EP2600090A1 - Procédé et dispositif destinés à la production d'oxygène sous pression par décomposition à basse température de l'air - Google Patents

Procédé et dispositif destinés à la production d'oxygène sous pression par décomposition à basse température de l'air Download PDF

Info

Publication number
EP2600090A1
EP2600090A1 EP12007828.2A EP12007828A EP2600090A1 EP 2600090 A1 EP2600090 A1 EP 2600090A1 EP 12007828 A EP12007828 A EP 12007828A EP 2600090 A1 EP2600090 A1 EP 2600090A1
Authority
EP
European Patent Office
Prior art keywords
pressure
air
oxygen
compressed
heat exchanger
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
EP12007828.2A
Other languages
German (de)
English (en)
Other versions
EP2600090B1 (fr
Inventor
Alexander Alekseev
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Linde GmbH
Original Assignee
Linde GmbH
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Family has litigation
First worldwide family litigation filed litigation Critical https://patents.darts-ip.com/?family=47191487&utm_source=google_patent&utm_medium=platform_link&utm_campaign=public_patent_search&patent=EP2600090(A1) "Global patent litigation dataset” by Darts-ip is licensed under a Creative Commons Attribution 4.0 International License.
Application filed by Linde GmbH filed Critical Linde GmbH
Priority to EP12007828.2A priority Critical patent/EP2600090B1/fr
Publication of EP2600090A1 publication Critical patent/EP2600090A1/fr
Application granted granted Critical
Publication of EP2600090B1 publication Critical patent/EP2600090B1/fr
Not-in-force legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Images

Classifications

    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J3/00—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification
    • F25J3/02—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream
    • F25J3/04—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream for air
    • F25J3/04151—Purification and (pre-)cooling of the feed air; recuperative heat-exchange with product streams
    • F25J3/04187—Cooling of the purified feed air by recuperative heat-exchange; Heat-exchange with product streams
    • F25J3/04193—Division of the main heat exchange line in consecutive sections having different functions
    • F25J3/042—Division of the main heat exchange line in consecutive sections having different functions having an intermediate feed connection
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J3/00—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification
    • F25J3/02—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream
    • F25J3/04—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream for air
    • F25J3/04006—Providing pressurised feed air or process streams within or from the air fractionation unit
    • F25J3/04012—Providing pressurised feed air or process streams within or from the air fractionation unit by compression of warm gaseous streams; details of intake or interstage cooling
    • F25J3/04018—Providing pressurised feed air or process streams within or from the air fractionation unit by compression of warm gaseous streams; details of intake or interstage cooling of main feed air
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J3/00—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification
    • F25J3/02—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream
    • F25J3/04—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream for air
    • F25J3/04006—Providing pressurised feed air or process streams within or from the air fractionation unit
    • F25J3/04048—Providing pressurised feed air or process streams within or from the air fractionation unit by compression of cold gaseous streams, e.g. intermediate or oxygen enriched (waste) streams
    • F25J3/04054—Providing pressurised feed air or process streams within or from the air fractionation unit by compression of cold gaseous streams, e.g. intermediate or oxygen enriched (waste) streams of air
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J3/00—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification
    • F25J3/02—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream
    • F25J3/04—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream for air
    • F25J3/04006—Providing pressurised feed air or process streams within or from the air fractionation unit
    • F25J3/04078—Providing pressurised feed air or process streams within or from the air fractionation unit providing pressurized products by liquid compression and vaporisation with cold recovery, i.e. so-called internal compression
    • F25J3/04084—Providing pressurised feed air or process streams within or from the air fractionation unit providing pressurized products by liquid compression and vaporisation with cold recovery, i.e. so-called internal compression of nitrogen
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J3/00—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification
    • F25J3/02—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream
    • F25J3/04—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream for air
    • F25J3/04006—Providing pressurised feed air or process streams within or from the air fractionation unit
    • F25J3/04078—Providing pressurised feed air or process streams within or from the air fractionation unit providing pressurized products by liquid compression and vaporisation with cold recovery, i.e. so-called internal compression
    • F25J3/0409—Providing pressurised feed air or process streams within or from the air fractionation unit providing pressurized products by liquid compression and vaporisation with cold recovery, i.e. so-called internal compression of oxygen
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J3/00—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification
    • F25J3/02—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream
    • F25J3/04—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream for air
    • F25J3/04006—Providing pressurised feed air or process streams within or from the air fractionation unit
    • F25J3/04078—Providing pressurised feed air or process streams within or from the air fractionation unit providing pressurized products by liquid compression and vaporisation with cold recovery, i.e. so-called internal compression
    • F25J3/04096—Providing pressurised feed air or process streams within or from the air fractionation unit providing pressurized products by liquid compression and vaporisation with cold recovery, i.e. so-called internal compression of argon or argon enriched stream
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J3/00—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification
    • F25J3/02—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream
    • F25J3/04—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream for air
    • F25J3/04151—Purification and (pre-)cooling of the feed air; recuperative heat-exchange with product streams
    • F25J3/04163—Hot end purification of the feed air
    • F25J3/04169—Hot end purification of the feed air by adsorption of the impurities
    • F25J3/04175—Hot end purification of the feed air by adsorption of the impurities at a pressure of substantially more than the highest pressure column
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J3/00—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification
    • F25J3/02—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream
    • F25J3/04—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream for air
    • F25J3/04248—Generation of cold for compensating heat leaks or liquid production, e.g. by Joule-Thompson expansion
    • F25J3/04284—Generation of cold for compensating heat leaks or liquid production, e.g. by Joule-Thompson expansion using internal refrigeration by open-loop gas work expansion, e.g. of intermediate or oxygen enriched (waste-)streams
    • F25J3/0429—Generation of cold for compensating heat leaks or liquid production, e.g. by Joule-Thompson expansion using internal refrigeration by open-loop gas work expansion, e.g. of intermediate or oxygen enriched (waste-)streams of feed air, e.g. used as waste or product air or expanded into an auxiliary column
    • F25J3/04296—Claude expansion, i.e. expanded into the main or high pressure column
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J3/00—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification
    • F25J3/02—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream
    • F25J3/04—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream for air
    • F25J3/04248—Generation of cold for compensating heat leaks or liquid production, e.g. by Joule-Thompson expansion
    • F25J3/04333—Generation of cold for compensating heat leaks or liquid production, e.g. by Joule-Thompson expansion using quasi-closed loop internal vapor compression refrigeration cycles, e.g. of intermediate or oxygen enriched (waste-)streams
    • F25J3/04339—Generation of cold for compensating heat leaks or liquid production, e.g. by Joule-Thompson expansion using quasi-closed loop internal vapor compression refrigeration cycles, e.g. of intermediate or oxygen enriched (waste-)streams of air
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J3/00—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification
    • F25J3/02—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream
    • F25J3/04—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream for air
    • F25J3/04248—Generation of cold for compensating heat leaks or liquid production, e.g. by Joule-Thompson expansion
    • F25J3/04375—Details relating to the work expansion, e.g. process parameter etc.
    • F25J3/04393—Details relating to the work expansion, e.g. process parameter etc. using multiple or multistage gas work expansion
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J3/00—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification
    • F25J3/02—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream
    • F25J3/04—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream for air
    • F25J3/04406—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream for air using a dual pressure main column system
    • F25J3/04412—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream for air using a dual pressure main column system in a classical double column flowsheet, i.e. with thermal coupling by a main reboiler-condenser in the bottom of low pressure respectively top of high pressure column
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J3/00—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification
    • F25J3/02—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream
    • F25J3/04—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream for air
    • F25J3/04642—Recovering noble gases from air
    • F25J3/04648—Recovering noble gases from air argon
    • F25J3/04654—Producing crude argon in a crude argon column
    • F25J3/04666—Producing crude argon in a crude argon column as a parallel working rectification column of the low pressure column in a dual pressure main column system
    • F25J3/04672—Producing crude argon in a crude argon column as a parallel working rectification column of the low pressure column in a dual pressure main column system having a top condenser
    • F25J3/04678—Producing crude argon in a crude argon column as a parallel working rectification column of the low pressure column in a dual pressure main column system having a top condenser cooled by oxygen enriched liquid from high pressure column bottoms
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J3/00—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification
    • F25J3/02—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream
    • F25J3/04—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream for air
    • F25J3/04642—Recovering noble gases from air
    • F25J3/04648—Recovering noble gases from air argon
    • F25J3/04654—Producing crude argon in a crude argon column
    • F25J3/04666—Producing crude argon in a crude argon column as a parallel working rectification column of the low pressure column in a dual pressure main column system
    • F25J3/04672—Producing crude argon in a crude argon column as a parallel working rectification column of the low pressure column in a dual pressure main column system having a top condenser
    • F25J3/04703—Producing crude argon in a crude argon column as a parallel working rectification column of the low pressure column in a dual pressure main column system having a top condenser being arranged in more than one vessel
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J3/00—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification
    • F25J3/02—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream
    • F25J3/04—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream for air
    • F25J3/04642—Recovering noble gases from air
    • F25J3/04648—Recovering noble gases from air argon
    • F25J3/04721—Producing pure argon, e.g. recovered from a crude argon column
    • F25J3/04727—Producing pure argon, e.g. recovered from a crude argon column using an auxiliary pure argon column for nitrogen rejection
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J2235/00—Processes or apparatus involving steps for increasing the pressure or for conveying of liquid process streams
    • F25J2235/58—Processes or apparatus involving steps for increasing the pressure or for conveying of liquid process streams the fluid being argon or crude argon
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J2240/00—Processes or apparatus involving steps for expanding of process streams
    • F25J2240/02—Expansion of a process fluid in a work-extracting turbine (i.e. isentropic expansion), e.g. of the feed stream
    • F25J2240/04—Multiple expansion turbines in parallel
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J2245/00—Processes or apparatus involving steps for recycling of process streams
    • F25J2245/50—Processes or apparatus involving steps for recycling of process streams the recycled stream being oxygen
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J2270/00—Refrigeration techniques used
    • F25J2270/02—Internal refrigeration with liquid vaporising loop

Definitions

  • the invention relates to a method according to the preamble of patent claim 1.
  • the distillation column system of the invention may be designed as a two-column system (for example as a classic Linde double column system) or as a three-column or multi-column system. It may in addition to the columns for nitrogen-oxygen separation, further devices for obtaining high purity products and / or other air components, in particular of noble gases, for example, an argon production and / or a krypton-xenon recovery
  • a liquid pressurized oxygen product stream is vaporized against a heat carrier and finally recovered as a gaseous pressure product.
  • This method is also called internal compression. It serves for the production of pressure oxygen. In the case of a supercritical pressure, no phase transition takes place in the true sense, the product stream is then "pseudo-evaporated".
  • a high-pressure heat carrier is liquefied (or pseudo-liquefied when it is under supercritical pressure).
  • the heat transfer medium is often formed by part of the air, in the present case by the "second partial flow" of the compressed feed air.
  • EP 1139046 A1 EP 1146301 A1 .
  • DE 10213212 A1 DE 10213211 A1 .
  • EP 1357342 A1 or DE 10238282 A1 DE 10302389 A1 .
  • DE 10332863 A1 EP 1544559 A1 .
  • EP 1666824 A1 EP 1672301 A1 .
  • DE 102005028012 A1 .
  • WO 2007033838 A1 WO 2007104449 A1 .
  • EP 1845324 A1 is
  • the "main heat exchanger system” serves to cool feed air in indirect heat exchange with return streams from the distillation column system. It may be formed of one or more parallel and / or serially connected heat exchanger sections, for example one or more plate heat exchanger blocks.
  • the method of the invention belongs to the class of high pressure processes in which the total air in a main air compressor is compressed to well above high pressure column pressure.
  • the system works with a single externally driven machine, namely this main air compressor.
  • the configuration in which the compressed cooled and purified air is split into two streams - turbine stream ("second substream") and inductor stream ("first substream”).
  • the turbine stream is cooled in the heat exchanger and then relaxed in a turbine, for example, to the pressure of the high pressure column and passed into this.
  • the throttle flow is in a booster stage (“compressor"), driven by the turbine, recompressed, passed through the heat exchanger and thereby cooled and is then passed into the rectification section.
  • the invention is therefore based on the object to provide a method of the type mentioned above and a corresponding device, which are economically particularly favorable, especially at a relatively small inductor current ("first partial flow").
  • a recirculation flow which is formed by a part of the first partial flow of air (the throttle flow) guided through the after-compressor, flows in a circle through the after-compressor. This increases the amount of air to be compressed in the booster.
  • the recycle stream is preferably withdrawn at the exit from the main heat exchanger (at the cold end), depressurized in a throttle valve to a pressure slightly higher than the pressure before entry into the reboiler.
  • the relaxed recycle stream is passed through the main heat exchanger and mixed again with the first part stream before entering the reboiler.
  • This recirculation of the inductor current causes the amount of gas to be compressed in the booster stage (the booster) to increase, the pressure ratio being smaller and the booster and turbine volumes match better.
  • a conventional buildable and particularly efficient booster turbine can be used.
  • the heating of the return flow can be carried out up to the warm end of the main heat exchanger or up to an intermediate temperature.
  • the introduction of the recirculation stream into the first partial stream upstream of the postcompressor can in principle also be effected by introducing the recycle stream into the total air stream before it is divided; the "return to the first partial flow" is then performed upstream of the branch of the first partial flow from the second partial flow.
  • the recycle stream is introduced into the first substream immediately before the postcompressor.
  • the system has only a single externally driven compressor, the main air compressor, and only a single expansion machine (turbine). Despite this comparatively simple structure, it is very energy-efficient by the process of the invention.
  • the total air is compressed in the invention to a first air pressure, which is for example 10 to 30 bar and preferably between 10 and 20 bar.
  • the invention also relates to a device according to claim 4.
  • the device according to the invention can be supplemented by device features which correspond to the features of the dependent method claims.
  • Atmospheric air 1 is sucked in via a filter from a main air compressor 3 and compressed there to a first air pressure of about 18 bar.
  • the main air compressor preferably has several stages with intermediate cooling.
  • the compressed total air is then cooled in a pre-cooler 4 and cleaned in a cleaning device 5.
  • the purified feed air 6 is divided under the first air pressure into a first partial flow 7 and a second partial flow 8.
  • approximately 45% of the total air 6 forms the first partial flow 7, the remainder the second partial flow 8.
  • the first partial flow 7 is fed via line 9 to a secondary compressor 10 with aftercooler 11 and further compressed there to a second air pressure of about 28 bar.
  • the booster 10 is formed in one stage.
  • the post-compressed first partial flow 12 is fed to a main heat exchanger 13 at the warm end, where it is cooled and liquefied and finally withdrawn again at the cold end via line 14.
  • Most of the liquefied first substream is introduced via line 15 and throttle valve 16 in the distillation column system for nitrogen-oxygen separation, which has a high pressure column 17, a low pressure column 18 and a main condenser 19, which is designed as a condenser-evaporator.
  • the operating pressures are 5 to 6 bar in the high-pressure column and 1.2 to 1.6 bar in the low-pressure column.
  • a portion of the introduced into the high-pressure column 17 liquid air is removed again via line 20, cooled in a supercooling countercurrent 21 and fed via throttle valve 22 in the low-pressure column 18.
  • the second partial stream 8 of the feed air is cooled in the main heat exchanger 13 only to an intermediate temperature.
  • the cooled second partial flow 23 is introduced into a relaxation machine, which is formed here by a turbine 24.
  • the second air stream is working expanded relaxed to something about high pressure column pressure.
  • the expanded second partial stream 25 is fed in completely gaseous or substantially completely gaseous state of the high-pressure column immediately above the sump.
  • the expansion machine 24 is directly mechanically coupled to the booster compressor 10, in particular sit after-compressor and turbine on a common shaft.
  • Argon portion 30 comprises a split crude argon column and a pure argon column, is fed by an argon transition fraction 31 and provides a liquid pure argon (LAR) product 32. Otherwise, it operates according to known principles.
  • the top nitrogen 33 of the high-pressure column 17 is condensed at least to a part 34 in the main condenser 19.
  • the liquid nitrogen obtained is fed to a first part 36 as reflux to the high-pressure column 17.
  • a second part 37 is cooled in the subcooling countercurrent 21 and fed via throttle valve 38 into the top of the low pressure column 18. At least a part of it is used as a liquid reflux in the low-pressure column 18.
  • an oxygen product stream is produced 39 withdrawn liquid and brought in liquid state to an elevated pressure of about 30 bar.
  • the high-pressure oxygen 41 is vaporized in the main heat exchanger 13 and warmed to approximately ambient temperature. Via line 42, it is finally recovered as an internally compressed pressure oxygen product (GOX-IC).
  • a portion 60 of the warm residual gas 54 can be used as a regeneration gas (regas gas) in the cleaning device 5.
  • liquid argon 32 can be internally compressed from the argon part 30 in a pump 55 and recovered after (pseudo) evaporation via line 56 as gaseous pressure product (GAR-IC).
  • GAR-IC gaseous pressure product
  • a recycle stream 57 is branched off from the liquefied first substream 14, here downstream of the cold end of the main heat exchanger 12.
  • the recycle stream 57 when depressurized in a throttle valve 58 to a pressure of slightly more than 18 bar, returns to the cold end of the main heat exchanger fed and warmed there to an intermediate temperature of 260 K.
  • the warmed recycle stream 59 is finally fed to the first part stream 7 upstream of the post-compressor 10.
  • the booster 10 in FIG. 1 is operated in warm conditions, ie with an inlet temperature no more than 20 K below ambient temperature.
  • FIG. 2 differs from FIG. 1 in that the after-compressor 110 is operated as a cold compressor, that is to say with an inlet temperature which is more than 20 K below the ambient temperature, in the example at 210 ° K.
  • the recirculation flow 159 also becomes at a lower intermediate temperature of approximately 205 K taken from the main heat exchanger 13 and only downstream of the cooling of the first partial flow 107 combined with this.
  • the division into first partial flow 107 and second partial flow 123 takes place here within the main heat exchanger 13.
  • the recompressed first substream 112 is fed to the main heat exchanger 13 at an intermediate temperature.
  • the expansion machine 124 is not only mechanically coupled to the cold booster 110. Rather, there is an additional oil brake 161 on the common shaft (alternative to the oil brake, a generator could also be used).
  • a second turbine 224 is used instead of the oil brake, which is coupled to a generator 261.
  • a dissipative brake for example an oil brake.
  • the first turbine 124 is mechanically connected only to the cold secondary compressor 110.
  • the two turbines 124, 224 each have the same pressures and temperatures at the inlet and outlet.
  • FIG. 4 differs from the previous embodiments in that the recycle stream 357 is branched off from the first part stream already before the cold end of the main heat exchanger, ie at something at a higher temperature, which may not be higher than dew point, in the example under 130 K. Die During the expansion in the throttle valve 358 generated cold can thus contribute to the cooling of feed air in the main heat exchanger 13.
  • the pre-cooling 4 and the cleaning 5 can be performed at a lower pressure than the first air pressure, as in FIG. 5 is shown.
  • the system must then in addition to the main air compressor 403 another externally driven air compressor 463 having the total purified air 462 from this lower air pressure of, for example, 18 bar to the first air pressure recompressed.
  • the air compressor 463 has an aftercooler, which is not shown in the drawing, and may be of one or more stages and may have an intermediate cooling.

Landscapes

  • Engineering & Computer Science (AREA)
  • Physics & Mathematics (AREA)
  • Mechanical Engineering (AREA)
  • Thermal Sciences (AREA)
  • General Engineering & Computer Science (AREA)
  • Health & Medical Sciences (AREA)
  • Emergency Medicine (AREA)
  • Separation By Low-Temperature Treatments (AREA)
EP12007828.2A 2011-12-01 2012-11-20 Procédé et dispositif destinés à la production d'oxygène sous pression par décomposition à basse température de l'air Not-in-force EP2600090B1 (fr)

Priority Applications (1)

Application Number Priority Date Filing Date Title
EP12007828.2A EP2600090B1 (fr) 2011-12-01 2012-11-20 Procédé et dispositif destinés à la production d'oxygène sous pression par décomposition à basse température de l'air

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
EP11009537 2011-12-01
EP12007828.2A EP2600090B1 (fr) 2011-12-01 2012-11-20 Procédé et dispositif destinés à la production d'oxygène sous pression par décomposition à basse température de l'air

Publications (2)

Publication Number Publication Date
EP2600090A1 true EP2600090A1 (fr) 2013-06-05
EP2600090B1 EP2600090B1 (fr) 2014-07-16

Family

ID=47191487

Family Applications (1)

Application Number Title Priority Date Filing Date
EP12007828.2A Not-in-force EP2600090B1 (fr) 2011-12-01 2012-11-20 Procédé et dispositif destinés à la production d'oxygène sous pression par décomposition à basse température de l'air

Country Status (2)

Country Link
US (1) US20130139548A1 (fr)
EP (1) EP2600090B1 (fr)

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2016005031A1 (fr) * 2014-07-05 2016-01-14 Linde Aktiengesellschaft Procédé et dispositif de fractionnement de l'air à basse température à consommation d'énergie variable
WO2018215716A1 (fr) * 2017-05-24 2018-11-29 L'air Liquide, Societe Anonyme Pour L'etude Et L'exploitation Des Procedes Georges Claude Procédé et appareil pour la séparation de l'air par distillation cryogénique
US10794630B2 (en) 2017-08-03 2020-10-06 L'air Liquide Societe Anonyme Pour L'etude Et L'exploitation Des Procedes Georges Claude Method and device for separating air by cryogenic distillation

Citations (73)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE830805C (de) 1944-11-19 1952-02-07 Linde Eismasch Ag Verfahren zur Gas-, insbesondere zur Luftzerlegung
DE901542C (de) 1952-01-10 1954-01-11 Linde Eismasch Ag Verfahren zur Zerlegung von Luft durch Verfluessigung und Rektifikation
US2712738A (en) 1952-01-10 1955-07-12 Linde S Eismaschinen Ag Method for fractionating air by liquefaction and rectification
DE952908C (de) 1953-10-11 1956-11-22 Linde Eismasch Ag Verfahren zur Zerlegung von Luft
US2784572A (en) 1953-01-02 1957-03-12 Linde S Eismaschinen Ag Method for fractionating air by liquefaction and rectification
DE1103363B (de) 1958-09-24 1961-03-30 Linde Eismasch Ag Verfahren und Vorrichtung zur Erzeugung eines ausgeglichenen Kaeltehaushaltes bei der Gewinnung von unter hoeherem Druck stehenden Gasgemischen und/oder Gasgemisch-komponenten durch Rektifikation
DE1112997B (de) 1960-08-13 1961-08-24 Linde Eismasch Ag Verfahren und Einrichtung zur Gaszerlegung durch Rektifikation bei tiefer Temperatur
DE1117616B (de) 1960-10-14 1961-11-23 Linde Eismasch Ag Verfahren und Einrichtung zum Gewinnen besonders reiner Zerlegungsprodukte in Tieftemperaturgaszerlegungsanlagen
DE1124529B (de) 1957-07-04 1962-03-01 Linde Eismasch Ag Verfahren und Einrichtung zur Durchfuehrung von Waermeaustauschvorgaengen in einer mit vorgeschalteten Regeneratoren arbeitenden Gaszerlegungsanlage
DE1187248B (de) 1963-03-29 1965-02-18 Linde Eismasch Ag Verfahren und Einrichtung zur Gewinnung von Sauerstoffgas mit 70 bis 98% O-Gehalt
DE1199293B (de) 1963-03-29 1965-08-26 Linde Eismasch Ag Verfahren und Vorrichtung zur Luftzerlegung in einem Einsaeulenrektifikator
US3216206A (en) 1961-11-29 1965-11-09 Linde Eismasch Ag Low temperature distillation of normally gaseous substances
US3222878A (en) 1962-12-21 1965-12-14 Linde Eismasch Ag Method and apparatus for fractionation of air
DE1235347B (de) 1964-05-13 1967-03-02 Linde Ag Verfahren und Vorrichtung zum Betrieb von umschaltbaren Waermeaustauschern bei der Tieftemperaturgaszerlegung
DE1258882B (de) 1963-06-19 1968-01-18 Linde Ag Verfahren und Anlage zur Luftzerlegung durch Rektifikation unter Verwendung eines Hochdruckgas-Kaeltekreislaufes zur Druckverdampfung fluessigen Sauerstoffs
DE1263037B (de) 1965-05-19 1968-03-14 Linde Ag Verfahren zur Zerlegung von Luft in einer Rektifikationssaeule und damit gekoppelterZerlegung eines Wasserstoff enthaltenden Gasgemisches
US3416323A (en) 1966-01-13 1968-12-17 Linde Ag Low temperature production of highly compressed gaseous and/or liquid oxygen
DE1501723A1 (de) 1966-01-13 1969-06-26 Linde Ag Verfahren und Vorrichtung zur Erzeugung gasfoermigen Hochdrucksauerstoffs bei der Tieftemperaturrektifikation von Luft
DE2535132A1 (de) 1975-08-06 1977-02-10 Linde Ag Verfahren und vorrichtung zur herstellung von sauerstoff durch zweistufige tieftemperaturrektifikation von luft
DE2646690A1 (de) 1976-10-15 1978-04-20 Linde Ag Verfahren und vorrichtung zur herstellung einer mischung von sauerstoff und wasserdampf unter druck
US4555256A (en) 1982-05-03 1985-11-26 Linde Aktiengesellschaft Process and device for the production of gaseous oxygen at elevated pressure
US5036672A (en) 1989-02-23 1991-08-06 Linde Aktiengesellschaft Process and apparatus for air fractionation by rectification
EP0504029A1 (fr) * 1991-03-11 1992-09-16 L'air Liquide, Societe Anonyme Pour L'etude Et L'exploitation Des Procedes Georges Claude Procédé de production d'oxygène gazeux sous pression
US5263328A (en) 1991-03-26 1993-11-23 Linde Aktiengesellschaft Process for low-temperature air fractionation
US5644934A (en) 1994-12-05 1997-07-08 Linde Aktiengesellchaft Process and device for low-temperature separation of air
US5845517A (en) 1995-08-11 1998-12-08 Linde Aktiengesellschaft Process and device for air separation by low-temperature rectification
DE19803437A1 (de) 1998-01-29 1999-03-18 Linde Ag Verfahren und Vorrichtung zur Gewinnung eines Druckprodukts durch Tieftemperaturzerlegung von Luft
US5953937A (en) 1995-07-21 1999-09-21 Linde Aktiengesellschaft Process and apparatus for the variable production of a gaseous pressurized product
EP0955509A1 (fr) 1998-04-30 1999-11-10 Linde Aktiengesellschaft Procédé et appareil pour la production d'oxygène à haute pureté
US6038885A (en) 1997-07-30 2000-03-21 Linde Aktiengesellschaft Air separation process
DE19909744A1 (de) 1999-03-05 2000-05-04 Linde Ag Zweisäulensystem zur Tieftemperaturzerlegung von Luft
EP1031804A1 (fr) 1999-02-26 2000-08-30 Linde Technische Gase GmbH Procédé de séparation des gaz de l'air avec recyclage d'azote
DE19954593A1 (de) 1999-11-12 2000-09-28 Linde Ag Verfahren und Vorrichtung zur Tieftemperaturzerlegung von Luft
DE10013073A1 (de) 2000-03-17 2000-10-19 Linde Ag Verfahren und Vorrichtung zur Tieftemperaturzerlegung von Luft
EP1067345A1 (fr) 1999-07-05 2001-01-10 Linde Aktiengesellschaft Procédé et dispositif pour la séparation cryogénique des constituants de l'air
EP1074805A1 (fr) 1999-08-05 2001-02-07 Linde Aktiengesellschaft Procédé et dispositif pour la production d'oxygène sous pression
US6185960B1 (en) 1998-04-08 2001-02-13 Linde Aktiengesellschaft Process and device for the production of a pressurized gaseous product by low-temperature separation of air
EP1134525A1 (fr) 2000-03-17 2001-09-19 Linde Aktiengesellschaft Procédé de production d'azote liquide et gazeux avec une quantité variable de liquide
EP1139046A1 (fr) 2000-03-29 2001-10-04 Linde Aktiengesellschaft Procédé et installation de production d'un produit sous haute pression par séparation cryogénique de l'air
EP1146301A1 (fr) 2000-04-12 2001-10-17 Linde Gas Aktiengesellschaft Procédé et dispositif de production d'azote à haute pression par séparation d'air
EP1150082A1 (fr) 2000-04-28 2001-10-31 Linde Aktiengesellschaft Procédé et dispositif d'échange de chaleur
US6314755B1 (en) 1999-02-26 2001-11-13 Linde Aktiengesellschaft Double column system for the low-temperature fractionation of air
EP1213552A1 (fr) 2000-12-06 2002-06-12 Linde Aktiengesellschaft Système à machines pour la détente de deux courants de procédé
DE10115258A1 (de) 2001-03-28 2002-07-18 Linde Ag Maschinensystem und dessen Anwendung
DE10213212A1 (de) 2002-03-25 2002-10-17 Linde Ag Verfahren und Vorrichtung zur Erzeugung zweier Druckprodukte durch Tieftemperatur-Luftzerlegung
DE10213211A1 (de) 2002-03-25 2002-10-17 Linde Ag Verfahren zur Tieftemperatur-Luftzerlegung mit abgeschottetem Kreislaufsystem
EP1284404A1 (fr) 2001-08-13 2003-02-19 Linde Aktiengesellschaft Procédé et dispositif pour la production d'un produit sous pression par séparation cryogénique de l'air
EP1308680A1 (fr) 2001-10-31 2003-05-07 Linde AG Procédé et dispositif de production de krypton et/ou xénon par distillation cryogénique de l'air
DE10238282A1 (de) 2002-08-21 2003-05-28 Linde Ag Verfahren zur Tieftemperatur-Zerlegung von Luft
DE10302389A1 (de) 2003-01-22 2003-06-18 Linde Ag Verfahren und Vorrichtung zur Tieftemperaturzerlegung von Luft
EP1357342A1 (fr) 2002-04-17 2003-10-29 Linde Aktiengesellschaft Système de séparation d'air cryogénique à trois colonnes avec production d'argon
DE10332863A1 (de) 2003-07-18 2004-02-26 Linde Ag Verfahren und Vorrichtung zur Gewinnung von Krypton und/oder Xenon durch Tieftemperaturzerlegung von Luft
DE10334560A1 (de) 2003-05-28 2004-12-16 Linde Ag Verfahren und Vorrichtung zur Gewinnung von Krypton und/oder Xenon durch Tieftemperaturzerlegung von Luft
DE10334559A1 (de) 2003-05-28 2004-12-16 Linde Ag Verfahren und Vorrichtung zur Gewinnung von Krypton und/oder Xenon durch Tieftemperaturzerlegung von Luft
EP1544559A1 (fr) 2003-12-20 2005-06-22 Linde AG Procédé et dispositif pour la séparation cryogénique d'air
EP1585926A1 (fr) 2002-12-19 2005-10-19 Karges-Faulconbridge, Inc. Systeme pour extraction liquide et procedes
DE102005029274A1 (de) 2004-08-17 2006-02-23 Linde Ag Verfahren und Vorrichtung zur Gewinnung eines gasförmigen Druckprodukts durch Tieftemperatur-Zerlegung von Luft
EP1666824A1 (fr) 2004-12-03 2006-06-07 Linde Aktiengesellschaft Procédé et dispositif pour la récupération d'Argon par séparation cryogénique d'air
EP1672301A1 (fr) 2004-12-03 2006-06-21 Linde AG Installation pour la séparation cryogénique d'un mélange gazeux en particulier d'air
DE102005028012A1 (de) 2005-06-16 2006-09-14 Linde Ag Verfahren und Vorrichtung zur Tieftemperaturzerlegung von Luft
DE102006032731A1 (de) 2006-07-14 2007-01-18 Linde Ag Verfahren und Anlage zur Luftzerlegung
WO2007033838A1 (fr) 2005-09-23 2007-03-29 Linde Aktiengesellschaft Procede et dispositif pour analyser la temperature de l'air
DE102007014643A1 (de) 2007-03-27 2007-09-20 Linde Ag Verfahren und Vorrichtung zur Erzeugung von gasförmigem Druckprodukt durch Tieftemperaturzerlegung von Luft
WO2007104449A1 (fr) 2006-03-15 2007-09-20 Linde Aktiengesellschaft Procédé et dispositif de décomposition de l'air à basse température
EP1845324A1 (fr) 2006-04-13 2007-10-17 Linde Aktiengesellschaft Procédé et dispositif de production d'un produit sous haute pression par séparation cryogénique d'air
EP1892490A1 (fr) 2006-08-16 2008-02-27 Linde Aktiengesellschaft Procédé et dispositif de production variable d'un produit comprimé par séparation cryogénique d'un gaz
EP2015013A2 (fr) 2007-07-07 2009-01-14 Linde Aktiengesellschaft Procédé et dispositif de production d'un gaz sous pression par séparation cryogénique d'air
EP2015012A2 (fr) 2007-07-07 2009-01-14 Linde Aktiengesellschaft Procédé pour la séparation cryogénique d'air
EP2026024A1 (fr) 2007-07-30 2009-02-18 Linde Aktiengesellschaft Procédé et dispositif pour la production d'argon par séparation cryogénique d'air
WO2009095188A2 (fr) 2008-01-28 2009-08-06 Linde Aktiengesellschaft Procédé et dispositif de séparation de l'air à basse température
DE102008016355A1 (de) 2008-03-29 2009-10-01 Linde Ag Verfahren und Vorrichtung zur Tieftemperaturzerlegung von Luft
WO2011018207A2 (fr) * 2009-08-11 2011-02-17 Linde Aktiengesellschaft Procédé et dispositif pour générer un produit gazeux sous pression contenant de l'oxygène par fractionnement cryogénique de l'air
EP2299221A2 (fr) * 2009-09-21 2011-03-23 Linde Aktiengesellschaft Procédé et dispositif destinés à la décomposition à basse température d'air

Family Cites Families (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE1815532A1 (de) * 1968-12-18 1970-06-25 Linde Ag Verfahren zum Erzeugen von Kaelte
GB1520103A (en) * 1977-03-19 1978-08-02 Air Prod & Chem Production of liquid oxygen and/or liquid nitrogen
GB9513766D0 (en) * 1995-07-06 1995-09-06 Boc Group Plc Air separation
US5678425A (en) * 1996-06-07 1997-10-21 Air Products And Chemicals, Inc. Method and apparatus for producing liquid products from air in various proportions
US5911388A (en) * 1997-01-15 1999-06-15 Sundstrand Corporation Environmental control system with energy recovery and bleed air assist
US6006545A (en) * 1998-08-14 1999-12-28 L'air Liquide, Societe Anonyme Pour L'etude Et L'exploitation Des Procedes Liquefier process
FR2798075B1 (fr) * 1999-09-03 2001-11-09 Air Liquide Conduite d'un systeme de purification d'air a regeneration thermique
US6694776B1 (en) * 2003-05-14 2004-02-24 Praxair Technology, Inc. Cryogenic air separation system for producing oxygen

Patent Citations (99)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE830805C (de) 1944-11-19 1952-02-07 Linde Eismasch Ag Verfahren zur Gas-, insbesondere zur Luftzerlegung
DE901542C (de) 1952-01-10 1954-01-11 Linde Eismasch Ag Verfahren zur Zerlegung von Luft durch Verfluessigung und Rektifikation
US2712738A (en) 1952-01-10 1955-07-12 Linde S Eismaschinen Ag Method for fractionating air by liquefaction and rectification
US2784572A (en) 1953-01-02 1957-03-12 Linde S Eismaschinen Ag Method for fractionating air by liquefaction and rectification
DE952908C (de) 1953-10-11 1956-11-22 Linde Eismasch Ag Verfahren zur Zerlegung von Luft
DE1124529B (de) 1957-07-04 1962-03-01 Linde Eismasch Ag Verfahren und Einrichtung zur Durchfuehrung von Waermeaustauschvorgaengen in einer mit vorgeschalteten Regeneratoren arbeitenden Gaszerlegungsanlage
US3083544A (en) 1958-09-24 1963-04-02 Linde S Eismaschinen Ag Hollri Rectification of gases
DE1103363B (de) 1958-09-24 1961-03-30 Linde Eismasch Ag Verfahren und Vorrichtung zur Erzeugung eines ausgeglichenen Kaeltehaushaltes bei der Gewinnung von unter hoeherem Druck stehenden Gasgemischen und/oder Gasgemisch-komponenten durch Rektifikation
DE1112997B (de) 1960-08-13 1961-08-24 Linde Eismasch Ag Verfahren und Einrichtung zur Gaszerlegung durch Rektifikation bei tiefer Temperatur
US3214925A (en) 1960-08-13 1965-11-02 Linde Eismasch Ag System for gas separation by rectification at low temperatures
DE1117616B (de) 1960-10-14 1961-11-23 Linde Eismasch Ag Verfahren und Einrichtung zum Gewinnen besonders reiner Zerlegungsprodukte in Tieftemperaturgaszerlegungsanlagen
US3280574A (en) 1960-10-14 1966-10-25 Linde Ag High pressure pure gas for preventing contamination by low pressure raw gas in reversing regenerators
DE1226616B (de) 1961-11-29 1966-10-13 Linde Ag Verfahren und Einrichtung zur Gewinnung von gasfoermigem Drucksauerstoff mit gleichzeitiger Erzeugung fluessiger Zerlegungsprodukte durch Tieftemperatur-Luftzerlegung
US3216206A (en) 1961-11-29 1965-11-09 Linde Eismasch Ag Low temperature distillation of normally gaseous substances
US3222878A (en) 1962-12-21 1965-12-14 Linde Eismasch Ag Method and apparatus for fractionation of air
DE1229561B (de) 1962-12-21 1966-12-01 Linde Ag Verfahren und Vorrichtung zum Zerlegen von Luft durch Verfluessigung und Rektifikation mit Hilfe eines Inertgaskreislaufes
DE1187248B (de) 1963-03-29 1965-02-18 Linde Eismasch Ag Verfahren und Einrichtung zur Gewinnung von Sauerstoffgas mit 70 bis 98% O-Gehalt
DE1199293B (de) 1963-03-29 1965-08-26 Linde Eismasch Ag Verfahren und Vorrichtung zur Luftzerlegung in einem Einsaeulenrektifikator
US3371496A (en) 1963-03-29 1968-03-05 Linde Ag Wash liquid production by heat exchange with low pressure liquid oxygen
US3426543A (en) 1963-06-19 1969-02-11 Linde Ag Combining pure liquid and vapor nitrogen streams from air separation for crude hydrogen gas washing
DE1258882B (de) 1963-06-19 1968-01-18 Linde Ag Verfahren und Anlage zur Luftzerlegung durch Rektifikation unter Verwendung eines Hochdruckgas-Kaeltekreislaufes zur Druckverdampfung fluessigen Sauerstoffs
DE1235347B (de) 1964-05-13 1967-03-02 Linde Ag Verfahren und Vorrichtung zum Betrieb von umschaltbaren Waermeaustauschern bei der Tieftemperaturgaszerlegung
US3401531A (en) 1965-05-19 1968-09-17 Linde Ag Heat exchange of compressed nitrogen and liquid oxygen in ammonia synthesis feed gas production
DE1263037B (de) 1965-05-19 1968-03-14 Linde Ag Verfahren zur Zerlegung von Luft in einer Rektifikationssaeule und damit gekoppelterZerlegung eines Wasserstoff enthaltenden Gasgemisches
US3416323A (en) 1966-01-13 1968-12-17 Linde Ag Low temperature production of highly compressed gaseous and/or liquid oxygen
DE1501723A1 (de) 1966-01-13 1969-06-26 Linde Ag Verfahren und Vorrichtung zur Erzeugung gasfoermigen Hochdrucksauerstoffs bei der Tieftemperaturrektifikation von Luft
DE1501722A1 (de) 1966-01-13 1969-06-26 Linde Ag Verfahren zur Tieftemperatur-Luftzerlegung zur Erzeugung von hochverdichtetem gasfoermigem und/oder fluessigem Sauerstoff
US3500651A (en) 1966-01-13 1970-03-17 Linde Ag Production of high pressure gaseous oxygen by low temperature rectification of air
DE2535132A1 (de) 1975-08-06 1977-02-10 Linde Ag Verfahren und vorrichtung zur herstellung von sauerstoff durch zweistufige tieftemperaturrektifikation von luft
US4279631A (en) 1975-08-06 1981-07-21 Linde Aktiengesellschaft Process and apparatus for the production of oxygen by two-stage low-temperature rectification of air
DE2646690A1 (de) 1976-10-15 1978-04-20 Linde Ag Verfahren und vorrichtung zur herstellung einer mischung von sauerstoff und wasserdampf unter druck
US4555256A (en) 1982-05-03 1985-11-26 Linde Aktiengesellschaft Process and device for the production of gaseous oxygen at elevated pressure
EP0093448B1 (fr) 1982-05-03 1986-10-15 Linde Aktiengesellschaft Procédé et dispositif pour obtenir de l'oxygène gazeux sous pression élevée
US5036672A (en) 1989-02-23 1991-08-06 Linde Aktiengesellschaft Process and apparatus for air fractionation by rectification
EP0384483B1 (fr) 1989-02-23 1992-07-22 Linde Aktiengesellschaft Procédé et dispositif de rectification d'air
EP0504029A1 (fr) * 1991-03-11 1992-09-16 L'air Liquide, Societe Anonyme Pour L'etude Et L'exploitation Des Procedes Georges Claude Procédé de production d'oxygène gazeux sous pression
US5329776A (en) 1991-03-11 1994-07-19 L'air Liquide, Societe Anonyme Pour L'etude Et L'exploitation Des Procedes Georges Claude Process and apparatus for the production of gaseous oxygen under pressure
US5263328A (en) 1991-03-26 1993-11-23 Linde Aktiengesellschaft Process for low-temperature air fractionation
EP0505812B1 (fr) 1991-03-26 1995-10-18 Linde Aktiengesellschaft Procédé de séparation d'air à basse température
US5644934A (en) 1994-12-05 1997-07-08 Linde Aktiengesellchaft Process and device for low-temperature separation of air
EP0716280B1 (fr) 1994-12-05 2001-05-16 Linde Aktiengesellschaft Procédé et dispositif de séparation d'air à basse température
US5953937A (en) 1995-07-21 1999-09-21 Linde Aktiengesellschaft Process and apparatus for the variable production of a gaseous pressurized product
EP0842385B1 (fr) 1995-07-21 2001-04-18 Linde Aktiengesellschaft Procede et dispositif de production variable d'un produit gazeux comprime
US5845517A (en) 1995-08-11 1998-12-08 Linde Aktiengesellschaft Process and device for air separation by low-temperature rectification
EP0758733B1 (fr) 1995-08-11 2000-11-02 Linde Aktiengesellschaft Procédé de séparation d'air par rectification à basse température
US6038885A (en) 1997-07-30 2000-03-21 Linde Aktiengesellschaft Air separation process
EP0895045B1 (fr) 1997-07-30 2002-11-27 Linde Aktiengesellschaft Procédé de séparation d'air
DE19803437A1 (de) 1998-01-29 1999-03-18 Linde Ag Verfahren und Vorrichtung zur Gewinnung eines Druckprodukts durch Tieftemperaturzerlegung von Luft
US6185960B1 (en) 1998-04-08 2001-02-13 Linde Aktiengesellschaft Process and device for the production of a pressurized gaseous product by low-temperature separation of air
EP0949471B1 (fr) 1998-04-08 2002-12-18 Linde AG Unité de séparation de l'air à deux modes de fonctionnement
EP0955509A1 (fr) 1998-04-30 1999-11-10 Linde Aktiengesellschaft Procédé et appareil pour la production d'oxygène à haute pureté
US6196022B1 (en) 1998-04-30 2001-03-06 Linde Aktiengesellschaft Process and device for recovering high-purity oxygen
US6314755B1 (en) 1999-02-26 2001-11-13 Linde Aktiengesellschaft Double column system for the low-temperature fractionation of air
EP1031804A1 (fr) 1999-02-26 2000-08-30 Linde Technische Gase GmbH Procédé de séparation des gaz de l'air avec recyclage d'azote
DE19909744A1 (de) 1999-03-05 2000-05-04 Linde Ag Zweisäulensystem zur Tieftemperaturzerlegung von Luft
EP1067345A1 (fr) 1999-07-05 2001-01-10 Linde Aktiengesellschaft Procédé et dispositif pour la séparation cryogénique des constituants de l'air
US6336345B1 (en) 1999-07-05 2002-01-08 Linde Aktiengesellschaft Process and apparatus for low temperature fractionation of air
EP1074805A1 (fr) 1999-08-05 2001-02-07 Linde Aktiengesellschaft Procédé et dispositif pour la production d'oxygène sous pression
US6332337B1 (en) 1999-08-05 2001-12-25 Linde Aktiengesellschaft Method and apparatus for recovering oxygen at hyperbaric pressure
DE19954593A1 (de) 1999-11-12 2000-09-28 Linde Ag Verfahren und Vorrichtung zur Tieftemperaturzerlegung von Luft
US6477860B2 (en) 2000-03-17 2002-11-12 Linde Aktiengesellschaft Process for obtaining gaseous and liquid nitrogen with a variable proportion of liquid product
DE10013073A1 (de) 2000-03-17 2000-10-19 Linde Ag Verfahren und Vorrichtung zur Tieftemperaturzerlegung von Luft
EP1134525A1 (fr) 2000-03-17 2001-09-19 Linde Aktiengesellschaft Procédé de production d'azote liquide et gazeux avec une quantité variable de liquide
EP1139046A1 (fr) 2000-03-29 2001-10-04 Linde Aktiengesellschaft Procédé et installation de production d'un produit sous haute pression par séparation cryogénique de l'air
EP1146301A1 (fr) 2000-04-12 2001-10-17 Linde Gas Aktiengesellschaft Procédé et dispositif de production d'azote à haute pression par séparation d'air
EP1150082A1 (fr) 2000-04-28 2001-10-31 Linde Aktiengesellschaft Procédé et dispositif d'échange de chaleur
EP1213552A1 (fr) 2000-12-06 2002-06-12 Linde Aktiengesellschaft Système à machines pour la détente de deux courants de procédé
DE10115258A1 (de) 2001-03-28 2002-07-18 Linde Ag Maschinensystem und dessen Anwendung
EP1284404A1 (fr) 2001-08-13 2003-02-19 Linde Aktiengesellschaft Procédé et dispositif pour la production d'un produit sous pression par séparation cryogénique de l'air
US20030051504A1 (en) 2001-08-13 2003-03-20 Linde Aktiengesellschaft Process and device for obtaining a compressed product by low temperature separation of air
EP1308680A1 (fr) 2001-10-31 2003-05-07 Linde AG Procédé et dispositif de production de krypton et/ou xénon par distillation cryogénique de l'air
US6612129B2 (en) 2001-10-31 2003-09-02 Linde Aktiengesellschaft Process and apparatus for producing krypton and/or xenon by low-temperature fractionation of air
DE10213211A1 (de) 2002-03-25 2002-10-17 Linde Ag Verfahren zur Tieftemperatur-Luftzerlegung mit abgeschottetem Kreislaufsystem
DE10213212A1 (de) 2002-03-25 2002-10-17 Linde Ag Verfahren und Vorrichtung zur Erzeugung zweier Druckprodukte durch Tieftemperatur-Luftzerlegung
EP1357342A1 (fr) 2002-04-17 2003-10-29 Linde Aktiengesellschaft Système de séparation d'air cryogénique à trois colonnes avec production d'argon
DE10238282A1 (de) 2002-08-21 2003-05-28 Linde Ag Verfahren zur Tieftemperatur-Zerlegung von Luft
EP1585926A1 (fr) 2002-12-19 2005-10-19 Karges-Faulconbridge, Inc. Systeme pour extraction liquide et procedes
DE10302389A1 (de) 2003-01-22 2003-06-18 Linde Ag Verfahren und Vorrichtung zur Tieftemperaturzerlegung von Luft
DE10334560A1 (de) 2003-05-28 2004-12-16 Linde Ag Verfahren und Vorrichtung zur Gewinnung von Krypton und/oder Xenon durch Tieftemperaturzerlegung von Luft
DE10334559A1 (de) 2003-05-28 2004-12-16 Linde Ag Verfahren und Vorrichtung zur Gewinnung von Krypton und/oder Xenon durch Tieftemperaturzerlegung von Luft
DE10332863A1 (de) 2003-07-18 2004-02-26 Linde Ag Verfahren und Vorrichtung zur Gewinnung von Krypton und/oder Xenon durch Tieftemperaturzerlegung von Luft
EP1544559A1 (fr) 2003-12-20 2005-06-22 Linde AG Procédé et dispositif pour la séparation cryogénique d'air
DE102005029274A1 (de) 2004-08-17 2006-02-23 Linde Ag Verfahren und Vorrichtung zur Gewinnung eines gasförmigen Druckprodukts durch Tieftemperatur-Zerlegung von Luft
EP1666824A1 (fr) 2004-12-03 2006-06-07 Linde Aktiengesellschaft Procédé et dispositif pour la récupération d'Argon par séparation cryogénique d'air
EP1672301A1 (fr) 2004-12-03 2006-06-21 Linde AG Installation pour la séparation cryogénique d'un mélange gazeux en particulier d'air
DE102005028012A1 (de) 2005-06-16 2006-09-14 Linde Ag Verfahren und Vorrichtung zur Tieftemperaturzerlegung von Luft
WO2007033838A1 (fr) 2005-09-23 2007-03-29 Linde Aktiengesellschaft Procede et dispositif pour analyser la temperature de l'air
WO2007104449A1 (fr) 2006-03-15 2007-09-20 Linde Aktiengesellschaft Procédé et dispositif de décomposition de l'air à basse température
EP1845324A1 (fr) 2006-04-13 2007-10-17 Linde Aktiengesellschaft Procédé et dispositif de production d'un produit sous haute pression par séparation cryogénique d'air
DE102006032731A1 (de) 2006-07-14 2007-01-18 Linde Ag Verfahren und Anlage zur Luftzerlegung
EP1892490A1 (fr) 2006-08-16 2008-02-27 Linde Aktiengesellschaft Procédé et dispositif de production variable d'un produit comprimé par séparation cryogénique d'un gaz
DE102007014643A1 (de) 2007-03-27 2007-09-20 Linde Ag Verfahren und Vorrichtung zur Erzeugung von gasförmigem Druckprodukt durch Tieftemperaturzerlegung von Luft
EP2015013A2 (fr) 2007-07-07 2009-01-14 Linde Aktiengesellschaft Procédé et dispositif de production d'un gaz sous pression par séparation cryogénique d'air
EP2015012A2 (fr) 2007-07-07 2009-01-14 Linde Aktiengesellschaft Procédé pour la séparation cryogénique d'air
EP2026024A1 (fr) 2007-07-30 2009-02-18 Linde Aktiengesellschaft Procédé et dispositif pour la production d'argon par séparation cryogénique d'air
WO2009095188A2 (fr) 2008-01-28 2009-08-06 Linde Aktiengesellschaft Procédé et dispositif de séparation de l'air à basse température
DE102008016355A1 (de) 2008-03-29 2009-10-01 Linde Ag Verfahren und Vorrichtung zur Tieftemperaturzerlegung von Luft
WO2011018207A2 (fr) * 2009-08-11 2011-02-17 Linde Aktiengesellschaft Procédé et dispositif pour générer un produit gazeux sous pression contenant de l'oxygène par fractionnement cryogénique de l'air
EP2299221A2 (fr) * 2009-09-21 2011-03-23 Linde Aktiengesellschaft Procédé et dispositif destinés à la décomposition à basse température d'air

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
HAUSEN/LINDE: "Tieftemperaturtechnik, 2. Auflage", 1985, pages: 281 - 337

Cited By (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2016005031A1 (fr) * 2014-07-05 2016-01-14 Linde Aktiengesellschaft Procédé et dispositif de fractionnement de l'air à basse température à consommation d'énergie variable
CN106489059A (zh) * 2014-07-05 2017-03-08 林德股份公司 以可变能耗低温分离空气的方法和设备
CN106662394A (zh) * 2014-07-05 2017-05-10 林德股份公司 以可变能耗低温分离空气的方法和设备
CN106489059B (zh) * 2014-07-05 2019-11-05 林德股份公司 以可变能耗低温分离空气的方法和设备
CN106662394B (zh) * 2014-07-05 2019-11-05 林德股份公司 以可变能耗低温分离空气的方法和设备
WO2018215716A1 (fr) * 2017-05-24 2018-11-29 L'air Liquide, Societe Anonyme Pour L'etude Et L'exploitation Des Procedes Georges Claude Procédé et appareil pour la séparation de l'air par distillation cryogénique
RU2761562C2 (ru) * 2017-05-24 2021-12-09 Л'Эр Ликид, Сосьете Аноним Пур Л'Этюд Э Л'Эксплуатасьон Де Проседе Жорж Клод Способ и устройство для разделения воздуха криогенной дистилляцией
US12025372B2 (en) 2017-05-24 2024-07-02 L'air Liquide, Societe Anonyme Pour L'etude Et L'exploitation Des Procedes Georges Claude Method and apparatus for air separation by cryogenic distillation
US10794630B2 (en) 2017-08-03 2020-10-06 L'air Liquide Societe Anonyme Pour L'etude Et L'exploitation Des Procedes Georges Claude Method and device for separating air by cryogenic distillation
US10866024B2 (en) 2017-08-03 2020-12-15 L'air Liquide, Societe Anonyme Pour L'etude Et L'exploitation Des Procedes Georges Claude Device and method for separating air by cryogenic distillation

Also Published As

Publication number Publication date
EP2600090B1 (fr) 2014-07-16
US20130139548A1 (en) 2013-06-06

Similar Documents

Publication Publication Date Title
EP2235460B1 (fr) Procédé et installation pour la séparation cryogénique d'air
EP3164654B1 (fr) Procédé et dispositif de fractionnement de l'air à basse température à consommation d'énergie variable
EP2015012A2 (fr) Procédé pour la séparation cryogénique d'air
EP1357342B1 (fr) Système de séparation d'air cryogénique à trois colonnes avec production d'argon
EP2015013A2 (fr) Procédé et dispositif de production d'un gaz sous pression par séparation cryogénique d'air
WO2007104449A1 (fr) Procédé et dispositif de décomposition de l'air à basse température
DE102010052545A1 (de) Verfahren und Vorrichtung zur Gewinnung eines gasförmigen Druckprodukts durch Tieftemperaturzerlegung von Luft
DE102007014643A1 (de) Verfahren und Vorrichtung zur Erzeugung von gasförmigem Druckprodukt durch Tieftemperaturzerlegung von Luft
DE102010052544A1 (de) Verfahren zur Gewinnung eines gasförmigen Druckprodukts durch Tieftemperaturzerlegung von Luft
DE102009048456A1 (de) Verfahren und Vorrichtung zur Tieftemperaturzerlegung von Luft
EP2236964A1 (fr) Procédé et dispositif de séparation de l'air à basse température
EP2520886A1 (fr) Procédé et dispositif de production d'un produit comprimé à oxygène gazeux par décomposition à basse température d'air
EP3290843A2 (fr) Procédé et dispositif destiné à fabriquer de l'azote pressurisé et liquide par décomposition à basse température de l'air
EP2963369B1 (fr) Procede et dispositif cryogeniques de separation d'air
EP2053331A1 (fr) Procédé et dispositif de séparation de l'air à basse température
EP2600090B1 (fr) Procédé et dispositif destinés à la production d'oxygène sous pression par décomposition à basse température de l'air
EP2551619A1 (fr) Procédé et dispositif destinés à l'obtention d'oxygène pressurisé et d'azote pressurisé par la décomposition à basse température de l'air
DE102007042462A1 (de) Verfahren und Vorrichtung zur Tieftemperaturzerlegung von Luft
EP1750074A1 (fr) Procédé et dispositif pour la séparation cryogénique d'air
EP2914913B1 (fr) Procédé de séparation d'air à basse température dans une installation de séparation d'air et installation de séparation d'air
WO2011110301A2 (fr) Procédé et dispositif de séparation de l'air à basse température
DE19933558C5 (de) Dreisäulenverfahren und -vorrichtung zur Tieftemperaturzerlegung von Luft
EP3067650B1 (fr) Installation et procede de production d'oxygene par separation cryogenique de l'air
EP1199532B1 (fr) Système de séparation d'air cryogénique à trois colonnes
EP3343159A1 (fr) Procédé et dispositif de production d'oxygène gazeux et azote comprimé gazeux

Legal Events

Date Code Title Description
PUAI Public reference made under article 153(3) epc to a published international application that has entered the european phase

Free format text: ORIGINAL CODE: 0009012

AK Designated contracting states

Kind code of ref document: A1

Designated state(s): AL AT BE BG CH CY CZ DE DK EE ES FI FR GB GR HR HU IE IS IT LI LT LU LV MC MK MT NL NO PL PT RO RS SE SI SK SM TR

AX Request for extension of the european patent

Extension state: BA ME

GRAP Despatch of communication of intention to grant a patent

Free format text: ORIGINAL CODE: EPIDOSNIGR1

17P Request for examination filed

Effective date: 20131107

RBV Designated contracting states (corrected)

Designated state(s): AL AT BE BG CH CY CZ DE DK EE ES FI FR GB GR HR HU IE IS IT LI LT LU LV MC MK MT NL NO PL PT RO RS SE SI SK SM TR

RIC1 Information provided on ipc code assigned before grant

Ipc: F25J 3/04 20060101AFI20131129BHEP

INTG Intention to grant announced

Effective date: 20131217

GRAJ Information related to disapproval of communication of intention to grant by the applicant or resumption of examination proceedings by the epo deleted

Free format text: ORIGINAL CODE: EPIDOSDIGR1

GRAP Despatch of communication of intention to grant a patent

Free format text: ORIGINAL CODE: EPIDOSNIGR1

INTG Intention to grant announced

Effective date: 20140410

INTG Intention to grant announced

Effective date: 20140417

GRAS Grant fee paid

Free format text: ORIGINAL CODE: EPIDOSNIGR3

GRAA (expected) grant

Free format text: ORIGINAL CODE: 0009210

AK Designated contracting states

Kind code of ref document: B1

Designated state(s): AL AT BE BG CH CY CZ DE DK EE ES FI FR GB GR HR HU IE IS IT LI LT LU LV MC MK MT NL NO PL PT RO RS SE SI SK SM TR

REG Reference to a national code

Ref country code: GB

Ref legal event code: FG4D

Free format text: NOT ENGLISH

REG Reference to a national code

Ref country code: CH

Ref legal event code: EP

REG Reference to a national code

Ref country code: IE

Ref legal event code: FG4D

Free format text: LANGUAGE OF EP DOCUMENT: GERMAN

REG Reference to a national code

Ref country code: AT

Ref legal event code: REF

Ref document number: 677897

Country of ref document: AT

Kind code of ref document: T

Effective date: 20140815

REG Reference to a national code

Ref country code: DE

Ref legal event code: R096

Ref document number: 502012000986

Country of ref document: DE

Effective date: 20140828

REG Reference to a national code

Ref country code: NL

Ref legal event code: VDEP

Effective date: 20140716

REG Reference to a national code

Ref country code: LT

Ref legal event code: MG4D

PG25 Lapsed in a contracting state [announced via postgrant information from national office to epo]

Ref country code: FI

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20140716

Ref country code: LT

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20140716

Ref country code: PT

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20141117

Ref country code: BG

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20141016

Ref country code: SE

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20140716

Ref country code: ES

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20140716

Ref country code: GR

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20141017

Ref country code: NO

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20141016

PG25 Lapsed in a contracting state [announced via postgrant information from national office to epo]

Ref country code: IS

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20141116

Ref country code: LV

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20140716

Ref country code: RS

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20140716

Ref country code: PL

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20140716

Ref country code: NL

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20140716

Ref country code: CY

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20140716

REG Reference to a national code

Ref country code: DE

Ref legal event code: R026

Ref document number: 502012000986

Country of ref document: DE

PLBI Opposition filed

Free format text: ORIGINAL CODE: 0009260

PG25 Lapsed in a contracting state [announced via postgrant information from national office to epo]

Ref country code: CZ

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20140716

Ref country code: SK

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20140716

Ref country code: IT

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20140716

Ref country code: RO

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20140716

Ref country code: DK

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20140716

Ref country code: EE

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20140716

PLAX Notice of opposition and request to file observation + time limit sent

Free format text: ORIGINAL CODE: EPIDOSNOBS2

26 Opposition filed

Opponent name: L AIR LIQIDE, SOCIETE ANONYME POUR L ETUDE ET L EX

Effective date: 20150416

PG25 Lapsed in a contracting state [announced via postgrant information from national office to epo]

Ref country code: MC

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20140716

Ref country code: BE

Free format text: LAPSE BECAUSE OF NON-PAYMENT OF DUE FEES

Effective date: 20141130

Ref country code: LU

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20141120

REG Reference to a national code

Ref country code: IE

Ref legal event code: MM4A

PLAF Information modified related to communication of a notice of opposition and request to file observations + time limit

Free format text: ORIGINAL CODE: EPIDOSCOBS2

REG Reference to a national code

Ref country code: FR

Ref legal event code: PLFP

Year of fee payment: 4

PG25 Lapsed in a contracting state [announced via postgrant information from national office to epo]

Ref country code: IE

Free format text: LAPSE BECAUSE OF NON-PAYMENT OF DUE FEES

Effective date: 20141120

PLBB Reply of patent proprietor to notice(s) of opposition received

Free format text: ORIGINAL CODE: EPIDOSNOBS3

PG25 Lapsed in a contracting state [announced via postgrant information from national office to epo]

Ref country code: SI

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20140716

REG Reference to a national code

Ref country code: CH

Ref legal event code: PL

PG25 Lapsed in a contracting state [announced via postgrant information from national office to epo]

Ref country code: LI

Free format text: LAPSE BECAUSE OF NON-PAYMENT OF DUE FEES

Effective date: 20151130

Ref country code: HR

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20140716

Ref country code: TR

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20140716

Ref country code: MT

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20140716

Ref country code: CH

Free format text: LAPSE BECAUSE OF NON-PAYMENT OF DUE FEES

Effective date: 20151130

Ref country code: HU

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT; INVALID AB INITIO

Effective date: 20121120

REG Reference to a national code

Ref country code: FR

Ref legal event code: PLFP

Year of fee payment: 5

PLCK Communication despatched that opposition was rejected

Free format text: ORIGINAL CODE: EPIDOSNREJ1

REG Reference to a national code

Ref country code: DE

Ref legal event code: R100

Ref document number: 502012000986

Country of ref document: DE

PG25 Lapsed in a contracting state [announced via postgrant information from national office to epo]

Ref country code: SM

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20140716

PLBN Opposition rejected

Free format text: ORIGINAL CODE: 0009273

STAA Information on the status of an ep patent application or granted ep patent

Free format text: STATUS: OPPOSITION REJECTED

27O Opposition rejected

Effective date: 20170513

REG Reference to a national code

Ref country code: FR

Ref legal event code: PLFP

Year of fee payment: 6

PG25 Lapsed in a contracting state [announced via postgrant information from national office to epo]

Ref country code: MK

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20140716

REG Reference to a national code

Ref country code: FR

Ref legal event code: PLFP

Year of fee payment: 7

PG25 Lapsed in a contracting state [announced via postgrant information from national office to epo]

Ref country code: AL

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20140716

REG Reference to a national code

Ref country code: AT

Ref legal event code: MM01

Ref document number: 677897

Country of ref document: AT

Kind code of ref document: T

Effective date: 20171120

PG25 Lapsed in a contracting state [announced via postgrant information from national office to epo]

Ref country code: AT

Free format text: LAPSE BECAUSE OF NON-PAYMENT OF DUE FEES

Effective date: 20171120

REG Reference to a national code

Ref country code: DE

Ref legal event code: R081

Ref document number: 502012000986

Country of ref document: DE

Owner name: LINDE GMBH, DE

Free format text: FORMER OWNER: LINDE AG, 80331 MUENCHEN, DE

PGFP Annual fee paid to national office [announced via postgrant information from national office to epo]

Ref country code: FR

Payment date: 20211119

Year of fee payment: 10

Ref country code: DE

Payment date: 20211122

Year of fee payment: 10

Ref country code: GB

Payment date: 20211123

Year of fee payment: 10

REG Reference to a national code

Ref country code: DE

Ref legal event code: R119

Ref document number: 502012000986

Country of ref document: DE

GBPC Gb: european patent ceased through non-payment of renewal fee

Effective date: 20221120

PG25 Lapsed in a contracting state [announced via postgrant information from national office to epo]

Ref country code: GB

Free format text: LAPSE BECAUSE OF NON-PAYMENT OF DUE FEES

Effective date: 20221120

Ref country code: DE

Free format text: LAPSE BECAUSE OF NON-PAYMENT OF DUE FEES

Effective date: 20230601

PG25 Lapsed in a contracting state [announced via postgrant information from national office to epo]

Ref country code: FR

Free format text: LAPSE BECAUSE OF NON-PAYMENT OF DUE FEES

Effective date: 20221130