ES2514290B2 - Negros de humo modificados que tienen cantidades de hidrocarburos poliaromáticos (pah) bajas y elastómeros que contienen los mismos. - Google Patents

Negros de humo modificados que tienen cantidades de hidrocarburos poliaromáticos (pah) bajas y elastómeros que contienen los mismos. Download PDF

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Publication number
ES2514290B2
ES2514290B2 ES201490096A ES201490096A ES2514290B2 ES 2514290 B2 ES2514290 B2 ES 2514290B2 ES 201490096 A ES201490096 A ES 201490096A ES 201490096 A ES201490096 A ES 201490096A ES 2514290 B2 ES2514290 B2 ES 2514290B2
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low
pah
elastomer
same
polyaromatic hydrocarbon
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ES2514290R1 (es
ES2514290A2 (es
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Frederick H. Rumpf
Michael D. Morris
James A. Belmont
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Cabot Corp
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Cabot Corp
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    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K5/00—Use of organic ingredients
    • C08K5/16—Nitrogen-containing compounds
    • C08K5/34—Heterocyclic compounds having nitrogen in the ring
    • C08K5/3467—Heterocyclic compounds having nitrogen in the ring having more than two nitrogen atoms in the ring
    • C08K5/3472—Five-membered rings
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K5/00—Use of organic ingredients
    • C08K5/36—Sulfur-, selenium-, or tellurium-containing compounds
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09C—TREATMENT OF INORGANIC MATERIALS, OTHER THAN FIBROUS FILLERS, TO ENHANCE THEIR PIGMENTING OR FILLING PROPERTIES ; PREPARATION OF CARBON BLACK  ; PREPARATION OF INORGANIC MATERIALS WHICH ARE NO SINGLE CHEMICAL COMPOUNDS AND WHICH ARE MAINLY USED AS PIGMENTS OR FILLERS
    • C09C1/00—Treatment of specific inorganic materials other than fibrous fillers; Preparation of carbon black
    • C09C1/44—Carbon
    • C09C1/48—Carbon black
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09C—TREATMENT OF INORGANIC MATERIALS, OTHER THAN FIBROUS FILLERS, TO ENHANCE THEIR PIGMENTING OR FILLING PROPERTIES ; PREPARATION OF CARBON BLACK  ; PREPARATION OF INORGANIC MATERIALS WHICH ARE NO SINGLE CHEMICAL COMPOUNDS AND WHICH ARE MAINLY USED AS PIGMENTS OR FILLERS
    • C09C1/00—Treatment of specific inorganic materials other than fibrous fillers; Preparation of carbon black
    • C09C1/44—Carbon
    • C09C1/48—Carbon black
    • C09C1/50—Furnace black ; Preparation thereof
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09C—TREATMENT OF INORGANIC MATERIALS, OTHER THAN FIBROUS FILLERS, TO ENHANCE THEIR PIGMENTING OR FILLING PROPERTIES ; PREPARATION OF CARBON BLACK  ; PREPARATION OF INORGANIC MATERIALS WHICH ARE NO SINGLE CHEMICAL COMPOUNDS AND WHICH ARE MAINLY USED AS PIGMENTS OR FILLERS
    • C09C1/00—Treatment of specific inorganic materials other than fibrous fillers; Preparation of carbon black
    • C09C1/44—Carbon
    • C09C1/48—Carbon black
    • C09C1/52—Channel black ; Preparation thereof
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09C—TREATMENT OF INORGANIC MATERIALS, OTHER THAN FIBROUS FILLERS, TO ENHANCE THEIR PIGMENTING OR FILLING PROPERTIES ; PREPARATION OF CARBON BLACK  ; PREPARATION OF INORGANIC MATERIALS WHICH ARE NO SINGLE CHEMICAL COMPOUNDS AND WHICH ARE MAINLY USED AS PIGMENTS OR FILLERS
    • C09C1/00—Treatment of specific inorganic materials other than fibrous fillers; Preparation of carbon black
    • C09C1/44—Carbon
    • C09C1/48—Carbon black
    • C09C1/54—Acetylene black; thermal black ; Preparation thereof
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09C—TREATMENT OF INORGANIC MATERIALS, OTHER THAN FIBROUS FILLERS, TO ENHANCE THEIR PIGMENTING OR FILLING PROPERTIES ; PREPARATION OF CARBON BLACK  ; PREPARATION OF INORGANIC MATERIALS WHICH ARE NO SINGLE CHEMICAL COMPOUNDS AND WHICH ARE MAINLY USED AS PIGMENTS OR FILLERS
    • C09C1/00—Treatment of specific inorganic materials other than fibrous fillers; Preparation of carbon black
    • C09C1/44—Carbon
    • C09C1/48—Carbon black
    • C09C1/56—Treatment of carbon black ; Purification
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2002/00—Crystal-structural characteristics
    • C01P2002/80—Crystal-structural characteristics defined by measured data other than those specified in group C01P2002/70
    • C01P2002/87—Crystal-structural characteristics defined by measured data other than those specified in group C01P2002/70 by chromatography data, e.g. HPLC, gas chromatography
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00—Physical properties of inorganic compounds
    • C01P2006/12—Surface area
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K3/00—Use of inorganic substances as compounding ingredients
    • C08K3/02—Elements
    • C08K3/04—Carbon
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K9/00—Use of pretreated ingredients
    • C08K9/04—Ingredients treated with organic substances
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09C—TREATMENT OF INORGANIC MATERIALS, OTHER THAN FIBROUS FILLERS, TO ENHANCE THEIR PIGMENTING OR FILLING PROPERTIES ; PREPARATION OF CARBON BLACK  ; PREPARATION OF INORGANIC MATERIALS WHICH ARE NO SINGLE CHEMICAL COMPOUNDS AND WHICH ARE MAINLY USED AS PIGMENTS OR FILLERS
    • C09C3/00—Treatment in general of inorganic materials, other than fibrous fillers, to enhance their pigmenting or filling properties
    • C09C3/08—Treatment with low-molecular-weight non-polymer organic compounds
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02T—CLIMATE CHANGE MITIGATION TECHNOLOGIES RELATED TO TRANSPORTATION
    • Y02T10/00—Road transport of goods or passengers
    • Y02T10/80—Technologies aiming to reduce greenhouse gasses emissions common to all road transportation technologies
    • Y02T10/86—Optimisation of rolling resistance, e.g. weight reduction 

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Pigments, Carbon Blacks, Or Wood Stains (AREA)
  • Compositions Of Macromolecular Compounds (AREA)
  • Carbon And Carbon Compounds (AREA)
  • Inks, Pencil-Leads, Or Crayons (AREA)

Abstract

Se describen negros de humo modificados, tal como negro de hules, que tienen una concentración de PAH baja. Adicionalmente, además se describen composiciones de hule o elastoméricas que contienen el negro de humo modificado de la presente invención, así como métodos para hacer negro de humo modificado que tiene una concentración PAH baja.

Description

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P201490096
02-09-2014
heteroarileno, o alquilarileno sustituido o no sustituido;
k es un entero desde 1 hasta 8; y
Q es (CH2)w, (CH2)x O(CH2)z, (CH2)x NR(CH2)z, o (CH2)x S(CH2)z, donde x es 1 hasta 6, z es 1 hasta 6, y w es 2 hasta 6. SkR puede ser SkH. Para SkR, cuando R no es H, k es 2 hasta 8, y 5 cuando R es H, k es 1 hasta 8;
E es un grupo que contiene poliazufre, tal como Sw (donde w es 2 hasta 8), SSO, SSO2, SOSO2, SO2SO2; y
el triazol puede opcionalmente estar N-sustituido con un sustituyente NDD’, donde
D y D’, que son los mismos o diferentes, son H o alquilo C1-C4.
10 Los ejemplos más específicos del triazol incluyen, pero no se limitan a, 3-amino-1,2,4-triazol-5tiol, 3-amino-1,2,4-triazol-5-il-disulfuro; 1,2,4-triazol-3-tiol; 1,2,4-triazol-3-il-disulfuro; 3-amino1,2,4-triazol-5-il-trisulfuro; 4-amino-3-hidrazino-1,2,4-triazol-5-tiol, y los similares.
Para propósitos de la presente invención, el pirazol incluye un químico que tiene un grupo que contiene pirazol. El pirazol puede ser un polipirazol que contiene tiol o polisulfuro. Los ejemplos 15 del pirazol pueden incluir un pirazol que tiene la fórmula (o tautómeros del mismo):
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o un pirazol que tiene la fórmula (o tautómeros del mismo):
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P201490096
02-09-2014
de calor alto a 1400 C durante 2 hrs en un horno que reduce los niveles de PAH significativamente como se muestra en la Tabla 3. Como también puede apreciarse, la actividad de la superficie se afectó en gran parte (desactivado), por ejemplo como se muestra por el I2No, que aumentó significativamente, que refleja los efecto del tratamiento de calor.
El negro de humo CB-2, como se muestra en la Tabla 4 y Tabla 5 a continuación, luego se trató para unir/adsorber un grupo químico, como se describe en el Ejemplo 2 para obtener CB-3, o como se describe en el Ejemplo 3 para obtener CB-4. Se señala que diversos experimentos con los varios CB1-7 se repitieron como se muestra en las tablas a continuación.
Tabla 4
Compuestos sSBR
Corrida
Muestras CB Actividad de la superficie Histéresis Resistencia
BR MB %
max tan D-60 M300/M100
1
CB-1 (control) 35.7 0.257 4.12
2
CB-6 (recocido únicamente) 28.5 0.386 3.34
3
CB-5 (control) 40.5 0.363 4.01
4
CB-2 (recocido únicamente) 7.4 0.325 2.23
5
CB-3 (presente invención) 18.3 0.255 3.00
70
P201490096
02-09-2014
(continuación)
Compuestos sSBR
Corrida
Muestras CB Actividad de la superficie Histéresis Resistencia
BR MB %
max tan D-60 M300/M100
6
CB-4 (presente invención) 37.2 0.252 3.33
7
CB-6 (recocido) 28.5 0.377 3.48
8
CB-5 (control) 37.4 0.364 3.91
9
CB-7 (presente invención) 35.6 0.284 3.77
10
CB-2 (recocido) 8.2 0.333 2.17
11
CB-7 (presente invención) 39.6 0.286 3.83
71
P201490096
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Tabla 5
Compuestos NR
Corrida
Muestra CB Actividad de la superficie Histéresis Resistencia
BR
TDmax@60C M300/M100
12
CB-1 43.8 0.169 5.31
13
CB-2 33 0.186 3.16
14
CB-2 35 0.198 3.17
15
CB-3 44 0.138 4.24
16
CB-3 46 0.131 4.34
17
CB-6 76 0.226 5.00
18
CB-6 76 0.223 5.03
19
CB-5 76 0.203 5.31
20
CB-5 72 0.196 5.39
21
CB-7 72 0.137 5.06
22
CB-7 70 0.15 4.96
23
CB-6 72 0.224 4.80
24
CB-5 74 0.205 5.62
Similarmente, el negro de humo CB-5 fue similar a un negro de humo comercialmente disponible de Cabot Corporation. Este negro de humo es “tal cual” sin ningún tratamiento para
72
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Claims (1)

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ES201490096A 2012-03-02 2013-02-28 Negros de humo modificados que tienen cantidades de hidrocarburos poliaromáticos (pah) bajas y elastómeros que contienen los mismos. Active ES2514290B2 (es)

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US201261606282P 2012-03-02 2012-03-02
US61/606,282 2012-03-02
PCT/US2013/028269 WO2013130772A1 (en) 2012-03-02 2013-02-28 Modified carbon blacks having low pah amounts and elastomers containing the same

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ES2514290A2 ES2514290A2 (es) 2014-10-27
ES2514290R1 ES2514290R1 (es) 2014-11-24
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JP (2) JP6247231B2 (es)
KR (1) KR101664639B1 (es)
CN (1) CN104334649B (es)
AU (1) AU2013225987B2 (es)
CA (1) CA2865000C (es)
CL (1) CL2014002305A1 (es)
CO (1) CO7131386A2 (es)
CZ (1) CZ2014562A3 (es)
DE (1) DE112013001250B4 (es)
ES (1) ES2514290B2 (es)
FR (1) FR2987625B1 (es)
GB (1) GB2514499A (es)
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MY (1) MY173227A (es)
PL (1) PL233772B1 (es)
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SK (1) SK288666B6 (es)
WO (1) WO2013130772A1 (es)

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