobalthydroxiden mit hoher dichte und grosser teilchengrösse, sowie die mit diesem verfahren erhaltenen produkte
ES00944062T ES2235906T3 (es) 1999-06-29 2000-06-28 Procedimiento para fabricar hidroxido de cobalto, o hidroxidos mixtos de cobalto, de alta densidad y gran tamaño de particula y un producto fabricado mediante este procedimiento.
EP00944062A EP1210295B1 (en) 1999-06-29 2000-06-28 Process for making high density and large particle size cobalt hydroxide or cobalt mixed hydroxides and a product made by this process
CNB008097429A CN1164499C (zh) 1999-06-29 2000-06-28 氢氧化钴或由钴与其它金属形成的合金氢氧化物
CA2377152A CA2377152C (en) 1999-06-29 2000-06-28 Process for making high density and large particle size cobalt hydroxide or cobalt mixed hydroxides and a product made by this process
DE60017421T DE60017421T2 (de) 1999-06-29 2000-06-28 Verfahren zur herstellung von kobalthydroxiden oder gemischten kobalthydroxiden mit hoher dichte und grosser teilchengrösse, sowie die mit diesem verfahren erhaltenen produkte
PCT/FI2000/000581 WO2001000532A1 (en) 1999-06-29 2000-06-28 Process for making high density and large particle size cobalt hydroxide or cobalt mixed hydroxides and a product made by this process
AU58298/00A AU5829800A (en) 1999-06-29 2000-06-28 Process for making high density and large particle size cobalt hydroxide or cobalt mixed hydroxides and a product made by this process
NO20016394A NO20016394L (no) 1999-06-29 2001-12-27 Prosess for å lage kobolthydroksid eller koboltblandede hydroksider med höy tetthet og stor partikkelstörrelse og etprodukt laget ved denne prosessen

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
FI991478 1999-06-29
FI991478A FI110093B (sv) 1999-06-29 1999-06-29 Kobolthydroxid eller koboltlegeringshydroxid med hög densitet och stor partikelstorlek

Publications (3)

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FI991478A0 FI991478A0 (sv) 1999-06-29
FI991478A FI991478A (sv) 2000-12-30
FI110093B true FI110093B (sv) 2002-11-29

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FI991478A FI110093B (sv) 1999-06-29 1999-06-29 Kobolthydroxid eller koboltlegeringshydroxid med hög densitet och stor partikelstorlek

Country Status (11)

Country Link
EP (1) EP1210295B1 (sv)
JP (1) JP3961826B2 (sv)
CN (1) CN1164499C (sv)
AT (1) ATE286855T1 (sv)
AU (1) AU5829800A (sv)
CA (1) CA2377152C (sv)
DE (1) DE60017421T2 (sv)
ES (1) ES2235906T3 (sv)
FI (1) FI110093B (sv)
NO (1) NO20016394L (sv)
WO (1) WO2001000532A1 (sv)

Families Citing this family (20)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP4359092B2 (ja) * 2003-08-21 2009-11-04 Agcセイミケミカル株式会社 二次電池正極用のリチウムコバルト複合酸化物の製造方法
CN1733599B (zh) * 2004-08-13 2010-04-28 中国人民解放军63971部队 过渡金属氧化物或氢氧化物湿凝胶的制备方法
JP4846280B2 (ja) * 2005-06-23 2011-12-28 株式会社田中化学研究所 オキシ水酸化コバルト粒子及びその製造方法
JP4846309B2 (ja) * 2005-09-09 2011-12-28 株式会社田中化学研究所 ニッケルマンガンコバルト複合酸化物の製造方法
JP4746476B2 (ja) * 2006-05-10 2011-08-10 三井金属鉱業株式会社 水酸化コバルト粒子および酸化コバルト粒子
JP4746477B2 (ja) * 2006-05-10 2011-08-10 三井金属鉱業株式会社 水酸化コバルト粒子および酸化コバルト粒子
CN101955234B (zh) * 2009-07-15 2012-04-04 海南金亿新材料股份有限公司 一种高纯纳米级氢氧化钴的制备方法
WO2012164141A1 (en) * 2011-05-31 2012-12-06 Omg Kokkola Chemicals Oy Lithium cobalt oxide material
US10351440B2 (en) 2011-05-31 2019-07-16 Freeport Colbalt Oy Lithium cobalt oxide material
JP5961004B2 (ja) * 2012-02-21 2016-08-02 日本化学工業株式会社 水酸化コバルトの製造方法、酸化コバルトの製造方法及びコバルト酸リチウムの製造方法
CN103232076A (zh) * 2013-05-16 2013-08-07 漳州师范学院 不同粒径氢氧化钴的合成方法
JP6233175B2 (ja) 2014-02-05 2017-11-22 住友金属鉱山株式会社 水酸化コバルト粒子及びその製造方法、並びに正極活物質及びその製造方法
CN105304897B (zh) * 2014-11-29 2017-09-15 广东天劲新能源科技股份有限公司 一种大颗粒氢氧化钴电池材料的制备方法
CN104439280A (zh) * 2014-12-09 2015-03-25 英德佳纳金属科技有限公司 一种同时制备氢氧化钴和钴粉的方法
CN104445442B (zh) * 2014-12-09 2016-05-11 英德佳纳金属科技有限公司 一种低氯/硫、大粒径氢氧化钴及其制备方法
CN106552630A (zh) * 2016-10-26 2017-04-05 上海纳米技术及应用国家工程研究中心有限公司 一种球状CoOX基催化剂及制备方法和应用
CN110676063A (zh) * 2019-08-19 2020-01-10 深圳职业技术学院 一种高导电性氢氧化钴电极材料、其制备方法以及一种电极和电容器
CN113753965B (zh) * 2021-08-24 2022-11-15 广东邦普循环科技有限公司 一种氢氧化钴的合成方法及氢氧化钴
CN114735759A (zh) * 2022-05-20 2022-07-12 宁波互邦新材料有限公司 一种锂电池正极材料回收生产锂电池氢氧化亚钴的方法
CN114835172B (zh) * 2022-05-31 2023-11-03 荆门市格林美新材料有限公司 一种氢氧化钴颗粒及其制备方法与应用

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US5057299A (en) * 1989-12-08 1991-10-15 Minnesota Mining And Manufacturing Company Method for making beta cobaltous hydroxide
US5569444A (en) * 1990-06-18 1996-10-29 Blanchard; Philippe Process of obtaining a metal hydroxide powder and powder obtained by the process

Also Published As

Publication number Publication date
JP3961826B2 (ja) 2007-08-22
FI991478A (sv) 2000-12-30
DE60017421D1 (de) 2005-02-17
CA2377152C (en) 2010-05-25
ATE286855T1 (de) 2005-01-15
AU5829800A (en) 2001-01-31
CN1164499C (zh) 2004-09-01
JP2003503300A (ja) 2003-01-28
EP1210295B1 (en) 2005-01-12
FI991478A0 (sv) 1999-06-29
ES2235906T3 (es) 2005-07-16
NO20016394L (no) 2002-02-28
CA2377152A1 (en) 2001-01-04
DE60017421T2 (de) 2005-12-22
CN1359353A (zh) 2002-07-17
WO2001000532A1 (en) 2001-01-04
NO20016394D0 (no) 2001-12-27
EP1210295A1 (en) 2002-06-05

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