EP1144723B1 - Procede pour appliquer un revetement sur des appareils ou des parties d'appareils utilises pour la construction d'installations chimiques - Google Patents

Procede pour appliquer un revetement sur des appareils ou des parties d'appareils utilises pour la construction d'installations chimiques Download PDF

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Publication number
EP1144723B1
EP1144723B1 EP99967007A EP99967007A EP1144723B1 EP 1144723 B1 EP1144723 B1 EP 1144723B1 EP 99967007 A EP99967007 A EP 99967007A EP 99967007 A EP99967007 A EP 99967007A EP 1144723 B1 EP1144723 B1 EP 1144723B1
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EP
European Patent Office
Prior art keywords
metal
polymer
layer
parts
deposited
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
EP99967007A
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German (de)
English (en)
Other versions
EP1144723A2 (fr
EP1144723A3 (fr
Inventor
Stephan Hüffer
Thilo Krebs
Wolfgang Loth
Bernd Rumpf
Jürgen STURM
Bernd Diebold
Jürgen KORKHAUS
Joachim Nilges
Axel Franke
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BASF SE
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BASF SE
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Publication of EP1144723A3 publication Critical patent/EP1144723A3/fr
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Publication of EP1144723B1 publication Critical patent/EP1144723B1/fr
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

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Classifications

    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F28—HEAT EXCHANGE IN GENERAL
    • F28F—DETAILS OF HEAT-EXCHANGE AND HEAT-TRANSFER APPARATUS, OF GENERAL APPLICATION
    • F28F19/00—Preventing the formation of deposits or corrosion, e.g. by using filters or scrapers
    • F28F19/02—Preventing the formation of deposits or corrosion, e.g. by using filters or scrapers by using coatings, e.g. vitreous or enamel coatings
    • F28F19/06—Preventing the formation of deposits or corrosion, e.g. by using filters or scrapers by using coatings, e.g. vitreous or enamel coatings of metal
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F28—HEAT EXCHANGE IN GENERAL
    • F28F—DETAILS OF HEAT-EXCHANGE AND HEAT-TRANSFER APPARATUS, OF GENERAL APPLICATION
    • F28F19/00—Preventing the formation of deposits or corrosion, e.g. by using filters or scrapers
    • F28F19/02—Preventing the formation of deposits or corrosion, e.g. by using filters or scrapers by using coatings, e.g. vitreous or enamel coatings
    • C—CHEMISTRY; METALLURGY
    • C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C18/00—Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating
    • C23C18/16—Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating by reduction or substitution, e.g. electroless plating
    • C23C18/1601—Process or apparatus
    • C23C18/1603—Process or apparatus coating on selected surface areas
    • C23C18/1614—Process or apparatus coating on selected surface areas plating on one side
    • C23C18/1616—Process or apparatus coating on selected surface areas plating on one side interior or inner surface
    • C—CHEMISTRY; METALLURGY
    • C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C18/00—Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating
    • C23C18/16—Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating by reduction or substitution, e.g. electroless plating
    • C23C18/1601—Process or apparatus
    • C23C18/1633—Process of electroless plating
    • C23C18/1655—Process features
    • C23C18/1662—Use of incorporated material in the solution or dispersion, e.g. particles, whiskers, wires
    • C—CHEMISTRY; METALLURGY
    • C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C18/00—Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating
    • C23C18/16—Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating by reduction or substitution, e.g. electroless plating
    • C23C18/31—Coating with metals
    • C23C18/32—Coating with nickel, cobalt or mixtures thereof with phosphorus or boron
    • C—CHEMISTRY; METALLURGY
    • C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C18/00—Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating
    • C23C18/16—Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating by reduction or substitution, e.g. electroless plating
    • C23C18/31—Coating with metals
    • C23C18/32—Coating with nickel, cobalt or mixtures thereof with phosphorus or boron
    • C23C18/34—Coating with nickel, cobalt or mixtures thereof with phosphorus or boron using reducing agents
    • C23C18/36—Coating with nickel, cobalt or mixtures thereof with phosphorus or boron using reducing agents using hypophosphites
    • C—CHEMISTRY; METALLURGY
    • C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C18/00—Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating
    • C23C18/16—Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating by reduction or substitution, e.g. electroless plating
    • C23C18/31—Coating with metals
    • C23C18/38—Coating with copper
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F28—HEAT EXCHANGE IN GENERAL
    • F28F—DETAILS OF HEAT-EXCHANGE AND HEAT-TRANSFER APPARATUS, OF GENERAL APPLICATION
    • F28F2245/00—Coatings; Surface treatments
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
    • Y10T428/00—Stock material or miscellaneous articles
    • Y10T428/12—All metal or with adjacent metals
    • Y10T428/12493—Composite; i.e., plural, adjacent, spatially distinct metal components [e.g., layers, joint, etc.]
    • Y10T428/12535—Composite; i.e., plural, adjacent, spatially distinct metal components [e.g., layers, joint, etc.] with additional, spatially distinct nonmetal component
    • Y10T428/12556—Organic component
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
    • Y10T428/00—Stock material or miscellaneous articles
    • Y10T428/12—All metal or with adjacent metals
    • Y10T428/12493—Composite; i.e., plural, adjacent, spatially distinct metal components [e.g., layers, joint, etc.]
    • Y10T428/12771—Transition metal-base component
    • Y10T428/12861—Group VIII or IB metal-base component
    • Y10T428/12944—Ni-base component
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
    • Y10T428/00—Stock material or miscellaneous articles
    • Y10T428/31504—Composite [nonstructural laminate]
    • Y10T428/31678—Of metal

Claims (14)

  1. Procédé pour appliquer un revêtement sur des appareils ou des parties d'appareils utilisés pour la construction d'installations chimiques, caractérisé en ce que l'on dépose, de façon autocatalytique, une couche métallique puis une couche de dispersion polymère-métallique sur l'appareil ou sur les appareils ou sur les parties d'appareils destinés à être revêtus, dans un premier temps en déposant, de façon autocatalytique, une couche de métal et de phosphore d'une épaisseur de 1 µm à 15 µm, puis en mettant cette couche en contact avec une solution d'électrolyte métallique qui contient, outre l'électrolyte métallique, un réducteur ainsi que le polymère ou le mélange de polymères destinés au dépôt sous forme dispersée, au moins un polymère étant halogéné et étant constitué de particules sphériques présentant une granulométrie moyenne de 0,1 µm à 1,0 µm.
  2. Procédé selon la revendication 1, caractérisé en ce que les appareils et les parties d'appareils utilisés pour la construction d'installations chimiques sont des parois internes d'appareil, de récipient ou de réacteur, des dispositifs d'évacuation, des ferrures et accessoires de tuyauteries, des systèmes de canalisation, des pompes, des filtres, des condenseurs, des centrifugeuses, des colonnes, des séchoirs, des broyeurs, des installations fixes, des corps de garnissage, des appareils polyvalents qui sont constitués d'un matériau métallique.
  3. Procédé selon la revendication 1 et 2, caractérisé en ce que l'on met en oeuvre, en tant qu'électrolyte métallique, une solution électrolytique de cuivre ou de nickel, et, en tant que réducteur, un phosphinate ou un boranate.
  4. Procédé selon les revendications 1 à 3, caractérisé en ce que l'on ajoute à la solution électrolytique métallique une dispersion d'un polymère halogéné.
  5. Procédé selon les revendications 1 à 4, caractérisé en ce que l'on met en oeuvre, en tant qu'électrolyte métallique, une solution de sel de nickel que l'on soumet à une réduction in situ avec un phosphinate de métal alcalin et à laquelle on ajoute, en tant que polymère halogéné, une dispersion de polytétrafluoroéthylène.
  6. Procédé selon les revendications 1 à 5, caractérisé en ce que l'on dépose une couche de nickel-phosphore-polytétrafluoroéthylène d'une épaisseur de 1 µm à 100 µm.
  7. Procédé selon les revendications 1 à 6, caractérisé en ce que l'on dépose une couche de nickel-phosphore-polytétrafluoroéthylène d'une épaisseur de 3 µm à 50 µm.
  8. Procédé selon les revendications 1 à 7, caractérisé en ce que l'on dépose une couche de nickel-phosphore-polytétrafluoroéthylène d'une épaisseur de 5 µm à 25 µm.
  9. Procédé selon les revendications 1 à 8, caractérisé en ce que l'on ajoute à la solution électrolytique métallique une dispersion supplémentaire d'un polymère halogéné ou non halogéné.
  10. Procédé selon la revendication 9, caractérisé en ce que l'on met en oeuvre, en tant que polymère supplémentaire, le polytétrafluoroéthylène ou le polyéthylène ou le polypropylène.
  11. Procédé selon les revendications 9 à 10, caractérisé en ce que l'on met en oeuvre, en tant que polymère supplémentaire, le polytétrafluoroéthylène ou le polyéthylène ou le polypropylène constitués de particules présentant une granulométrie moyenne de 5 µm à 50 µm.
  12. Appareils et parties d'appareils utilisés pour la construction d'installations chimiques que l'on peut obtenir à partir d'un procédé selon les revendications 1 à 11.
  13. Parois internes d'appareil, de récipient ou de réacteur, dispositifs d'évacuation, ferrures et accessoires de tuyauteries, systèmes de canalisation, pompes, filtres, condenseurs, centrifugeuses, colonnes, séchoirs, broyeurs, installations fixes, corps de garnissage ou appareils polyvalents que l'on peut obtenir à partir d'un procédé selon les revendications 1 à 12.
  14. Mise en oeuvre des parois internes d'appareil, de récipient ou de réacteur, des dispositifs de déversement, des ferrures et accessoires de tuyauteries, des systèmes de canalisation, des pompes, des filtres, des condenseurs, des centrifugeuses, des colonnes, des séchoirs, des broyeurs, des installations fixes, des corps de garnissage ou des appareils polyvalents selon les revendications 12 et 13 en vue d'éviter ou de réduire des dépôts issus de fluides.
EP99967007A 1998-12-30 1999-12-24 Procede pour appliquer un revetement sur des appareils ou des parties d'appareils utilises pour la construction d'installations chimiques Expired - Lifetime EP1144723B1 (fr)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
DE19860526 1998-12-30
DE19860526A DE19860526A1 (de) 1998-12-30 1998-12-30 Wärmeüberträger mit verringerter Neigung, Ablagerungen zu bilden und Verfahren zu deren Herstellung
PCT/EP1999/010371 WO2000040774A2 (fr) 1998-12-30 1999-12-24 Procede pour appliquer un revetement sur des appareils ou des parties d'appareils utilises pour la construction d'installations chimiques

Publications (3)

Publication Number Publication Date
EP1144723A2 EP1144723A2 (fr) 2001-10-17
EP1144723A3 EP1144723A3 (fr) 2002-11-13
EP1144723B1 true EP1144723B1 (fr) 2003-04-09

Family

ID=7892984

Family Applications (3)

Application Number Title Priority Date Filing Date
EP99967007A Expired - Lifetime EP1144723B1 (fr) 1998-12-30 1999-12-24 Procede pour appliquer un revetement sur des appareils ou des parties d'appareils utilises pour la construction d'installations chimiques
EP99965554A Expired - Lifetime EP1144725B1 (fr) 1998-12-30 1999-12-24 Procede pour appliquer un revetement sur des reacteurs destines a la polymerisation haute pression de 1-olefines
EP99964672A Expired - Lifetime EP1144724B1 (fr) 1998-12-30 1999-12-24 Echangeur de chaleur presentant une tendance reduite a former des depots, et son procede de production

Family Applications After (2)

Application Number Title Priority Date Filing Date
EP99965554A Expired - Lifetime EP1144725B1 (fr) 1998-12-30 1999-12-24 Procede pour appliquer un revetement sur des reacteurs destines a la polymerisation haute pression de 1-olefines
EP99964672A Expired - Lifetime EP1144724B1 (fr) 1998-12-30 1999-12-24 Echangeur de chaleur presentant une tendance reduite a former des depots, et son procede de production

Country Status (10)

Country Link
US (3) US6509103B1 (fr)
EP (3) EP1144723B1 (fr)
JP (3) JP2003511551A (fr)
KR (3) KR20010103724A (fr)
CN (3) CN1338008A (fr)
AT (3) ATE227360T1 (fr)
CA (2) CA2358099A1 (fr)
DE (4) DE19860526A1 (fr)
ES (2) ES2197710T3 (fr)
WO (3) WO2000040775A2 (fr)

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US6513581B1 (en) 2003-02-04
ATE245210T1 (de) 2003-08-15
US6617047B1 (en) 2003-09-09
DE59905005D1 (de) 2003-05-15
EP1144725A2 (fr) 2001-10-17
DE19860526A1 (de) 2000-07-06
JP2002534606A (ja) 2002-10-15
JP2002534605A (ja) 2002-10-15
WO2000040773A3 (fr) 2000-11-09
EP1144723A2 (fr) 2001-10-17
CN1636305A (zh) 2005-07-06
EP1144725B1 (fr) 2003-07-16
EP1144724B1 (fr) 2002-11-06
WO2000040774A2 (fr) 2000-07-13
WO2000040774A3 (fr) 2002-09-26
JP2003511551A (ja) 2003-03-25
CN1338008A (zh) 2002-02-27
DE59903362D1 (de) 2002-12-12
CA2358099A1 (fr) 2000-07-13
EP1144723A3 (fr) 2002-11-13
ATE237006T1 (de) 2003-04-15
ES2204184T3 (es) 2004-04-16
CN1332810A (zh) 2002-01-23
ATE227360T1 (de) 2002-11-15
WO2000040775A3 (fr) 2000-11-09
KR20010100013A (ko) 2001-11-09
EP1144724A2 (fr) 2001-10-17
WO2000040775A2 (fr) 2000-07-13
CA2358097A1 (fr) 2000-07-13
US6509103B1 (en) 2003-01-21
DE59906313D1 (de) 2003-08-21
WO2000040773A2 (fr) 2000-07-13
ES2197710T3 (es) 2004-01-01
KR20010103724A (ko) 2001-11-23
KR20010100009A (ko) 2001-11-09

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