EP1549729B2 - Verfahren zur herstellung eines festen riechstoffkonzentrates - Google Patents

Verfahren zur herstellung eines festen riechstoffkonzentrates Download PDF

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Publication number
EP1549729B2
EP1549729B2 EP03748123.1A EP03748123A EP1549729B2 EP 1549729 B2 EP1549729 B2 EP 1549729B2 EP 03748123 A EP03748123 A EP 03748123A EP 1549729 B2 EP1549729 B2 EP 1549729B2
Authority
EP
European Patent Office
Prior art keywords
solid
mixture
fragrance
fatty alcohol
liquid
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
EP03748123.1A
Other languages
German (de)
English (en)
French (fr)
Other versions
EP1549729B1 (de
EP1549729A1 (de
Inventor
Raymond Heinz
Hans-Jürgen HUPPERT
Katharina Girke
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Bell Flavors and Fragrances Duft und Aroma GmbH
Original Assignee
Bell Flavors and Fragrances Duft und Aroma GmbH
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Family has litigation
First worldwide family litigation filed litigation Critical https://patents.darts-ip.com/?family=32049241&utm_source=google_patent&utm_medium=platform_link&utm_campaign=public_patent_search&patent=EP1549729(B2) "Global patent litigation dataset” by Darts-ip is licensed under a Creative Commons Attribution 4.0 International License.
Application filed by Bell Flavors and Fragrances Duft und Aroma GmbH filed Critical Bell Flavors and Fragrances Duft und Aroma GmbH
Publication of EP1549729A1 publication Critical patent/EP1549729A1/de
Publication of EP1549729B1 publication Critical patent/EP1549729B1/de
Application granted granted Critical
Publication of EP1549729B2 publication Critical patent/EP1549729B2/de
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

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Classifications

    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/50—Perfumes
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/50—Perfumes
    • C11D3/502—Protected perfumes
    • C11D3/505—Protected perfumes encapsulated or adsorbed on a carrier, e.g. zeolite or clay

Definitions

  • the invention relates to a process for the preparation of a solid fragrance concentrate, which is advantageously used for perfuming solid soaps and solid detergents and dishwashing detergents in powder, granule, chip or tablet form.
  • fragrances or fragrance mixtures are liquid at normal temperature and often volatile substances whose introduction into solid household chemical or cosmetic products such.
  • solid soaps or in powder, granular, chip or tablet detergent and detergent problems As solid soaps or in powder, granular, chip or tablet detergent and detergent problems.
  • Powdered solid washing and rinsing agents were intensively mixed according to the prior art prior to packaging or before their formation into tablets, chips, etc. with finely sprayed liquid fragrance concentrate.
  • fragrances When the fragrances are sprayed, high losses of substance occur during evaporation due to evaporation.
  • the often volatile and combustible fragrances together with air form explosive gas-air mixtures, which can lead to deflagrations and fires in the production plants.
  • From the DE 19735783 A1 is also a high-dosage perfume shaped article having a content of 20 to 50 wt .-% perfume and the balance, ie at least 50% carrier material of fatty acid and fatty acid salt known.
  • the support material of at least 50 wt .-% of the total mass of the perfume molding can be up to 50 wt .-% by conventional ingredients of detergents and cleaners, such as. For example, enzyme, bleach, foam inhibitors, dyes, pH adjusting agents, etc. are replaced, these ingredients have only partial carrier material properties.
  • the latter perfume moldings are limited to a perfume uptake of 50 wt .-%.
  • the fatty acids and fatty acid salts used as support materials are only partially biodegradable.
  • a solid fragrance composition which includes a soap gel, an organic solvent and a fragrance.
  • a fragrance is gelatinous and not really firm.
  • solid fragrance also disclosed a gel-like product consisting of a gelling agent, an ether and a fragrance, wherein the proportion of the ether is greater than that of the fragrance.
  • the gel-like consistency makes this type of solid fragrances of the prior art for introducing z. B. in powdery solid detergents and detergents unsuitable.
  • liquid fragrances are erfingdungshack dissolved in normal temperature solid surfactants or Kotensiden comprising fatty alcohol (s) or a mixture of fatty alcohol (s) with fatty acid (s) and / or fatty alcohol ethoxylate and / or polyethylene glycol.
  • liquid fragrances By means of the process according to the invention, up to 60% by weight of liquid fragrances can be dissolved in the surfactants or cosurfactants or the surfactant / cosurfactant mixtures and solidified to give a solid perfume concentrate according to the invention.
  • the solid fragrance concentrates obtained in the above manner can be prepared by known methods in pastillierter or granulated form, and they can be easily added in this form in the production of solid soaps and powder, granular or tablet detergent and rinse and precisely metered.

Landscapes

  • Chemical & Material Sciences (AREA)
  • Wood Science & Technology (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Organic Chemistry (AREA)
  • Dispersion Chemistry (AREA)
  • Detergent Compositions (AREA)
  • Fats And Perfumes (AREA)
  • Cosmetics (AREA)
  • Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
  • Jellies, Jams, And Syrups (AREA)
EP03748123.1A 2002-10-11 2003-10-08 Verfahren zur herstellung eines festen riechstoffkonzentrates Expired - Lifetime EP1549729B2 (de)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
DE10247583A DE10247583C5 (de) 2002-10-11 2002-10-11 Verfahren zur Herstellung eines festen Riechstoffkonzentrates
DE10247583 2002-10-11
PCT/EP2003/011109 WO2004035721A1 (de) 2002-10-11 2003-10-08 Verfahren zur herstellung eines festen riechstoffkonzentrates

Publications (3)

Publication Number Publication Date
EP1549729A1 EP1549729A1 (de) 2005-07-06
EP1549729B1 EP1549729B1 (de) 2007-01-03
EP1549729B2 true EP1549729B2 (de) 2014-06-04

Family

ID=32049241

Family Applications (1)

Application Number Title Priority Date Filing Date
EP03748123.1A Expired - Lifetime EP1549729B2 (de) 2002-10-11 2003-10-08 Verfahren zur herstellung eines festen riechstoffkonzentrates

Country Status (9)

Country Link
US (1) US7485610B2 (enExample)
EP (1) EP1549729B2 (enExample)
JP (1) JP2006516153A (enExample)
CN (1) CN1692154B (enExample)
AT (1) ATE350455T1 (enExample)
DE (2) DE10247583C5 (enExample)
EA (1) EA006727B1 (enExample)
ES (1) ES2280772T5 (enExample)
WO (1) WO2004035721A1 (enExample)

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DE10357676A1 (de) * 2003-12-10 2005-07-21 Henkel Kgaa Duftkomposite
GB2417204A (en) 2004-08-19 2006-02-22 Bell Flavours & Fragrances Ltd Air treatment apparatus
DE102004052929A1 (de) * 2004-10-29 2006-05-04 Bell Flavors & Fragrances Duft Und Aroma Gmbh Verfahren und Vorrichtung zur Herstellung von festem Duftstoff
DE102005025041A1 (de) * 2005-05-30 2006-12-07 Bell Flavors & Fragrances Duft Und Aroma Gmbh Mittel zur Anwendung in Spülmaschinen sowie Vorrichtung für dessen dosierte Einbringung während der Spül- und Trocknungsphasen
DE102005036415A1 (de) * 2005-07-29 2007-02-01 Bell Flavors & Fragrances Duft Und Aroma Gmbh Verfahren zur Anlagerung eines verflüchtigbaren Wirkstoffes an ein festes Stützmaterial und zur gesteuerten Freisetzung des Wirkstoffes in die Umgebung
DE102006029092A1 (de) * 2006-06-24 2007-12-27 Bell Flavors & Fragrances Duft Und Aroma Gmbh Verfahren zur Aromatisierung von zellulosehaltigen Produkten
JP5465823B2 (ja) * 2006-12-13 2014-04-09 ユニ・チャーム株式会社 機能性シートおよび吸収性物品
DE102007037147A1 (de) * 2007-08-07 2009-02-12 Henkel Ag & Co. Kgaa Duftkomposite mit verbesserter Duftfreisetzung
WO2010078067A1 (en) * 2008-12-30 2010-07-08 Bell Flavors And Fragrances, Inc. Carbohydrate treatment for fragranced articles
GB2471303A (en) 2009-06-24 2010-12-29 Bell Flavors & Fragrances Duft Und Aroma Gmbh Microparticles and method of making microparticles
US8476219B2 (en) 2009-11-05 2013-07-02 The Procter & Gamble Company Laundry scent additive
CA2682636C (en) * 2009-11-05 2010-06-15 The Procter & Gamble Company Laundry scent additive
CN103249826B (zh) 2010-12-23 2015-07-15 西姆莱斯有限公司 用于洗涤剂的芳香剂微粒
US20130065812A1 (en) * 2011-09-14 2013-03-14 Ecolab Usa Inc. Water-dilutable solid concentrate
US20130126634A1 (en) 2011-11-22 2013-05-23 Ecolab Usa Inc. Solid air freshener
CN104854229B (zh) 2012-12-20 2018-08-07 宝洁公司 衣物洗涤香味添加剂
CN103405346B (zh) * 2013-06-08 2015-04-22 苏州靖羽新材料有限公司 一种固体香水的制备方法
US9717815B2 (en) 2014-07-30 2017-08-01 Georgia-Pacific Consumer Products Lp Air freshener dispensers, cartridges therefor, systems, and methods
MX388812B (es) 2015-10-23 2025-03-20 Basf Se Soluciones solidas de sustancias odoriferas y agentes aromatizantes con polimeros de vinillactama.
EP3282003B1 (en) 2016-08-09 2020-09-02 Takasago International Corporation Solid composition comprising free and encapsulated fragrances
WO2018055115A1 (de) * 2016-09-26 2018-03-29 Henkel Ag & Co. Kgaa Parfümhaltige schmelzkörper enthaltend hochethoxylierte, nichtionische tenside
AU2017355252A1 (en) 2016-11-02 2019-06-06 Dow Global Technologies Llc Solid non-aqueous gel air odorizer
CN107260128B (zh) * 2017-06-13 2020-09-29 江苏金森海默生物技术有限公司 一种嗅觉障碍检测试剂盒及其应用
DE102017222992A1 (de) * 2017-12-18 2019-06-19 Henkel Ag & Co. Kgaa Herstellung parfümhaltiger Schmelzkörper
CN111286414B (zh) * 2019-11-28 2021-04-27 纳爱斯浙江科技有限公司 一种衣物留香珠及其制备方法
WO2025040240A1 (en) * 2023-08-18 2025-02-27 Symrise Ag Perfume oil capsules for solid formulations with fragrance boost
CN117467499A (zh) * 2023-11-29 2024-01-30 云南养瑞科技集团有限公司 一种液体香料等物质转为具有缓释功能的固体香料的方法

Citations (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2300769A (en) † 1940-03-28 1942-11-03 Palol Perfumed Products Inc Solid perfume
EP0036720A1 (en) † 1980-03-11 1981-09-30 Unilever Plc Detergent composition
EP0397246A2 (en) † 1989-05-11 1990-11-14 The Procter & Gamble Company Coated perfume particles
EP0469228A1 (en) † 1990-07-31 1992-02-05 The Procter & Gamble Company Improved perfume carriage and delivery system for laundry applications
EP0679715A1 (en) † 1994-04-29 1995-11-02 INTERNATIONAL FLAVORS & FRAGRANCES, INC. Formulation of a fat surfactant vehicle containing a fragrance
WO1999009136A1 (de) † 1997-08-18 1999-02-25 Henkel Kommanditgesellschaft Auf Aktien Hochdosierte duftstoff-formkörper
EP0909807A1 (en) † 1997-10-10 1999-04-21 Takasago International Corp. Scented candle and manufacturing method for making same
WO1999021953A1 (de) † 1997-10-23 1999-05-06 Henkel Kommanditgesellschaft Auf Aktien Verfahren zur herstellung von duftperlen
DE19948667A1 (de) † 1999-10-08 2001-04-12 Henkel Kgaa Reinigungsmittelkomponente mit doppelkontrollierter Duftfreisetzung
WO2002038713A1 (en) † 2000-11-09 2002-05-16 Salvona, L.L.C. A controlled delivery system for fabric care products

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GB1169656A (en) * 1967-12-18 1969-11-05 Fumio Enomoto Scented Composition
FR2123824A5 (en) 1971-02-02 1972-09-15 Oreal Solid perfumed soap - contains a soap gel with volatile solvent water and volatile perfume
US3945950A (en) 1974-10-02 1976-03-23 Universal Oil Products Company Solid perfumed compositions of matter
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JPS60182955A (ja) 1984-03-01 1985-09-18 中村物産株式会社 固形状香料の製造方法
AU3164989A (en) * 1988-03-23 1989-09-28 Union Camp Corporation Fragrance carriers for laundry compositions
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Patent Citations (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2300769A (en) † 1940-03-28 1942-11-03 Palol Perfumed Products Inc Solid perfume
EP0036720A1 (en) † 1980-03-11 1981-09-30 Unilever Plc Detergent composition
EP0397246A2 (en) † 1989-05-11 1990-11-14 The Procter & Gamble Company Coated perfume particles
EP0469228A1 (en) † 1990-07-31 1992-02-05 The Procter & Gamble Company Improved perfume carriage and delivery system for laundry applications
EP0679715A1 (en) † 1994-04-29 1995-11-02 INTERNATIONAL FLAVORS & FRAGRANCES, INC. Formulation of a fat surfactant vehicle containing a fragrance
WO1999009136A1 (de) † 1997-08-18 1999-02-25 Henkel Kommanditgesellschaft Auf Aktien Hochdosierte duftstoff-formkörper
EP0909807A1 (en) † 1997-10-10 1999-04-21 Takasago International Corp. Scented candle and manufacturing method for making same
WO1999021953A1 (de) † 1997-10-23 1999-05-06 Henkel Kommanditgesellschaft Auf Aktien Verfahren zur herstellung von duftperlen
DE19948667A1 (de) † 1999-10-08 2001-04-12 Henkel Kgaa Reinigungsmittelkomponente mit doppelkontrollierter Duftfreisetzung
WO2002038713A1 (en) † 2000-11-09 2002-05-16 Salvona, L.L.C. A controlled delivery system for fabric care products

Also Published As

Publication number Publication date
WO2004035721A1 (de) 2004-04-29
EA006727B1 (ru) 2006-04-28
EA200401487A1 (ru) 2005-10-27
DE10247583B4 (de) 2007-08-23
US20050227905A1 (en) 2005-10-13
EP1549729B1 (de) 2007-01-03
DE10247583A1 (de) 2004-04-29
ES2280772T5 (es) 2014-09-19
CN1692154A (zh) 2005-11-02
EP1549729A1 (de) 2005-07-06
DE50306219D1 (de) 2007-02-15
CN1692154B (zh) 2010-04-28
ATE350455T1 (de) 2007-01-15
US7485610B2 (en) 2009-02-03
ES2280772T3 (es) 2007-09-16
JP2006516153A (ja) 2006-06-22
DE10247583C5 (de) 2009-04-30

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