ES3024465T3 - Method of preparing epoxidation catalysts - Google Patents

Method of preparing epoxidation catalysts Download PDF

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Publication number
ES3024465T3
ES3024465T3 ES15740332T ES15740332T ES3024465T3 ES 3024465 T3 ES3024465 T3 ES 3024465T3 ES 15740332 T ES15740332 T ES 15740332T ES 15740332 T ES15740332 T ES 15740332T ES 3024465 T3 ES3024465 T3 ES 3024465T3
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ES
Spain
Prior art keywords
solid
catalyst
column
titanium tetrachloride
produce
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Active
Application number
ES15740332T
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English (en)
Spanish (es)
Inventor
Roger Grey
Debra Jackson
Daniel White
Sandor Nagy
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Lyondell Chemical Technology LP
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Lyondell Chemical Technology LP
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Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J21/00—Catalysts comprising the elements, oxides, or hydroxides of magnesium, boron, aluminium, carbon, silicon, titanium, zirconium, or hafnium
    • B01J21/06—Silicon, titanium, zirconium or hafnium; Oxides or hydroxides thereof
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J21/00—Catalysts comprising the elements, oxides, or hydroxides of magnesium, boron, aluminium, carbon, silicon, titanium, zirconium, or hafnium
    • B01J21/06—Silicon, titanium, zirconium or hafnium; Oxides or hydroxides thereof
    • B01J21/08—Silica
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J29/00—Catalysts comprising molecular sieves
    • B01J29/03—Catalysts comprising molecular sieves not having base-exchange properties
    • B01J29/0308—Mesoporous materials not having base exchange properties, e.g. Si-MCM-41
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J29/00—Catalysts comprising molecular sieves
    • B01J29/89—Silicates, aluminosilicates or borosilicates of titanium, zirconium or hafnium
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J35/00—Catalysts, in general, characterised by their form or physical properties
    • B01J35/60—Catalysts, in general, characterised by their form or physical properties characterised by their surface properties or porosity
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/02—Impregnation, coating or precipitation
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/02—Impregnation, coating or precipitation
    • B01J37/0201—Impregnation
    • B01J37/0203—Impregnation the impregnation liquid containing organic compounds
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/06—Washing
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/08—Heat treatment
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D301/00—Preparation of oxiranes
    • C07D301/02—Synthesis of the oxirane ring
    • C07D301/03—Synthesis of the oxirane ring by oxidation of unsaturated compounds, or of mixtures of unsaturated and saturated compounds
    • C07D301/12—Synthesis of the oxirane ring by oxidation of unsaturated compounds, or of mixtures of unsaturated and saturated compounds with hydrogen peroxide or inorganic peroxides or peracids
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D301/00—Preparation of oxiranes
    • C07D301/02—Synthesis of the oxirane ring
    • C07D301/03—Synthesis of the oxirane ring by oxidation of unsaturated compounds, or of mixtures of unsaturated and saturated compounds
    • C07D301/19—Synthesis of the oxirane ring by oxidation of unsaturated compounds, or of mixtures of unsaturated and saturated compounds with organic hydroperoxides
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2229/00—Aspects of molecular sieve catalysts not covered by B01J29/00
    • B01J2229/10—After treatment, characterised by the effect to be obtained
    • B01J2229/18—After treatment, characterised by the effect to be obtained to introduce other elements into or onto the molecular sieve itself
    • B01J2229/186—After treatment, characterised by the effect to be obtained to introduce other elements into or onto the molecular sieve itself not in framework positions
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2229/00—Aspects of molecular sieve catalysts not covered by B01J29/00
    • B01J2229/30—After treatment, characterised by the means used
    • B01J2229/32—Reaction with silicon compounds, e.g. TEOS, siliconfluoride
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J35/00—Catalysts, in general, characterised by their form or physical properties
    • B01J35/60—Catalysts, in general, characterised by their form or physical properties characterised by their surface properties or porosity
    • B01J35/63—Pore volume
    • B01J35/635—0.5-1.0 ml/g
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/02—Impregnation, coating or precipitation
    • B01J37/0201—Impregnation
    • B01J37/0209—Impregnation involving a reaction between the support and a fluid

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Physics & Mathematics (AREA)
  • Thermal Sciences (AREA)
  • Inorganic Chemistry (AREA)
  • Dispersion Chemistry (AREA)
  • Catalysts (AREA)
  • Epoxy Compounds (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
ES15740332T 2014-01-22 2015-01-22 Method of preparing epoxidation catalysts Active ES3024465T3 (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US201461930192P 2014-01-22 2014-01-22
PCT/US2015/012382 WO2015112672A1 (en) 2014-01-22 2015-01-22 Method of preparing epoxidation catalysts

Publications (1)

Publication Number Publication Date
ES3024465T3 true ES3024465T3 (en) 2025-06-04

Family

ID=53681920

Family Applications (1)

Application Number Title Priority Date Filing Date
ES15740332T Active ES3024465T3 (en) 2014-01-22 2015-01-22 Method of preparing epoxidation catalysts

Country Status (10)

Country Link
US (1) US9433925B2 (enExample)
EP (1) EP3096879B1 (enExample)
JP (1) JP6301482B2 (enExample)
KR (1) KR101799718B1 (enExample)
CN (1) CN105916581A (enExample)
BR (1) BR112016016282B1 (enExample)
ES (1) ES3024465T3 (enExample)
SA (1) SA516371507B1 (enExample)
SG (1) SG11201605483XA (enExample)
WO (1) WO2015112672A1 (enExample)

Families Citing this family (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106582809B (zh) * 2016-12-22 2019-08-30 红宝丽集团股份有限公司 一种烯烃环氧化催化剂及其制备方法
JP7128884B2 (ja) * 2018-03-15 2022-08-31 住友化学株式会社 チタン含有珪素酸化物成型体の製造方法、及びチタン含有珪素酸化物成型体
CN109675566A (zh) * 2019-01-30 2019-04-26 兰州城市学院 一种Co-Ti双金属有序介孔催化剂及其制备方法和应用
WO2021060263A1 (ja) * 2019-09-25 2021-04-01 住友化学株式会社 プロピレンオキサイドの製造方法
KR20220092567A (ko) * 2019-11-04 2022-07-01 라이온델 케미칼 테크놀로지, 엘.피. 티탄화 촉매, 티탄화 촉매의 제조 방법, 및 에폭시화 방법

Family Cites Families (15)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4367342A (en) 1969-04-02 1983-01-04 Shell Oil Company Olefin epoxidation
US4021454A (en) 1971-08-19 1977-05-03 Shell Oil Company Olefin epoxidation
JP3658790B2 (ja) * 1995-03-30 2005-06-08 住友化学株式会社 触媒及びオキシラン化合物の製造方法
US6011162A (en) * 1997-05-05 2000-01-04 Arco Chemical Technology, L.P. Epoxidation process using improved heterogeneous catalyst composition
ES2213285T3 (es) 1997-05-05 2004-08-16 Arco Chemical Technology, L.P. Procedimiento de epoxidacion usando una composicion de catalizador heterogeneo mejorada.
US6114552A (en) 1999-09-28 2000-09-05 Arco Chemical Technology, L.P. Heterogeneous epoxidation catalyst
MY131860A (en) 2000-06-21 2007-09-28 Shell Int Research Process for preparation of catalyst and use there of
US20050014960A1 (en) 2003-06-30 2005-01-20 Buijink Jan Karel Frederik Catalyst preparation
JP4599868B2 (ja) * 2004-03-30 2010-12-15 三菱化学株式会社 水添触媒およびその製造方法
US7276464B2 (en) * 2004-06-17 2007-10-02 Lyondell Chemical Technology, L.P. Titanium zeolite catalysts
US7875568B2 (en) * 2004-12-17 2011-01-25 Yangzi Petrochemical Company Co., Ltd. Supported nonmetallocene olefin polymerization catalyst, preparation method and use thereof
PL2065087T3 (pl) * 2007-11-30 2012-06-29 Borealis Tech Oy Sposób wytwarzania statystycznych kopolimerów propylenu
JP2009274062A (ja) * 2008-04-17 2009-11-26 Sumitomo Chemical Co Ltd チタノシリケート
MX339546B (es) * 2009-11-27 2016-05-30 Basf Se Proceso para la preparacion de un catalizador de zeolita de titanio.
JP5917511B2 (ja) * 2010-07-20 2016-05-18 カウンスィル オブ サイエンティフィック アンド インダストリアル リサーチＣｏｕｎｃｉｌ Ｏｆ Ｓｃｉｅｎｔｉｆｉｃ ＆ Ｉｎｄｕｓｔｒｉａｌ Ｒｅｓｅａｒｃｈ 規則性メソポーラスチタノケイ酸塩およびその調製のための方法

Also Published As

Publication number Publication date
CN105916581A (zh) 2016-08-31
EP3096879A1 (en) 2016-11-30
EP3096879B1 (en) 2025-04-02
JP6301482B2 (ja) 2018-03-28
WO2015112672A1 (en) 2015-07-30
US20150375200A1 (en) 2015-12-31
JP2017505223A (ja) 2017-02-16
SA516371507B1 (ar) 2018-06-27
BR112016016282B1 (pt) 2024-01-16
EP3096879A4 (en) 2017-09-27
US9433925B2 (en) 2016-09-06
KR20160111941A (ko) 2016-09-27
KR101799718B1 (ko) 2017-11-20
SG11201605483XA (en) 2016-08-30
BR112016016282A2 (enExample) 2017-08-08

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