EP2509797B1 - Reiberwalzen - Google Patents
Reiberwalzen Download PDFInfo
- Publication number
- EP2509797B1 EP2509797B1 EP10788320.9A EP10788320A EP2509797B1 EP 2509797 B1 EP2509797 B1 EP 2509797B1 EP 10788320 A EP10788320 A EP 10788320A EP 2509797 B1 EP2509797 B1 EP 2509797B1
- Authority
- EP
- European Patent Office
- Prior art keywords
- roller
- coating composition
- polyamide
- layer thickness
- roughness
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
- 239000008199 coating composition Substances 0.000 claims description 39
- 239000004642 Polyimide Substances 0.000 claims description 25
- 238000000034 method Methods 0.000 claims description 25
- 229920001721 polyimide Polymers 0.000 claims description 25
- 239000011248 coating agent Substances 0.000 claims description 22
- 238000000576 coating method Methods 0.000 claims description 22
- 239000004962 Polyamide-imide Substances 0.000 claims description 21
- 229920002312 polyamide-imide Polymers 0.000 claims description 21
- 239000007788 liquid Substances 0.000 claims description 19
- 239000004952 Polyamide Substances 0.000 claims description 12
- 229920002647 polyamide Polymers 0.000 claims description 12
- 238000007711 solidification Methods 0.000 claims description 6
- 230000008023 solidification Effects 0.000 claims description 6
- 239000004959 Rilsan Substances 0.000 claims description 5
- 238000007645 offset printing Methods 0.000 claims description 5
- 239000002904 solvent Substances 0.000 claims description 5
- 239000000654 additive Substances 0.000 claims description 3
- 239000003086 colorant Substances 0.000 claims description 3
- 238000001816 cooling Methods 0.000 claims description 3
- 238000001035 drying Methods 0.000 claims description 3
- 239000000945 filler Substances 0.000 claims description 3
- 238000010438 heat treatment Methods 0.000 claims description 3
- 239000000203 mixture Substances 0.000 claims description 3
- 238000005507 spraying Methods 0.000 claims description 3
- 238000010345 tape casting Methods 0.000 claims description 3
- 238000004528 spin coating Methods 0.000 claims 2
- 239000010409 thin film Substances 0.000 claims 2
- 238000007639 printing Methods 0.000 description 9
- 229910000831 Steel Inorganic materials 0.000 description 5
- 239000000463 material Substances 0.000 description 5
- 239000010959 steel Substances 0.000 description 5
- 238000000227 grinding Methods 0.000 description 4
- 238000004519 manufacturing process Methods 0.000 description 4
- 125000003118 aryl group Chemical group 0.000 description 3
- 229920000642 polymer Polymers 0.000 description 3
- 238000005496 tempering Methods 0.000 description 3
- KAKZBPTYRLMSJV-UHFFFAOYSA-N Butadiene Chemical compound C=CC=C KAKZBPTYRLMSJV-UHFFFAOYSA-N 0.000 description 2
- -1 aliphatic diamines Chemical class 0.000 description 2
- 229910052782 aluminium Inorganic materials 0.000 description 2
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 description 2
- 238000005266 casting Methods 0.000 description 2
- 125000005442 diisocyanate group Chemical group 0.000 description 2
- 229920005575 poly(amic acid) Polymers 0.000 description 2
- 239000000843 powder Substances 0.000 description 2
- 239000007858 starting material Substances 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- KXGFMDJXCMQABM-UHFFFAOYSA-N 2-methoxy-6-methylphenol Chemical compound [CH]OC1=CC=CC([CH])=C1O KXGFMDJXCMQABM-UHFFFAOYSA-N 0.000 description 1
- 150000008064 anhydrides Chemical class 0.000 description 1
- 238000007774 anilox coating Methods 0.000 description 1
- 239000004918 carbon fiber reinforced polymer Substances 0.000 description 1
- 239000000919 ceramic Substances 0.000 description 1
- 239000000470 constituent Substances 0.000 description 1
- 229920001577 copolymer Polymers 0.000 description 1
- 150000004985 diamines Chemical class 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 239000003822 epoxy resin Substances 0.000 description 1
- 238000001704 evaporation Methods 0.000 description 1
- 230000008020 evaporation Effects 0.000 description 1
- 239000011152 fibreglass Substances 0.000 description 1
- 229920002313 fluoropolymer Polymers 0.000 description 1
- 230000017525 heat dissipation Effects 0.000 description 1
- 239000000155 melt Substances 0.000 description 1
- 229910052751 metal Inorganic materials 0.000 description 1
- 239000002184 metal Substances 0.000 description 1
- 239000000178 monomer Substances 0.000 description 1
- 150000002825 nitriles Chemical class 0.000 description 1
- 230000010355 oscillation Effects 0.000 description 1
- 238000004806 packaging method and process Methods 0.000 description 1
- 239000003973 paint Substances 0.000 description 1
- 229920001568 phenolic resin Polymers 0.000 description 1
- 239000005011 phenolic resin Substances 0.000 description 1
- 229920000647 polyepoxide Polymers 0.000 description 1
- 229920002635 polyurethane Polymers 0.000 description 1
- 239000004814 polyurethane Substances 0.000 description 1
- 239000011148 porous material Substances 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 238000005096 rolling process Methods 0.000 description 1
- 229920003002 synthetic resin Polymers 0.000 description 1
- 239000000057 synthetic resin Substances 0.000 description 1
Images
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B41—PRINTING; LINING MACHINES; TYPEWRITERS; STAMPS
- B41N—PRINTING PLATES OR FOILS; MATERIALS FOR SURFACES USED IN PRINTING MACHINES FOR PRINTING, INKING, DAMPING, OR THE LIKE; PREPARING SUCH SURFACES FOR USE AND CONSERVING THEM
- B41N7/00—Shells for rollers of printing machines
- B41N7/005—Coating of the composition; Moulding; Reclaiming; Finishing; Trimming
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B41—PRINTING; LINING MACHINES; TYPEWRITERS; STAMPS
- B41F—PRINTING MACHINES OR PRESSES
- B41F31/00—Inking arrangements or devices
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B41—PRINTING; LINING MACHINES; TYPEWRITERS; STAMPS
- B41F—PRINTING MACHINES OR PRESSES
- B41F31/00—Inking arrangements or devices
- B41F31/002—Heating or cooling of ink or ink rollers
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B41—PRINTING; LINING MACHINES; TYPEWRITERS; STAMPS
- B41F—PRINTING MACHINES OR PRESSES
- B41F31/00—Inking arrangements or devices
- B41F31/02—Ducts, containers, supply or metering devices
- B41F31/14—Applications of messenger or other moving transfer rollers
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B41—PRINTING; LINING MACHINES; TYPEWRITERS; STAMPS
- B41F—PRINTING MACHINES OR PRESSES
- B41F31/00—Inking arrangements or devices
- B41F31/26—Construction of inking rollers
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B41—PRINTING; LINING MACHINES; TYPEWRITERS; STAMPS
- B41N—PRINTING PLATES OR FOILS; MATERIALS FOR SURFACES USED IN PRINTING MACHINES FOR PRINTING, INKING, DAMPING, OR THE LIKE; PREPARING SUCH SURFACES FOR USE AND CONSERVING THEM
- B41N7/00—Shells for rollers of printing machines
- B41N7/04—Shells for rollers of printing machines for damping rollers
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B41—PRINTING; LINING MACHINES; TYPEWRITERS; STAMPS
- B41N—PRINTING PLATES OR FOILS; MATERIALS FOR SURFACES USED IN PRINTING MACHINES FOR PRINTING, INKING, DAMPING, OR THE LIKE; PREPARING SUCH SURFACES FOR USE AND CONSERVING THEM
- B41N7/00—Shells for rollers of printing machines
- B41N7/06—Shells for rollers of printing machines for inking rollers
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B41—PRINTING; LINING MACHINES; TYPEWRITERS; STAMPS
- B41N—PRINTING PLATES OR FOILS; MATERIALS FOR SURFACES USED IN PRINTING MACHINES FOR PRINTING, INKING, DAMPING, OR THE LIKE; PREPARING SUCH SURFACES FOR USE AND CONSERVING THEM
- B41N2207/00—Location or type of the layers in shells for rollers of printing machines
- B41N2207/02—Top layers
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B41—PRINTING; LINING MACHINES; TYPEWRITERS; STAMPS
- B41N—PRINTING PLATES OR FOILS; MATERIALS FOR SURFACES USED IN PRINTING MACHINES FOR PRINTING, INKING, DAMPING, OR THE LIKE; PREPARING SUCH SURFACES FOR USE AND CONSERVING THEM
- B41N2207/00—Location or type of the layers in shells for rollers of printing machines
- B41N2207/14—Location or type of the layers in shells for rollers of printing machines characterised by macromolecular organic compounds
Definitions
- the present application relates to a method for. Production of a rigid roll, a rigid roll and their use.
- Offset printing is still the dominant technology in printing processes. It is an indirect printing process that is used in newspaper, magazine, catalog and packaging printing, etc.
- a printing plate is created, typically a thin aluminum plate. This is clamped on a plate cylinder and is in the printing machine with inking and dampening in conjunction. Lipophilic areas of the printing form accept ink while hydrophilic areas remain colorless.
- the ink is transferred to the blanket mounted on a blanket cylinder or offset cylinder.
- the blanket cylinder then transfers the ink to the medium to be printed using a counter-pressure cylinder or another blanket cylinder.
- the color is applied from the reservoir via a special inking unit.
- the ink is typically transported via the stool by means of a plurality of rollers.
- rigid rollers distributed via the stool by means of a plurality of rollers.
- elastic rollers ink rollers
- the distributor rollers typically consist of a steel core with a coating of Rilsan and are therefore often referred to as Rilsanwalzen. These are usually made in the following process: The bare steel core is heated and then introduced into a bath of Rilsan powder (a special grade of polyamide) rotating. The Rilsan powder melts in contact with the hot core, ensuring a relatively uniform coating. The surface quality of the coating is far from sufficient for use in offset printing, so they z. B. must be processed via a grinding process.
- US 5,099,759 relates to an anilox roll with a synthetic resin coating, for example based on polyimides or polyamide-imides.
- EP 0 942 833 B1 describes a paint roller in which an elastomeric coating material such as polymeric nitrile butadiene, phenolic resin, epoxy resin, polyurethane and other materials are applied to a roller.
- an elastomeric coating material such as polymeric nitrile butadiene, phenolic resin, epoxy resin, polyurethane and other materials are applied to a roller.
- the object of the present invention was to provide processes for producing rolls and rolls which overcome the above-mentioned disadvantages of the prior art.
- a roll core is provided in the first step.
- Typical roll cores are made of metal, especially steel and aluminum. But it may also be non-metallic roll cores, for example ceramic, glass fiber reinforced plastic (GfK) or carbon fiber reinforced plastic (CfK) act.
- GfK glass fiber reinforced plastic
- CfK carbon fiber reinforced plastic
- the roll core according to the invention is for an intemperated roll.
- InnertemperATOR rollers are rollers that can be tempered using a tempering medium.
- the tempering medium may be a liquid or tempered air.
- temperature controls are used for cooling.
- Corresponding rollers are for example from the DE 93 169 324 known.
- the roll core may have a roughness Rz of 0.1 to 100 ⁇ m, preferably 1 to 30 ⁇ m.
- the coating composition essentially comprises a polyimide or polyamide prepolymer.
- Starting materials for the preparation of polyimides are preferably aromatic and aliphatic diamines with aromatic tetracarboxylic dianhydrides; instead of the diamines, it is also possible to use diisocyanates.
- a polyamic acid is formed, which then reacts to form the polyimide.
- starting materials for polyamideimides are preferably aromatic tricarboxylic anhydrides with aromatic or aliphatic diamines or diisocyanates.
- Prepolymers are understood as meaning mixtures of reactive monomers which have already partially but not completely reacted with the polymer.
- the curing reaction takes place after application to the roll core. Curing is achieved or accelerated by heating.
- a range of 1 to 1000 microns has proven to be fundamentally suitable, with a range of 10 to 200 microns, or 20 to 120 microns is preferred.
- the coating composition is used essentially on the basis of a polyimide or polyamide-imide prepolymer, it may contain further substances, in particular fillers, additives, colorants, etc.
- the coating composition preferably contains a polyimide or polyamide-imide prepolymer as the main constituent ( ⁇ 50 wt .%).
- the coating composition of prepolymers contains only polyimide prepolymers.
- the coating composition contains only polyamide-imide prepolymers.
- the coating composition contains both polyimide prepolymers and polyamide-imide prepolymers.
- Another embodiment is a roller in which the coating composition contains a polyimide prepolymer and, in addition, polyamides or polyamideimides are contained in the coating composition.
- Another embodiment is a roller in which the coating composition contains dissolved polyimides instead of polyimide prepolymers.
- the coating composition additionally contains polyamides or polyamide prepolymers.
- the ratio of polyimide prepolymers to polyamides + polyamide prepolymers is preferably in the ratio of 10: 0 to 10: 9.
- the coating composition may also contain dissolved polyamide-imide.
- Suitable methods for applying the liquid coating composition are, in particular, spraying, knife coating, thin-layer rotary casting or ring coating.
- the liquid coating composition solidifies by a curing process, i. another reaction to the polymer.
- the prepolymer contains a solvent
- the solidification is assisted by the drying / evaporation of the solvent.
- the material applied according to the invention is preferably of such a uniform, high-quality surface that grinding of the coating composition after solidification is not required.
- the roller according to the invention for the printing process has excellent properties: high wear resistance, high chemical resistance, good ink acceptance, good ink delivery and good cleanability. These properties are also a result of the uncut surface, which thus has no pores and thus is also not susceptible to deposits from the printing process.
- the invention also provides a rigid, temperature-controlled roller, which is obtainable by the process according to the invention.
- the roller according to the invention is characterized by a roller core and a solidified, preferably non-polished, polyimide-based coating located thereon in a layer thickness of 1 to 1000 ⁇ m.
- the coating of the roller according to the invention may have a modulus of elasticity in the range from 0.5 to 500 MPa.
- the roll core has a roughness Rz of 0.1 to 100 microns, preferably 1 to 30 microns.
- the application of the coating composition can lead to a reduction of the roughness.
- the roughness of the solidified coating is less than the roughness of the roll core.
- the invention also provides a method for adjusting a predetermined roughness of the roll, in which a roll core is coated with a defined roughness to obtain a roll with a defined roughness of the coating composition.
- the roll according to the invention is suitable for internally tempered rolls and / or iridescent rolls.
- Internal tempered rolls are used to remove heat from the rolling process to provide even pressure conditions.
- "Oscillation” means that the roller is axially reciprocated during operation (i.e., in the rotating state) so as to achieve improved uniformity of the ink film.
- the rolls with a coating based on polyimide or polyamide-imide are not only advantageous as internally tempered rolls, but also in their non-tempered form.
- their production is facilitated by the fact that a grinding of the surface is not necessary.
- the roughness of the coating can be adjusted by the choice of the roughness of the roll core and the coating thickness.
- the rolls according to the invention are particularly suitable as rebar and Rilsan rolls.
- Her preferred fields of application are in offset printing.
- FIG. 1 shows an inking unit with a ductor roller 1, a lifting roller 2, distributor rollers 3, transfer rollers 4 and inking rollers 5.
- a solution of polyamic acid is applied to a steel core by thin-layer rotary casting.
- the material is heated so that a substantial proportion of the solvent evaporates. This results in the coating composition remaining stable after the end of the rotation. This is followed by a tempering of the roller at up to 250 ° C. Pressure tests with such a roller gave excellent results.
- Example 1 In the method according to Example 1, a steel core with a roughness Rz of 15 microns was used. In a coating with a thickness of 80 microns according to Example 1 remains on the surface an Rz of about 2.2 microns. In a coating with a layer thickness of 30 microns still remains an Rz of about 5 microns, i. By choosing the coating thickness, the roughness of the coating can be adjusted.
Landscapes
- Rolls And Other Rotary Bodies (AREA)
- Application Of Or Painting With Fluid Materials (AREA)
- Inking, Control Or Cleaning Of Printing Machines (AREA)
- Paints Or Removers (AREA)
Priority Applications (3)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
SI201030813T SI2509797T1 (sl) | 2009-12-07 | 2010-12-07 | Valji za deljenje |
PL10788320T PL2509797T3 (pl) | 2009-12-07 | 2010-12-07 | Walce rozcierające |
EP10788320.9A EP2509797B1 (de) | 2009-12-07 | 2010-12-07 | Reiberwalzen |
Applications Claiming Priority (3)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
EP09178216 | 2009-12-07 | ||
EP10788320.9A EP2509797B1 (de) | 2009-12-07 | 2010-12-07 | Reiberwalzen |
PCT/EP2010/069046 WO2011069998A1 (de) | 2009-12-07 | 2010-12-07 | Reiberwalzen |
Publications (2)
Publication Number | Publication Date |
---|---|
EP2509797A1 EP2509797A1 (de) | 2012-10-17 |
EP2509797B1 true EP2509797B1 (de) | 2014-10-01 |
Family
ID=41786424
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
EP10788320.9A Active EP2509797B1 (de) | 2009-12-07 | 2010-12-07 | Reiberwalzen |
Country Status (17)
Country | Link |
---|---|
US (1) | US9308765B2 (ko) |
EP (1) | EP2509797B1 (ko) |
JP (1) | JP5758910B2 (ko) |
KR (1) | KR101757836B1 (ko) |
CN (1) | CN102686411B (ko) |
AR (1) | AR079307A1 (ko) |
AU (1) | AU2010330001B2 (ko) |
BR (1) | BR112012013770B1 (ko) |
CA (1) | CA2783324C (ko) |
DK (1) | DK2509797T3 (ko) |
ES (1) | ES2526255T3 (ko) |
HK (1) | HK1170987A1 (ko) |
PL (1) | PL2509797T3 (ko) |
PT (1) | PT2509797E (ko) |
RU (1) | RU2612566C2 (ko) |
SI (1) | SI2509797T1 (ko) |
WO (1) | WO2011069998A1 (ko) |
Families Citing this family (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JP7044316B2 (ja) * | 2017-10-18 | 2022-03-30 | 富士機械工業株式会社 | グラビア印刷機 |
CN110239202B (zh) * | 2019-06-26 | 2023-06-23 | 云南卓印科技有限公司 | 一种平版印刷橡胶水辊及其制备方法 |
Family Cites Families (18)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US4183298A (en) * | 1977-12-23 | 1980-01-15 | Roland Offsetmaschinenfabrik Faber & Schleicher Ag | Water cooled ink roller for printing presses |
DE3787895T2 (de) * | 1987-10-05 | 1994-05-19 | Kinyosha Kk | Tintenrolle für druckpressen und verfahren zur herstellung. |
WO1989005732A1 (en) * | 1987-12-21 | 1989-06-29 | Kinyosha Co., Ltd | Ink roller for printing press and production thereof |
JP2643187B2 (ja) * | 1987-10-05 | 1997-08-20 | 株式会社金陽社 | インキ装置のインキ受渡しロール及びその製造方法 |
US5061533A (en) * | 1988-10-11 | 1991-10-29 | Mitsubishi Rayon Company Ltd. | Roll formed of carbon fiber composite material |
JPH0717052B2 (ja) * | 1991-07-05 | 1995-03-01 | ボールドウィン プリンティング コントロールズ リミテッド | 電子冷熱素子を利用して加熱または冷却されるシリンダまたはローラおよびその製造方法 |
DE4140048C2 (de) * | 1991-12-05 | 1995-09-21 | Roland Man Druckmasch | Farbwerk einer Druckmaschine, insbesondere Bogenoffsetdruckmaschine |
JP3318136B2 (ja) * | 1994-12-01 | 2002-08-26 | 株式会社リコー | 定着装置 |
EP0942833B1 (de) | 1996-12-07 | 2001-07-18 | WESTLAND GUMMIWERKE GmbH & Co. | Walze für farbverarbeitung |
DE19653911C2 (de) * | 1996-12-21 | 2003-03-27 | Roland Man Druckmasch | Druckmaschinenwalze mit einer farbfreundlichen Beschichtung der Ballenfläche des Walzenkerns, insbesondere Farbwalze |
JP4073345B2 (ja) * | 2003-03-24 | 2008-04-09 | 富士フイルム株式会社 | 平版印刷方法および印刷装置 |
DE10328742B4 (de) * | 2003-06-25 | 2009-10-29 | Kba-Metronic Aktiengesellschaft | Verfahren zum Aufbringen von Mitteln mit Flüssigkristallen auf Substrate |
TWI461306B (zh) * | 2006-07-19 | 2014-11-21 | Boettcher Gmbh & Co Felix | 隨機雷射處理之薄膜滾子 |
DE102006037615A1 (de) * | 2006-08-10 | 2008-02-14 | Felix Böttcher Gmbh & Co. Kg | Gummiwalzen mit rauer Oberfläche |
JP5334365B2 (ja) * | 2006-10-23 | 2013-11-06 | 株式会社ミヤコシ | オフセット印刷機の湿し水装置 |
JP2008143180A (ja) * | 2006-12-07 | 2008-06-26 | Heidelberger Druckmas Ag | インキ装置の洗浄装置を備えた印刷機 |
DE102007062940A1 (de) | 2007-12-21 | 2009-06-25 | Weros Technology Gmbh | Reiber- oder Übertragungswalze |
US8384748B2 (en) * | 2009-07-29 | 2013-02-26 | Xerox Corporation | Fabrication of improved aluminum rollers with low adhesion and ultra/super hydrophobicity and/or oleophobicity by electrospinning technique in solid ink-jet marking |
-
2010
- 2010-12-07 US US13/514,527 patent/US9308765B2/en active Active
- 2010-12-07 AR ARP100104504A patent/AR079307A1/es active IP Right Grant
- 2010-12-07 PL PL10788320T patent/PL2509797T3/pl unknown
- 2010-12-07 CN CN201080055206.4A patent/CN102686411B/zh active Active
- 2010-12-07 PT PT107883209T patent/PT2509797E/pt unknown
- 2010-12-07 KR KR1020127017355A patent/KR101757836B1/ko active IP Right Grant
- 2010-12-07 WO PCT/EP2010/069046 patent/WO2011069998A1/de active Application Filing
- 2010-12-07 AU AU2010330001A patent/AU2010330001B2/en not_active Ceased
- 2010-12-07 RU RU2012128529A patent/RU2612566C2/ru active
- 2010-12-07 SI SI201030813T patent/SI2509797T1/sl unknown
- 2010-12-07 JP JP2012542510A patent/JP5758910B2/ja not_active Expired - Fee Related
- 2010-12-07 BR BR112012013770A patent/BR112012013770B1/pt active IP Right Grant
- 2010-12-07 CA CA2783324A patent/CA2783324C/en active Active
- 2010-12-07 DK DK10788320.9T patent/DK2509797T3/en active
- 2010-12-07 EP EP10788320.9A patent/EP2509797B1/de active Active
- 2010-12-07 ES ES10788320.9T patent/ES2526255T3/es active Active
-
2012
- 2012-11-21 HK HK12111880.6A patent/HK1170987A1/xx not_active IP Right Cessation
Also Published As
Publication number | Publication date |
---|---|
SI2509797T1 (sl) | 2015-01-30 |
CA2783324A1 (en) | 2011-06-16 |
RU2612566C2 (ru) | 2017-03-09 |
CN102686411B (zh) | 2017-01-18 |
US9308765B2 (en) | 2016-04-12 |
DK2509797T3 (en) | 2014-12-01 |
KR20120094088A (ko) | 2012-08-23 |
AR079307A1 (es) | 2012-01-18 |
KR101757836B1 (ko) | 2017-07-26 |
RU2012128529A (ru) | 2014-01-20 |
HK1170987A1 (en) | 2013-03-15 |
CN102686411A (zh) | 2012-09-19 |
PT2509797E (pt) | 2015-01-05 |
AU2010330001B2 (en) | 2014-09-04 |
BR112012013770A2 (pt) | 2016-04-26 |
EP2509797A1 (de) | 2012-10-17 |
CA2783324C (en) | 2018-09-18 |
BR112012013770B1 (pt) | 2020-04-14 |
AU2010330001A1 (en) | 2012-06-21 |
WO2011069998A1 (de) | 2011-06-16 |
JP2013512803A (ja) | 2013-04-18 |
US20130029051A1 (en) | 2013-01-31 |
ES2526255T3 (es) | 2015-01-08 |
JP5758910B2 (ja) | 2015-08-05 |
PL2509797T3 (pl) | 2015-03-31 |
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