EP2520886A1 - Procédé et dispositif de production d'un produit comprimé à oxygène gazeux par décomposition à basse température d'air - Google Patents
Procédé et dispositif de production d'un produit comprimé à oxygène gazeux par décomposition à basse température d'air Download PDFInfo
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- EP2520886A1 EP2520886A1 EP11003707A EP11003707A EP2520886A1 EP 2520886 A1 EP2520886 A1 EP 2520886A1 EP 11003707 A EP11003707 A EP 11003707A EP 11003707 A EP11003707 A EP 11003707A EP 2520886 A1 EP2520886 A1 EP 2520886A1
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- Prior art keywords
- air
- pressure
- heat exchanger
- main heat
- cooled
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- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
- F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
- F25J3/00—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification
- F25J3/02—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream
- F25J3/04—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream for air
- F25J3/04248—Generation of cold for compensating heat leaks or liquid production, e.g. by Joule-Thompson expansion
- F25J3/04375—Details relating to the work expansion, e.g. process parameter etc.
- F25J3/04393—Details relating to the work expansion, e.g. process parameter etc. using multiple or multistage gas work expansion
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- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
- F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
- F25J3/00—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification
- F25J3/02—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream
- F25J3/04—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream for air
- F25J3/04006—Providing pressurised feed air or process streams within or from the air fractionation unit
- F25J3/04012—Providing pressurised feed air or process streams within or from the air fractionation unit by compression of warm gaseous streams; details of intake or interstage cooling
- F25J3/04024—Providing pressurised feed air or process streams within or from the air fractionation unit by compression of warm gaseous streams; details of intake or interstage cooling of purified feed air, so-called boosted air
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- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
- F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
- F25J3/00—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification
- F25J3/02—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream
- F25J3/04—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream for air
- F25J3/04006—Providing pressurised feed air or process streams within or from the air fractionation unit
- F25J3/04048—Providing pressurised feed air or process streams within or from the air fractionation unit by compression of cold gaseous streams, e.g. intermediate or oxygen enriched (waste) streams
- F25J3/04054—Providing pressurised feed air or process streams within or from the air fractionation unit by compression of cold gaseous streams, e.g. intermediate or oxygen enriched (waste) streams of air
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- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
- F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
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- F25J3/04—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream for air
- F25J3/04006—Providing pressurised feed air or process streams within or from the air fractionation unit
- F25J3/04078—Providing pressurised feed air or process streams within or from the air fractionation unit providing pressurized products by liquid compression and vaporisation with cold recovery, i.e. so-called internal compression
- F25J3/04084—Providing pressurised feed air or process streams within or from the air fractionation unit providing pressurized products by liquid compression and vaporisation with cold recovery, i.e. so-called internal compression of nitrogen
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- F25J3/04078—Providing pressurised feed air or process streams within or from the air fractionation unit providing pressurized products by liquid compression and vaporisation with cold recovery, i.e. so-called internal compression
- F25J3/0409—Providing pressurised feed air or process streams within or from the air fractionation unit providing pressurized products by liquid compression and vaporisation with cold recovery, i.e. so-called internal compression of oxygen
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- F25J3/04151—Purification and (pre-)cooling of the feed air; recuperative heat-exchange with product streams
- F25J3/04163—Hot end purification of the feed air
- F25J3/04169—Hot end purification of the feed air by adsorption of the impurities
- F25J3/04175—Hot end purification of the feed air by adsorption of the impurities at a pressure of substantially more than the highest pressure column
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- F25J3/04151—Purification and (pre-)cooling of the feed air; recuperative heat-exchange with product streams
- F25J3/04187—Cooling of the purified feed air by recuperative heat-exchange; Heat-exchange with product streams
- F25J3/0423—Subcooling of liquid process streams
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- F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
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- F25J3/04—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream for air
- F25J3/04248—Generation of cold for compensating heat leaks or liquid production, e.g. by Joule-Thompson expansion
- F25J3/04254—Generation of cold for compensating heat leaks or liquid production, e.g. by Joule-Thompson expansion using the cold stored in external cryogenic fluids
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- F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
- F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
- F25J3/00—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification
- F25J3/02—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream
- F25J3/04—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream for air
- F25J3/04248—Generation of cold for compensating heat leaks or liquid production, e.g. by Joule-Thompson expansion
- F25J3/04284—Generation of cold for compensating heat leaks or liquid production, e.g. by Joule-Thompson expansion using internal refrigeration by open-loop gas work expansion, e.g. of intermediate or oxygen enriched (waste-)streams
- F25J3/0429—Generation of cold for compensating heat leaks or liquid production, e.g. by Joule-Thompson expansion using internal refrigeration by open-loop gas work expansion, e.g. of intermediate or oxygen enriched (waste-)streams of feed air, e.g. used as waste or product air or expanded into an auxiliary column
- F25J3/04296—Claude expansion, i.e. expanded into the main or high pressure column
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- F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
- F25J3/00—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification
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- F25J3/04406—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream for air using a dual pressure main column system
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- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
- F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
- F25J3/00—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification
- F25J3/02—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream
- F25J3/04—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream for air
- F25J3/04472—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream for air using the cold from cryogenic liquids produced within the air fractionation unit and stored in internal or intermediate storages
- F25J3/04478—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream for air using the cold from cryogenic liquids produced within the air fractionation unit and stored in internal or intermediate storages for controlling purposes, e.g. start-up or back-up procedures
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- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
- F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
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- F25J3/04—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream for air
- F25J3/04763—Start-up or control of the process; Details of the apparatus used
- F25J3/04769—Operation, control and regulation of the process; Instrumentation within the process
- F25J3/04812—Different modes, i.e. "runs" of operation
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- F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
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- F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
- F25J2210/00—Processes characterised by the type or other details of the feed stream
- F25J2210/42—Nitrogen
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- F25J2245/50—Processes or apparatus involving steps for recycling of process streams the recycled stream being oxygen
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Definitions
- the invention relates to a method according to the preamble of patent claim 1.
- the distillation column system of the invention can be used as a two-column system (for example, as a classic Linde double column system), or as a three or more column system. It may in addition to the columns for nitrogen-oxygen separation, further devices for obtaining high purity products and / or other air components, in particular of noble gases, for example, an argon production and / or a krypton-xenon recovery
- a liquid pressurized oxygen product stream is vaporized against a heat carrier and finally recovered as a gaseous pressure product.
- This method is also called internal compression. It serves for the production of pressure oxygen. In the case of a supercritical pressure, no phase transition takes place in the true sense, the product stream is then "pseudo-evaporated".
- a liquid pressurized oxygen product stream is vaporized against a heat carrier and finally recovered as a gaseous pressure product.
- This method is also called internal compression. It serves for the production of pressure oxygen. In the case of a supercritical pressure, no phase transition takes place in the true sense, the product stream is then "pseudo-evaporated".
- a high-pressure heat carrier is liquefied (or pseudo-liquefied when it is under supercritical pressure).
- the heat transfer medium is frequently replaced by a part of Air formed, in the present case of the "second partial flow" of the compressed feed air.
- EP 1139046 A1 EP 1146301 A1 .
- DE 10213212 A1 DE 10213211 A1 .
- EP 1357342 A1 or DE 10238282 A1 DE 10302389 A1 .
- DE 10332863 A1 EP 1544559 A1 .
- EP 1666824 A1 EP 1672301 A1 .
- DE 102005028012 A1 .
- WO 2007033838 A1 WO 2007104449 A1 .
- EP 1845324 A1 is
- the "main heat exchanger system” serves to cool feed air in indirect heat exchange with return streams from the distillation column system. It may be formed of one or more parallel and / or serially connected heat exchanger sections, for example one or more plate heat exchanger blocks.
- post-compression system is here a system of at least two serially connected stages (hereinafter also referred to as “compressor stages”).
- compressor stages serially connected stages
- the invention has for its object to provide a method of the type mentioned above and a corresponding device, which are economically particularly favorable to operate by having an increased product yield, higher product purity, lower operating costs and / or lower investment costs.
- the adiabatic mode of operation of the recompression system ie the absence of any intercooling between its stages, not only leads to an apparatus saving, but also to an overall very efficient process.
- the second intermediate temperature at which the second air stream is supplied to the secondary compression system is below the temperature of the warm end of the main heat exchanger system, in particular by at least 10 K. It is for example 230 to 270 K.
- the distillation column system of the invention preferably comprises a high pressure column and a low pressure column.
- the first pressure to which the total air is compressed is at least 5 bar, preferably at least 10 bar higher than the operating pressure at the top of the high-pressure column.
- the work-performing expansion of the first air flow is performed in two parallel relaxation machines, with a two expansion machines with the last stage of the secondary compression system and the other of the two expansion machines with another stage of the secondary compression system is directly mechanically coupled
- Parallel connection here means that the two expansion machines have the same inlet pressure. Preferably, they also have the same inlet temperature and the same outlet pressure. Alternatively, they are operated with different inlet temperatures and / or with different outlet pressures.
- Pressures are referred to herein as "equal" when the pressure differential between the respective locations is not greater than the natural conduction losses due to pressure losses in piping, heat exchangers, coolers, adsorbers, etc. Similarly, two streams are at the same temperature even if their temperature differs by a value corresponding to a temperature difference due to natural variations or to common insulation losses along a pipe.
- the expansion machines are formed for example by turbines, each with a turbine wheel.
- a “direct mechanical coupling” here means a direct connection between the expansion machine and the after-compressor stage via a common shaft, in particular not via a transmission.
- one of the expansion machines must be coupled to a warm braking device, ie to a dissipative brake (for example oil brake), to a generator or to a warm compressor for generating process refrigeration.
- a dissipative brake for example oil brake
- This can be realized by using a corresponding third expansion machine, which is not coupled to any of the stages of the Nachverdichtungssystems, or in that on the shaft of one of the above-mentioned expansion machines additionally an oil brake or a generator is arranged.
- the second air stream is cooled downstream of the Nachverdichtungssystems in an aftercooler in indirect heat exchange with cooling water before it is fed to the warm end of the main heat exchanger system.
- a part of the mechanical energy generated in the expansion machine which is coupled to the last stage of the Nachverdichtungssystems, are released into the warm.
- the corresponding expansion machine generates both the energy required for driving the last stage and at least a portion of the required process cooling.
- it produces all the cold needed in the process to compensate for insulation and replacement losses and, where appropriate, for product liquefaction.
- the recompression system has exactly two stages.
- the recompression system has exactly three stages or more than three stages, wherein the work-performing expansion of the first air flow is carried out in three parallel expansion machines, each of the three expansion machines with one stage of the Nachverdichtungssystems is directly mechanically coupled. This makes it possible to achieve even higher end pressures in the second air flow, furthermore without the use of external energy that goes beyond the drive of the main air compressor.
- a third air stream which is branched off from the feed air compressed to the first pressure (p1) in addition to the first and the second air flow, is cooled to the cold end under the first pressure (p1) in the main heat exchanger and then introduced into the distillation column system.
- the first and third air streams may be cooled in common passages of the main heat exchanger system to the first intermediate temperature, with the first air stream branched off at the first intermediate temperature and led out of the main heat exchanger system, while the third air stream continues to cool to the cold end , Alternatively, the first and third air streams may be cooled in separate passages of the main heat exchanger system.
- the third airflow supports the second airflow in the (pseudo) evaporation of the oxygen product stream.
- the entire compressed to the first pressure (p1) feed air is divided into the first and the second air flow, or - if three air streams are used - on the first, second and third air flow.
- some of the compressed air compressed in the main air compressor can still be used for other purposes. This portion of air, such as instrument air, does not constitute part of the "feed air" introduced into the distillation column system.
- the invention also relates to a device for the cryogenic separation of air according to the claims 7 to 10.
- FIG. 1 In the process of FIG. 1 is compressed atmospheric air 1 after flowing through a filter 2 in a main air compressor 3 to a first pressure p1 of about 18 bar.
- the compressed feed air 4 is in a cooling device 5, the is formed for example by a direct contact cooler or by one or more indirect cooling stages, cooled and then fed via line 6 to a cleaning device 7 having a pair of switchable container, which are filled with an adsorbent, in particular with a molecular sieve.
- the purified feed air 8 is divided into a first airflow 9, 10 (so-called turbine flow) and a second airflow 20 (so-called throttle flow) and an optional third airflow 9, 30 (additional throttle flow).
- the first air stream 9, 10 is fed directly to a main heat exchanger system 40 at its warm end.
- the main heat exchanger system 40 is formed in the example by a single heat exchanger block and hereinafter referred to as the main heat exchanger.
- the first air stream is cooled to a first intermediate temperature T1 and fed via line 10 under this intermediate temperature and the first pressure p1 two parallel relaxation machines 11, 12, which are each formed by a turboexpander.
- the working expanded first air stream 14 is reunited and introduced into a distillation column system, which in the example comprises a high pressure column 50, a low pressure column 51, a main condenser 52 and a subcooling countercurrent 53.
- the operating pressures (in each case at the top) are 3 to 12 bar in the high-pressure column and 1.2 to 4.5 bar in the low-pressure column, in a specific example 1.4 bar and 5.8 bar.
- the second air stream 20 is cooled in the main heat exchanger 40 to a second intermediate temperature T1 of 250 K.
- the cooled second air stream 21 is supplied under the second intermediate temperature T1 and below the first pressure p1 of the first stage 22 of a two-stage recompression system (22, 24, 25) and first recompressed to an intermediate pressure. Via line 23, it is passed directly (that is, in particular without intermediate cooling) to the second and last stage 24 of the secondary compression system and further compressed there to a second pressure p2 of 45 bar.
- the inlet temperature of the second stage 24 is approximately at the level of the ambient temperature, while the first stage 22 is operated as a cold compressor, ie with an inlet temperature at a significantly lower level.
- the heat of compression of the second stage 24 is removed in an aftercooler 25 by indirect heat exchange with cooling water.
- This two-tiered one Post-compression system is operated adiabatically, that is, there is no cooling between the two stages 22, 24 made.
- the recompressed second air stream 26 is fed under the second pressure p2 to the warm end of the main heat exchanger system 40, cooled in the main heat exchanger system 40 and liquefied or pseudo-liquefied, throttled to some high-pressure column pressure (27) and then via the lines 28 and 29 in The feed station is located some practical or theoretical plates above the feed of the first air stream 29. At least a portion of the supplied liquid air is withdrawn via line 35 back from the high pressure column 50 and the supercooling Countercurrent 53, line 36 and throttle valve 37 of the low pressure column 51 fed to a suitable first intermediate point.
- a third air stream 30 is shown, which is introduced together with the first via line 9 in the main heat exchanger 40. After the diversion of the first air flow at the first intermediate temperature of the third air flow continues its cooling in the main heat exchanger 40 to the cold end, it is optionally liquefied or pseudo-liquefied and then via a throttle valve 31 and the lines 32 and 29 together with the throttled second Air stream 28 introduced into the distillation column system.
- the two recompression stages 22 and 24 are each driven by a common shaft of the expansion machines 11, 12.
- Liquid raw oxygen 54 from the bottom of the high-pressure column 50 is cooled in the subcooling countercurrent 53 and introduced via line 55 and throttle valve 56 at a second intermediate point in the low pressure column 51, which is arranged below the first intermediate point.
- Liquid nitrogen 57 from the main condenser 52 is fed to a first part 58 as reflux to the top of the high pressure column 50.
- the remainder 59 is discharged to a part 60, 61 as liquid product (LIN) and fed to another part 62 of an internal compression.
- the liquid nitrogen 62 is brought in a nitrogen pump 63 to a pressure of 7 to 100 bar
- the high pressure liquid nitrogen 64 is vaporized in the main heat exchanger system 40 and to about ambient temperature warmed up.
- the nitrogen product stream 65 withdrawn from the hot end of the main heat exchanger system 40 exits the plant as a gaseous high pressure nitrogen compressed nitrogen product [GAN I (IC)].
- a liquid impure nitrogen stream 66 is withdrawn and abandoned after cooling in the subcooling countercurrent 53 via line 67 as reflux liquid to the head of the low pressure column 51.
- Via line 68 can - for example, when starting the system, but also in stationary operation - additional reflux liquid are applied to the low pressure column 51, for example, from a liquid tank comes from either an external source, with the liquid nitrogen 61 from the main capacitor 52 or both are fed.
- Liquid oxygen 69 is brought in an oxygen pump 46 to an elevated pressure of 6 to about 100 bar. A first portion thereof forms the "liquid oxygen product stream" and is supplied via line 71 to the cold end of the main heat exchanger 40.
- the oxygen product stream is vaporized or pseudo-evaporated under the elevated pressure in the main heat exchanger system 40, warmed to about ambient temperature, and finally withdrawn as gaseous internal compressed oxygen pressure product stream (GOCX IC) 72.
- GOCX IC gaseous internal compressed oxygen pressure product stream
- a second part 73, 76, 77 is discharged after throttling to a pressure of about 1.5 bar via a separator (phase separator) 75 - optionally after cooling in the subcooling countercurrent 53 - as a liquid product (LOX).
- the separated in the separator 75 steam 78 is returned to the low pressure column 51.
- Main heat exchanger 40 warmed to about ambient temperature.
- the warm nitrogen 82 is partially used under the high-pressure column pressure as a sealing gas (seal gas).
- Another part 83 is further compressed in a nitrogen compressor 84 with aftercooler 85 and finally withdrawn as another pressurized nitrogen product (GAN2).
- FIG. 2 is different from this FIG. 1 in that the adiabatic post-compression system is designed in three stages (22, 222, 24). To drive the three stages of the first air stream 10 in three parallel expansion machines 11, 211, 12 is relaxed work, each coupled to one of the Nachverdichtungst 22, 222, 24.
Priority Applications (1)
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EP11003707A EP2520886A1 (fr) | 2011-05-05 | 2011-05-05 | Procédé et dispositif de production d'un produit comprimé à oxygène gazeux par décomposition à basse température d'air |
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EP11003707A EP2520886A1 (fr) | 2011-05-05 | 2011-05-05 | Procédé et dispositif de production d'un produit comprimé à oxygène gazeux par décomposition à basse température d'air |
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EP2963369A1 (fr) * | 2014-07-05 | 2016-01-06 | Linde Aktiengesellschaft | Procede et dispositif cryogeniques de separation d'air |
EP2963370A1 (fr) * | 2014-07-05 | 2016-01-06 | Linde Aktiengesellschaft | Procede et dispositif cryogeniques de separation d'air |
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EP3101374A2 (fr) | 2015-06-03 | 2016-12-07 | Linde Aktiengesellschaft | Procede et installation cryogeniques de separation d'air |
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WO2020083520A1 (fr) * | 2018-10-26 | 2020-04-30 | Linde Aktiengesellschaft | Procédé pour extraire un ou plusieurs produits de l'air et installation de séparation d'air |
RU2783184C2 (ru) * | 2018-10-26 | 2022-11-09 | Линде Гмбх | Способ получения одного или более продуктов разделения воздуха, а также установка разделения воздуха |
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