EP0479010B1 - Dispositif et procédé de stérilisation, de remplissage et de fermeture d'une ouverture de remplissage - Google Patents
Dispositif et procédé de stérilisation, de remplissage et de fermeture d'une ouverture de remplissage Download PDFInfo
- Publication number
- EP0479010B1 EP0479010B1 EP19910115617 EP91115617A EP0479010B1 EP 0479010 B1 EP0479010 B1 EP 0479010B1 EP 19910115617 EP19910115617 EP 19910115617 EP 91115617 A EP91115617 A EP 91115617A EP 0479010 B1 EP0479010 B1 EP 0479010B1
- Authority
- EP
- European Patent Office
- Prior art keywords
- containers
- container
- aseptic chamber
- filling
- arrangement according
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
Images
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B65—CONVEYING; PACKING; STORING; HANDLING THIN OR FILAMENTARY MATERIAL
- B65B—MACHINES, APPARATUS OR DEVICES FOR, OR METHODS OF, PACKAGING ARTICLES OR MATERIALS; UNPACKING
- B65B55/00—Preserving, protecting or purifying packages or package contents in association with packaging
- B65B55/02—Sterilising, e.g. of complete packages
- B65B55/027—Packaging in aseptic chambers
Definitions
- the aseptic chamber is designed as a tunnel extending in the longitudinal direction of the machine, through which the cup-like containers to be filled are transported by means of a chain.
- the entire tunnel interior must be continuously supplied with aseptic air in order to maintain a higher pressure in the filling chamber than in the preceding sterilization chamber and in the surroundings. The effort for operating such a device is therefore great.
- the object is achieved in a device of the type mentioned in that the lower boundary wall of the aseptic chamber is formed by the transport device, which is sealed on an annular wall of the housing, that the containers are inserted into holders of the transport device, and that the areas of the filling openings containing the Containers protrude through the transport device so that only this area and the interior of the containers are connected to the aseptic chamber.
- the housing containing the aseptic chamber is preferably hermetically sealed except for the container inlet and the container outlet. This leads to the advantage that the device can also be kept sufficiently clean outside the actual aseptic chamber. In particular, there is the advantage that both the aseptic chamber and the housing surrounding it can be subjected to a washing process from time to time which is used to sterilize the entire machine at periodic intervals, for example once a day.
- a, preferably the lower, boundary of the aseptic chamber is formed by the transport device itself, which is designed as a carrier that transports the containers.
- the transport device itself, which is designed as a carrier that transports the containers.
- the carrier a rotating step-by-step indexing table rotating about a vertical axis, the circumference of which is guided close to the housing surrounding it.
- Such a cycle table ensures, for example in comparison to a chain transport, an outer exact movement sequence and a high positioning accuracy.
- such a tactical table can be installed in a relatively limited space, so that a very compact design is created.
- the cycle table is expediently designed in the form of a disk and provided with holders which clamp the containers on the outer circumference. With such a configuration, additional coupling means for the containers can be dispensed with.
- the aseptic chamber is under atmospheric pressure. This reduces any sealing problems.
- the containers (3) After alignment in station (8), the containers (3) remain permanently clamped so that the orientation is no longer lost. This is done in that the container (3) is taken over and held by another pair of jaws in station (8), while the holding jaws (11 and 12) move back in the open state.
- the holding jaws (11, 12) can be moved alternately in the direction of the arrows (K and L), so that in each case a group of three containers (3) can be transported further in the direction of the arrow (B).
- Each holding jaw (11, 12) is in turn movable in the transverse direction, i.e. according to the arrow directions (M and N) or (P and Q).
- the station (8) for aligning the containers (3) is finally followed by a station (13), which is only indicated by dash-dotted lines in FIG. 2 and contains the devices, for example, about a closure piece (17) assigned to the filling opening (9) on the can lid (16) local seal and erect (see also Fig. 3).
- the closure piece a so-called pull tab, remains open and erected, so that the container (3) subsequently can be cleaned and filled.
- the pull tab is fed from a film roll, not shown, and cut off.
- the rails (23) are designed as tubes to which a washing system, which will be explained later, is connected.
- the transport unit (4) which in each case removes a group of three containers (3) from the housing (6) in the direction of the arrow (C), takes over the sterilized, filled and closed containers (3) from the cycle table (21). Further stations for possible additional work, for example signing, can be provided here.
- the container outlet is labeled (25).
- the transport unit (4) is also mechanically driven by the base machine (1), with all important movements of the individual stations being generated mechanically via cam mechanisms.
- the basic machine (1) which contains a base frame (26) for all mechanical drives, has the tact table (21), which has a total of three rows (81) (see FIG. 2) for the containers (3) to be treated.
- the multi-row tact table (21) is incremented. It is assigned a so-called lifting yoke (27) which has a plate (28) for holding tools, for example blowing nozzles (40) for hot air or filling heads (41) for liquid contents (see FIG. 1).
- An essential component of the housing (6) placed on the base machine (1) is an essentially circular aseptic chamber (29) which has a rectangular cross section with an upper boundary wall (75) through which the individual tools are guided.
- the lower boundary wall of the aseptic chamber (29) is formed by the tact table (21), which has the shape of a circular disc and is guided with its circumference close to the ring wall of the housing (6), which in this area also forms the ring wall of the aseptic chamber ( 29) forms.
- the aseptic chamber (29) thus consists in principle of the side walls and the roof of the housing (6) and a bottom, which through the tact table (21) and the inside of the sterilizing container (3) is formed.
- the aseptic chamber (29) is used for the actual sterilization of the relevant parts of the container (3) and is located in the housing (6), which in turn is largely hermetically sealed from the outside.
- the aseptic chamber (29) see FIGS. 1 and 3) only the can lids (16) penetrating the tact table (21) and the pull tabs (17) protrude (FIG. 3), ie the areas of the filling openings (9) preferably designed as cardboard boxes container (3). This means that only these parts of the exterior of the can need to be sterilized. A new introduction of germs is low with this arrangement.
- the inside of the container (3), the can lid (16) and the pull tabs (17) are sterilized in one go, ie no separate devices for sterilizing the closures (17) are necessary.
- the sterilization process takes place under atmospheric pressure.
- the described shape of the inside of the aseptic chamber (29) brings specific technical advantages.
- the heating of the surface of the container (3) required before sterilization can be carried out at a much lower temperature, since it is now possible to heat the container (3) from the inside with sterile hot air, but from the outside with conventional heating elements.
- the sterile hot air which heats the inside of the container (3), can be kept at a low temperature level since the heating is supported from the outside. Compared to conventional devices, the temperature was reduced by 80 ° to 120 ° Celsius.
- Containers (3) which are normally coated with polyester on the inside, are treated more gently in this way. In addition, expensive sterile air is saved.
- the housing (6) is provided with suction devices (36, 37, 38) (Fig. 1) which are connected both to the aseptic chamber (29) and to the areas above or below.
- a suction device (36) is also assigned to the area (74) of the housing (6) above the aseptic chamber (29).
- the tools for the individual 30 workstations (42 to 71) described below are mounted on the lifting yoke (27), which can be raised and lowered in the direction of the arrow (H and I), so that the tools can be delivered to the containers (3).
- the first station (42) of the cycle table (21) is assigned to the container inlet (18) and is used to insert a group of three (20) of containers (3) from below into the holders (24) of the cycle table (21).
- Each container (3) of the group of three (20) is assigned to a row (81).
- the subsequent stations (43 and 44) form a lock (33) between the zones (30 and 31) already described.
- An empty station (45) follows.
- the containers (3) are preheated with hot air, so that later on, when the container (3) is sterilized, too large drops do not form.
- steam is then generated from an aqueous solution of approx. 65 % Water and approx. 35% hydrogen peroxide is obtained and introduced into the interior of the containers (3) through the filling openings (9), the area of the containers (3) surrounding the filling opening (9) above the cycle table (21) also being sterilized becomes.
- An empty station (48) follows again.
- the eight subsequent stations (49 to 56) of the zone (31) serve to blow in hot air in order to dry the containers (3) completely.
- a blower for sterile air is located on the lock (34) between the zones (31, 32), at the stations (57, 58).
- the following zone (32) serves to fill and close the sterilized containers (3).
- Two filling heads (59, 61) are provided, with an empty station (60) in between, which is kept free for further customer requests.
- foam suction takes place, in the station (63), if desired, inert gas can be blown in.
- the subsequent stations (64, 65) are used for heat sealing and subsequent cold resealing of the individual pull tabs (17).
- An empty station (66) preferably follows.
- the stations (67, 68) again form a lock (35) between the zones (32 and 30). This is followed by the station (69) for discharging a group of three (20) of containers (3) from the tact table (21). This is done in that a stamp mounted in the lifting yoke (27) pushes the container (3) from above out of the holder (24 or 24 ') of the cycle table (21).
- the stations (70 and 71) can be provided for identifying the containers, for example the date or the like.
- Narrow gaps in the aseptic chamber (29) and the locks (33, 34 and 35) between the individual zones (30, 31, 32) of the aseptic chamber (29) keep in connection with the suction devices (36, 37, 38) and blower devices (39) maintain the flow conditions within the aseptic chamber (29) which are important for the sterility of the machine.
- additional sterile cooling air is supplied via a blower device, so that a slight overpressure arises compared to the remaining zones (30 and 31) and no contaminated atmosphere can get into the filling area.
- the amount of air required is only very small because of the relatively small cross section of the aseptic chamber (29) and the division into zones.
- a washing process is carried out for cleaning and sterilizing the entire machine.
- Various line systems are provided for this, for example a washing device (76) with blowing openings (not shown in more detail) and a sterile air device (72) with blowing devices (73) which are directed both into the aseptic chamber (29) and into the space (74) above it .
- the transport unit (2) and the transport unit (4) are automatically decoupled from the drive of the base machine (1), so that the openings for the container inlet (18) and the container outlet (25) can be hermetically closed. In this state, the machine is subjected to the washing process.
- the washing device consists of line systems (not shown in more detail) for supplying, shutting off and distributing the washing media and also heating devices.
- the device in the broader sense includes devices for extracting hot air, sterile air and devices for sterilizing and supplying the filling material, as well as devices for preparing and supplying and removing the washing media, which have not yet been described in more detail.
Landscapes
- Engineering & Computer Science (AREA)
- Mechanical Engineering (AREA)
- Filling Of Jars Or Cans And Processes For Cleaning And Sealing Jars (AREA)
- Basic Packing Technique (AREA)
Claims (12)
- Dispositif pour stériliser et remplir des récipients (3) présentant un couvercle (16) muni d'un orifice de remplissage (9), pour stériliser des pièces d'obturation (17) affectées aux orifices de remplissage (9), et pour obturer des orifices de remplissage (9) avec les pièces d'obturation (17), comportant une enveloppe (6), présentant un orifice d'entrée (18) dans le récipient et un orifice de sortie (25) dans le récipient, enveloppe qui contient au moins une chambre aseptique (29), à laquelle on peut amener les récipients (3) à l'aide d'un dispositif de transport (21), caractérisé en ce que la paroi limite inférieure de la chambre aseptique (29) est formée par le dispositif de transport (21), qui est guidé d'une manière étanche contre une paroi annulaire de l'enveloppe (6) ; que les récipients (3) sont introduits dans des fixations (24, 24') du dispositif de transport (21) ; et que les zones des récipients (3) contenant les orifices de remplissage (9) traversent le dispositif de transport (21) de façon que seule cette zone et l'intérieur des récipients (3) soient en communication avec la chambre aseptique (29).
- Dispositif selon la revendication 1, caractérisé en ce que l'enveloppe (6) contenant la chambre aseptique (29) est étanchée d'une manière hermétique jusqu'à l'orifice d'entrée (18) et l'orifice de sortie (25) des récipients.
- Dispositif selon la revendication 1 ou 2, caractérisé en ce que l'enveloppe (6) est cylindrique, et la poutre (21) est une table à cadences, à transfert intermittent, tournant autour d'un axe vertical, table dont la périphérie est guidée d'une manière étanche contre l'enveloppe (6) qui l'entoure.
- Dispositif selon la revendication 3, caractérisé en ce que la table à cadences est conçue comme un disque, et est pourvue de supports (24, 24'), qui serrent les récipients (3) contre la périphérie extérieure.
- Dispositif selon l'une des revendications 1 à 4, caractérisé en ce que la chambre aseptique (29) est subdivisée en zones (30, 31, 32) séparées par des sas (33, 34, 35) pour l'orifice d'entrée (18) des récipients et pour l'orifice de sortie (25) des récipients, pour la stérilisation ainsi que pour le remplissage et l'obturation des récipients (3).
- Dispositif selon l'une des revendications 1 à 5, caractérisé en ce que des outils (40, 41), disposés contre un joug de levage (27), ainsi que des dispositifs d'aspiration (37) et des dispositifs de ventilation (73), dépassent dans le volume intérieur de la chambre aseptique (29).
- Dispositif selon l'une des revendications 1 à 6, caractérisé en ce que la chambre aseptique (29) sert aussi à stériliser les obturations (17) affectées aux orifices de remplissage (9).
- Dispositif selon l'une des revendications 1 à 7, caractérisé en ce que plusieurs rangées (81) de récipients (3), disposées les unes à côté des autres, sont affectées à la chambre aseptique (29).
- Dispositif selon l'une des revendications 1 à 8, caractérisé en ce que la chambre aseptique (29) est sous la pression atmosphérique.
- Dispositif selon l'une des revendications 5 à 9, caractérisé en ce que les sas (33, 34, 35) sont configurés de façon qu'il y ait toujours un récipient (3) dans le sans (33, 34, 35).
- Dispositif selon l'une des revendications 1 à 10, caractérisé en ce que la chambre aseptique (29) est pour l'essentiel constituée d'une paroi de limitation supérieure (75), d'une paroi annulaire extérieure latérale d'une enveloppe (6), d'une paroi annulaire intérieure, ainsi que de la table à cadences (21) formant le fond, et de la face intérieure des récipients (3).
- Procédé pour stériliser et remplir des récipients comportant un couvercle muni d'orifices de remplissage, pour stériliser des pièces d'obturation affectées aux orifices de remplissage et pour obturer les orifices de remplissage à l'aide des pièces d'obturation, caractérisé en ce qu'on fixe au récipient la pièce d'obturation avant la stérilisation ; que, pour assurer simultanément la stérilisation du volume intérieur des récipients, du couvercle et de la pièce d'obturation, seule est introduite dans une chambre aseptique la zone du récipient contenant l'orifice de remplissage ; et que la pièce d'obturation, après remplissage du récipient, est scellée dans la chambre aseptique pour obturer l'orifice de remplissage à l'aide du couvercle.
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
DE4031472A DE4031472C2 (de) | 1990-10-05 | 1990-10-05 | Vorrichtung zum Sterilisieren, Füllen und Verschließen von eine Füllöffnung aufweisenden Behältern |
DE4031472 | 1990-10-05 |
Publications (2)
Publication Number | Publication Date |
---|---|
EP0479010A1 EP0479010A1 (fr) | 1992-04-08 |
EP0479010B1 true EP0479010B1 (fr) | 1996-10-30 |
Family
ID=6415603
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
EP19910115617 Expired - Lifetime EP0479010B1 (fr) | 1990-10-05 | 1991-09-14 | Dispositif et procédé de stérilisation, de remplissage et de fermeture d'une ouverture de remplissage |
Country Status (4)
Country | Link |
---|---|
EP (1) | EP0479010B1 (fr) |
DE (2) | DE4031472C2 (fr) |
DK (1) | DK0479010T3 (fr) |
FI (1) | FI94331C (fr) |
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US11993414B2 (en) | 2021-12-13 | 2024-05-28 | Boomerang Water, Llc | Cleaning, filling, and capping containers |
Families Citing this family (27)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE4137098C2 (de) * | 1991-11-12 | 1996-06-05 | Tetra Pak Gmbh | Vorrichtung zum Verstellen des Aufnahmevolumens eines Gutträgers |
DE4224003A1 (de) * | 1992-07-21 | 1994-01-27 | Tetra Pak Gmbh | Vorrichtung zum Füllen und Verschließen von Fließmittelpackungen |
DE4305478A1 (de) * | 1993-02-23 | 1994-08-25 | Tetra Laval Holdings & Finance | Verfahren und Vorrichtung zum Sterilisieren von Packungen |
DE4314932A1 (de) * | 1993-05-06 | 1994-11-10 | Hamba Maschf | Becherfüllwerk für dünnflüssige bis pasteuse Molkerei- und Fettprodukte |
RU2140383C1 (ru) * | 1994-03-02 | 1999-10-27 | Ти-Эл Системз Корпорейшн | Устройство для наполнения фармацевтических емкостей (варианты) |
USRE38747E1 (en) | 1994-03-02 | 2005-06-28 | Robert Bosch Packaging Technology, Inc. | Vial filling apparatus |
DE19503458B4 (de) * | 1995-02-03 | 2007-10-31 | Rüdiger Haaga GmbH | Vorrichtung zum Verschließen einer Füllöffnung |
DE19504558C2 (de) * | 1995-02-11 | 1997-05-07 | Pkl Verpackungssysteme Gmbh | Vorrichtung zum Sterilisieren bei der Abfüllung vorzugsweiser flüssiger Lebensmittel in Packungsbehälter |
DE19533462A1 (de) * | 1995-09-09 | 1997-03-13 | Ruediger Haaga Gmbh | Vorrichtung zum Füllen von Behältern mit einer zu Schaumbildung neigenden Flüssigkeit |
IT1286071B1 (it) * | 1996-10-30 | 1998-07-07 | Oflame S R L | Macchina intubettatrice con regolazione automatica per la lavorazione di tubetti aventi lunghezze differenti |
US6484479B1 (en) * | 2000-04-10 | 2002-11-26 | Tetra Laval Holdings & Finance, Sa | Form, fill and seal apparatus with cavity bar |
DE10045064A1 (de) * | 2000-09-12 | 2002-03-28 | Tetra Laval Holdings & Finance | Vorwärmaufbau für einen Linearfüller |
DE10261706B4 (de) * | 2002-12-30 | 2005-01-05 | Sig Technology Ltd. | Füllmaschine und Verfahren zum Abfüllen von Lebensmitteln |
DE102004055784B3 (de) * | 2004-11-18 | 2006-04-27 | Sig Technology Ag | Vorrichtung und Verfahren zur laminaren Sterilluftzuführung während der Sterilisation und/oder aseptischen Befüllung |
DE102004055783A1 (de) * | 2004-11-18 | 2006-05-24 | Sig Technology Ag | Verfahren und Vorrichtung zum Sterilisieren kontinuierlich transportierter Behälter |
DE102005047427B3 (de) * | 2005-09-30 | 2006-12-28 | Sig Technology Ag | Vorrichtung zum Sterilisieren kontinuierlich hintereinander transportierter Behälter |
ATE396952T1 (de) † | 2005-11-16 | 2008-06-15 | Arol Spa | Vorrichtung und verfahren zum verschliessen von behältern |
DE102007001970A1 (de) * | 2007-01-13 | 2008-07-17 | Khs Ag | Verfahren und Vorrichtung zur Sterilisation von Behältern aus Metall |
DE102008018516A1 (de) * | 2008-04-12 | 2009-10-15 | Krones Ag | Vorrichtung zum Befüllen von Behältnissen |
DE102009007138A1 (de) | 2009-02-02 | 2010-08-05 | Krones Ag | Vorrichtung und Verfahren zum Behandeln von Behältnissen |
DE102010000501B4 (de) * | 2010-02-22 | 2021-05-27 | Krones Aktiengesellschaft | Behälterformungs- und Behälterbehandlungsanlage |
DE102010054788A1 (de) | 2010-12-16 | 2012-06-21 | Krones Aktiengesellschaft | Vorrichtung zum Sterilisieren von Behältnissen |
US20130091805A1 (en) * | 2011-10-14 | 2013-04-18 | Applied Silicone Corporation | System and method for curing, sterilization and aseptic packaging of medical devices |
CN104071363A (zh) * | 2014-07-04 | 2014-10-01 | 海南通用康力制药有限公司 | 注射用精氨酸阿司匹林粉针剂的分装流程及其自动分装系统 |
CN104445014B (zh) * | 2014-11-25 | 2016-08-24 | 镇江市顶智微电子科技有限公司 | 一种灌装瓶纠正推挤涮洗递进输送灌装系统 |
DE102015116534A1 (de) | 2015-07-23 | 2017-01-26 | Sig Technology Ag | Verfahren zum Sterilisieren von verpackten oder teilverpackten bzw. teilweise verschlossenen Gebrauchsgütern sowie dazu verwendbare Sammelbehälter und Umverpackungen |
WO2023114220A2 (fr) * | 2021-12-13 | 2023-06-22 | Boomerang Water, Llc | Conteneurs de nettoyage, de remplissage et de coiffage |
Family Cites Families (15)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US2575863A (en) * | 1948-03-09 | 1951-11-20 | Continental Can Co | Method of aseptic canning |
US2660513A (en) * | 1949-06-30 | 1953-11-24 | Ball Charles Olin | Method of sterilizing glass containers |
US2885845A (en) * | 1956-03-21 | 1959-05-12 | W F And John Barnes Company | Method and apparatus for aseptically canning |
US3018184A (en) * | 1958-12-23 | 1962-01-23 | Martin William Mck | Aseptic canning process and apparatus |
CH426602A (de) * | 1961-12-18 | 1966-12-15 | Owens Illinois Glass Co | Verfahren zur Gegendruckabfüllung heisser flüssiger oder pastöser Nahrungsmittel in Behälte und Einrichtung zur Durchführung des Verfahrens |
FR1592063A (fr) * | 1966-11-22 | 1970-05-11 | ||
SE423517B (sv) * | 1972-08-11 | 1982-05-10 | Tetra Pak Dev | Sett att under aseptiska betingelser forpacka sterilt fyllgods i behallare |
SE7311516L (fr) * | 1973-08-24 | 1975-02-25 | Tetra Pak Dev | |
US4296068A (en) * | 1979-02-19 | 1981-10-20 | Dai Nippon Insatsu Kabushiki Kaisha | Apparatus for sterilizing a succession of food containers or the like |
US4458734A (en) * | 1982-01-29 | 1984-07-10 | Scholle Corporation | Apparatus and method for aseptically filling a container |
DE3522996A1 (de) * | 1985-06-27 | 1987-01-08 | Kolbus Gmbh & Co Kg | Verfahren zur abgrenzung steriler raeume gegen austreten von toxischen sterilisationsmitteln oder eindringen von mikroorganismen, vorzugsweise in anwendung fuer fuellmaschinen, und vorrichtung zur durchfuehrung des verfahrens |
DE3816754A1 (de) * | 1987-05-14 | 1988-12-01 | Ammann Siegfried | Vorrichtung zum abfuellen von fluessigen medien in behaelter |
DE3809855A1 (de) * | 1987-08-01 | 1989-02-09 | Seitz Enzinger Noll Masch | Verfahren zum aseptischen bzw. sterilen abfuellen von fluessigem fuellgut in behaelter sowie vorrichtung zum durchfuehren dieses verfahrens |
DE8814813U1 (fr) * | 1988-11-29 | 1989-01-12 | Abel Gmbh & Co Abfuell- Und Pumpentechnik, 2059 Buechen, De | |
FI895421A0 (fi) * | 1989-07-10 | 1989-11-14 | Yhtyneet Paperitehtaat Oy | Foerfarande foer utformande av foerpackning. |
-
1990
- 1990-10-05 DE DE4031472A patent/DE4031472C2/de not_active Expired - Fee Related
-
1991
- 1991-09-14 EP EP19910115617 patent/EP0479010B1/fr not_active Expired - Lifetime
- 1991-09-14 DE DE59108313T patent/DE59108313D1/de not_active Expired - Fee Related
- 1991-09-14 DK DK91115617T patent/DK0479010T3/da active
- 1991-10-04 FI FI914671A patent/FI94331C/fi active
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US11993414B2 (en) | 2021-12-13 | 2024-05-28 | Boomerang Water, Llc | Cleaning, filling, and capping containers |
Also Published As
Publication number | Publication date |
---|---|
EP0479010A1 (fr) | 1992-04-08 |
FI94331B (fi) | 1995-05-15 |
FI914671A (fi) | 1992-04-06 |
FI914671A0 (fi) | 1991-10-04 |
DE4031472A1 (de) | 1992-04-09 |
FI94331C (fi) | 1995-08-25 |
DE59108313D1 (de) | 1996-12-05 |
DK0479010T3 (da) | 1996-11-25 |
DE4031472C2 (de) | 2001-06-28 |
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