EA009436B1 - Сцинтилляционное вещество (варианты) - Google Patents

Сцинтилляционное вещество (варианты) Download PDF

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Publication number
EA009436B1
EA009436B1 EA200600835A EA200600835A EA009436B1 EA 009436 B1 EA009436 B1 EA 009436B1 EA 200600835 A EA200600835 A EA 200600835A EA 200600835 A EA200600835 A EA 200600835A EA 009436 B1 EA009436 B1 EA 009436B1
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EA
Eurasian Patent Office
Prior art keywords
composition
scintillation
crystal
substance
cerium
Prior art date
Application number
EA200600835A
Other languages
English (en)
Russian (ru)
Other versions
EA200600835A1 (ru
Inventor
Александр Иосифович Загуменный
Сергей Александрович Кутовой
Юрий Дмитриевич Заварцев
Original Assignee
Зекотек Медикэл Системс Инк.
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Publication date
Application filed by Зекотек Медикэл Системс Инк. filed Critical Зекотек Медикэл Системс Инк.
Publication of EA200600835A1 publication Critical patent/EA200600835A1/ru
Publication of EA009436B1 publication Critical patent/EA009436B1/ru

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    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B35/00—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
    • C04B35/01—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics
    • C04B35/16—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics based on silicates other than clay
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09K—MATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
    • C09K11/00—Luminescent, e.g. electroluminescent, chemiluminescent materials
    • C09K11/08—Luminescent, e.g. electroluminescent, chemiluminescent materials containing inorganic luminescent materials
    • C09K11/77—Luminescent, e.g. electroluminescent, chemiluminescent materials containing inorganic luminescent materials containing rare earth metals
    • C09K11/7766—Luminescent, e.g. electroluminescent, chemiluminescent materials containing inorganic luminescent materials containing rare earth metals containing two or more rare earth metals
    • C09K11/77742—Silicates
    • C—CHEMISTRY; METALLURGY
    • C30—CRYSTAL GROWTH
    • C30B—SINGLE-CRYSTAL GROWTH; UNIDIRECTIONAL SOLIDIFICATION OF EUTECTIC MATERIAL OR UNIDIRECTIONAL DEMIXING OF EUTECTOID MATERIAL; REFINING BY ZONE-MELTING OF MATERIAL; PRODUCTION OF A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; SINGLE CRYSTALS OR HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; AFTER-TREATMENT OF SINGLE CRYSTALS OR A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; APPARATUS THEREFOR
    • C30B11/00—Single-crystal growth by normal freezing or freezing under temperature gradient, e.g. Bridgman-Stockbarger method
    • C—CHEMISTRY; METALLURGY
    • C30—CRYSTAL GROWTH
    • C30B—SINGLE-CRYSTAL GROWTH; UNIDIRECTIONAL SOLIDIFICATION OF EUTECTIC MATERIAL OR UNIDIRECTIONAL DEMIXING OF EUTECTOID MATERIAL; REFINING BY ZONE-MELTING OF MATERIAL; PRODUCTION OF A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; SINGLE CRYSTALS OR HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; AFTER-TREATMENT OF SINGLE CRYSTALS OR A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; APPARATUS THEREFOR
    • C30B15/00—Single-crystal growth by pulling from a melt, e.g. Czochralski method
    • C—CHEMISTRY; METALLURGY
    • C30—CRYSTAL GROWTH
    • C30B—SINGLE-CRYSTAL GROWTH; UNIDIRECTIONAL SOLIDIFICATION OF EUTECTIC MATERIAL OR UNIDIRECTIONAL DEMIXING OF EUTECTOID MATERIAL; REFINING BY ZONE-MELTING OF MATERIAL; PRODUCTION OF A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; SINGLE CRYSTALS OR HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; AFTER-TREATMENT OF SINGLE CRYSTALS OR A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; APPARATUS THEREFOR
    • C30B29/00—Single crystals or homogeneous polycrystalline material with defined structure characterised by the material or by their shape
    • C30B29/10—Inorganic compounds or compositions
    • C30B29/34—Silicates
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
    • C04B2235/30—Constituents and secondary phases not being of a fibrous nature
    • C04B2235/32—Metal oxides, mixed metal oxides, or oxide-forming salts thereof, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
    • C04B2235/3201—Alkali metal oxides or oxide-forming salts thereof
    • C04B2235/3203—Lithium oxide or oxide-forming salts thereof
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
    • C04B2235/30—Constituents and secondary phases not being of a fibrous nature
    • C04B2235/32—Metal oxides, mixed metal oxides, or oxide-forming salts thereof, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
    • C04B2235/3205—Alkaline earth oxides or oxide forming salts thereof, e.g. beryllium oxide
    • C04B2235/3208—Calcium oxide or oxide-forming salts thereof, e.g. lime
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
    • C04B2235/30—Constituents and secondary phases not being of a fibrous nature
    • C04B2235/32—Metal oxides, mixed metal oxides, or oxide-forming salts thereof, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
    • C04B2235/3224—Rare earth oxide or oxide forming salts thereof, e.g. scandium oxide
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
    • C04B2235/30—Constituents and secondary phases not being of a fibrous nature
    • C04B2235/32—Metal oxides, mixed metal oxides, or oxide-forming salts thereof, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
    • C04B2235/3224—Rare earth oxide or oxide forming salts thereof, e.g. scandium oxide
    • C04B2235/3225—Yttrium oxide or oxide-forming salts thereof
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
    • C04B2235/30—Constituents and secondary phases not being of a fibrous nature
    • C04B2235/32—Metal oxides, mixed metal oxides, or oxide-forming salts thereof, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
    • C04B2235/3224—Rare earth oxide or oxide forming salts thereof, e.g. scandium oxide
    • C04B2235/3227—Lanthanum oxide or oxide-forming salts thereof
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
    • C04B2235/30—Constituents and secondary phases not being of a fibrous nature
    • C04B2235/32—Metal oxides, mixed metal oxides, or oxide-forming salts thereof, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
    • C04B2235/3224—Rare earth oxide or oxide forming salts thereof, e.g. scandium oxide
    • C04B2235/3229—Cerium oxides or oxide-forming salts thereof

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  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Organic Chemistry (AREA)
  • Materials Engineering (AREA)
  • Metallurgy (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Ceramic Engineering (AREA)
  • Manufacturing & Machinery (AREA)
  • Structural Engineering (AREA)
  • Luminescent Compositions (AREA)
  • Crystals, And After-Treatments Of Crystals (AREA)
  • Measurement Of Radiation (AREA)
EA200600835A 2003-11-04 2004-03-12 Сцинтилляционное вещество (варианты) EA009436B1 (ru)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
RU2003132127/15A RU2242545C1 (ru) 2003-11-04 2003-11-04 Сцинтиляционное вещество (варианты)
PCT/RU2004/000094 WO2005042812A1 (en) 2003-11-04 2004-03-12 Scintillation substances (variants)

Publications (2)

Publication Number Publication Date
EA200600835A1 EA200600835A1 (ru) 2007-02-27
EA009436B1 true EA009436B1 (ru) 2007-12-28

Family

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Family Applications (1)

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EA200600835A EA009436B1 (ru) 2003-11-04 2004-03-12 Сцинтилляционное вещество (варианты)

Country Status (10)

Country Link
EP (1) EP1689916B1 (enExample)
JP (1) JP4115503B2 (enExample)
CN (1) CN100436660C (enExample)
AT (1) ATE417145T1 (enExample)
AU (1) AU2004286178B2 (enExample)
CA (1) CA2555754C (enExample)
DE (1) DE602004018378D1 (enExample)
EA (1) EA009436B1 (enExample)
RU (1) RU2242545C1 (enExample)
WO (1) WO2005042812A1 (enExample)

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2015152773A1 (ru) * 2014-04-03 2015-10-08 Георгий Алексеевич ДОСОВИЦКИЙ Способ получения люминесцентных силикатных стекол и композитов
RU2693875C1 (ru) * 2018-04-05 2019-07-08 Сергей Александрович Кутовой Химическое соединение на основе оксиортосиликатов, содержащих иттрий и скандий, для квантовой электроники

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FR2874021B1 (fr) * 2004-08-09 2006-09-29 Saint Gobain Cristaux Detecteu Materiau scintillateur dense et rapide a faible luminescence retardee
PT103200B (pt) * 2004-09-30 2006-08-24 Taguspark-Soc. Prom.Desenv.Parq.Ci.Tec.Area Lisboa Sistema de tomografia por emissão de positrões (pet)
US7238302B2 (en) * 2004-12-28 2007-07-03 Osram Sylvania Inc. Single-component, UV-emitting phosphor
JP4682718B2 (ja) * 2005-06-28 2011-05-11 日立化成工業株式会社 無機シンチレータ
CZ298519B6 (cs) * 2006-01-09 2007-10-24 Crytur S. R. O. Monokrystal LYGSO: Ce, využitelný pro výrobu scintilacních detektoru a zpusob jejich výroby
JP5049336B2 (ja) * 2006-03-21 2012-10-17 コーニンクレッカ フィリップス エレクトロニクス エヌ ヴィ エレクトロルミネセントデバイス
RU2315136C1 (ru) * 2006-05-05 2008-01-20 Александр Николаевич Анненков Сцинтилляционное вещество в виде кристаллического соединения на основе силиката
JP5055910B2 (ja) * 2006-06-02 2012-10-24 日立化成工業株式会社 単結晶の熱処理方法
JP5027463B2 (ja) * 2006-09-06 2012-09-19 株式会社日立製作所 画像表示装置
RU2459855C2 (ru) * 2007-02-06 2012-08-27 Конинклейке Филипс Электроникс Н.В. Люминесцентные материалы красного свечения
RU2357025C2 (ru) * 2007-03-26 2009-05-27 Александр Николаевич Анненков Сцинтилляционное вещество в виде кристаллического соединения на основе силиката
TW200930849A (en) * 2007-10-23 2009-07-16 Saint Gobain Ceramics & Plastics Inc Scintillator crystals and methods of forming
WO2009083852A2 (en) * 2007-12-21 2009-07-09 Koninklijke Philips Electronics N.V. Radiation-sensitive detector with a scintillator in a composite resin
DE102009030205A1 (de) * 2009-06-24 2010-12-30 Litec-Lp Gmbh Leuchtstoffe mit Eu(II)-dotierten silikatischen Luminophore
JP5655141B2 (ja) * 2010-07-19 2015-01-14 オーシャンズ キング ライティング サイエンスアンドテクノロジー カンパニー リミテッド 珪酸塩発光材料及びその調製方法
RU2466428C2 (ru) * 2010-08-17 2012-11-10 Учреждение Российской академии наук Институт синтетических полимерных материалов им. Н.С. Ениколопова РАН (ИСПМ РАН) Металлосодержащий пластмассовый сцинтиллятор
US20120061577A1 (en) 2010-09-14 2012-03-15 Zecotek Imaging Systems Pte. Ltd. Depth-of-interaction scintillation detectors
US20130207002A1 (en) * 2010-10-22 2013-08-15 Koninklijke Philips Electronics N.V. Luminescent material and light emitting device comprising such luminescent material
WO2012066425A2 (en) 2010-11-16 2012-05-24 Saint-Gobain Cristaux Et Detecteurs Scintillation compound including a rare earth element and a process of forming the same
JPWO2012137738A1 (ja) * 2011-04-04 2014-07-28 株式会社トクヤマ シンチレーター、放射線検出装置および放射線検出方法
US20140061537A1 (en) * 2012-04-13 2014-03-06 Zecotek Imaging Systems Singapore Pte Ltd Multi-doped lutetium based oxyorthosilicate scintillators having improved photonic properties
CN104271706A (zh) * 2012-05-08 2015-01-07 海洋王照明科技股份有限公司 核壳结构的硅酸盐发光材料及其制备方法
RU2564038C1 (ru) * 2014-04-03 2015-09-27 Общество с ограниченной ответственностью"НеоСцинт" Сцинтилляционное вещество
CN103951206B (zh) * 2014-05-08 2016-05-04 宁波大学 稀土离子掺杂的BaGdBr5微晶玻璃及其制备方法
WO2015185988A1 (en) * 2014-06-03 2015-12-10 Zecotek Imaging Systems Singapore Pte. Ltd Cerium doped rare-earth ortosilicate materials having defects for improvement or scintillation parameters
RU2579135C1 (ru) * 2014-12-09 2016-03-27 Федеральное государственное бюджетное учреждение науки Институт химии твердого тела Уральского Отделения РАН Силикат редкоземельных элементов в наноаморфном состоянии
WO2016135040A1 (en) 2015-02-26 2016-09-01 Saint-Gobain Cristaux & Détecteurs Scintillation crystal including a co-doped rare earth silicate, a radiation detection apparatus including the scintillation crystal, and a process of forming the same
CN105986320A (zh) * 2016-02-16 2016-10-05 安徽火天晶体科技有限公司 Sc,Ce共掺杂的硅酸镥、硅酸钇镥晶体及其熔体法生长方法
JP6451700B2 (ja) * 2016-06-29 2019-01-16 住友金属鉱山株式会社 酸化物単結晶の育成方法
RU2627573C1 (ru) * 2016-09-02 2017-08-08 Федеральное государственное бюджетное учреждение "Национальный исследовательский центр "Курчатовский институт" Сцинтилляционный материал для регистрации ионизирующего излучения (варианты)
CN108059957A (zh) * 2016-11-07 2018-05-22 上海新漫晶体材料科技有限公司 阴阳离子共掺杂高光输出低余辉闪烁体材料
CN108585853B (zh) * 2017-12-11 2021-12-24 上海大学 一种铕掺杂氧化钪闪烁体及其制备方法和用途
CN110629287A (zh) * 2019-10-23 2019-12-31 安徽工业大学 一种铈掺杂钽铌酸镧闪烁晶体材料及其制备方法
JP7361908B2 (ja) * 2019-10-28 2023-10-16 サン－ゴバン セラミックス アンド プラスティクス，インコーポレイティド 残光を低減するための多価カチオンを含むＣｓＩ（Ｔｌ）シンチレータ結晶、及びシンチレーション結晶を含む放射線検出装置
CN112390278B (zh) * 2020-11-16 2022-02-08 中国科学院上海硅酸盐研究所 一种强吸电子元素掺杂稀土正硅酸盐闪烁材料及其制备方法和应用
CN117107358A (zh) * 2023-10-07 2023-11-24 眉山博雅新材料股份有限公司 一种闪烁晶体及其生长方法、生长装置

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2015152773A1 (ru) * 2014-04-03 2015-10-08 Георгий Алексеевич ДОСОВИЦКИЙ Способ получения люминесцентных силикатных стекол и композитов
RU2693875C1 (ru) * 2018-04-05 2019-07-08 Сергей Александрович Кутовой Химическое соединение на основе оксиортосиликатов, содержащих иттрий и скандий, для квантовой электроники

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Publication number Publication date
JP4115503B2 (ja) 2008-07-09
EA200600835A1 (ru) 2007-02-27
WO2005042812A1 (en) 2005-05-12
ATE417145T1 (de) 2008-12-15
CA2555754C (en) 2009-06-02
AU2004286178A1 (en) 2005-05-12
EP1689916A4 (en) 2008-02-27
DE602004018378D1 (de) 2009-01-22
CN1902341A (zh) 2007-01-24
JP2007514631A (ja) 2007-06-07
CA2555754A1 (en) 2005-05-12
AU2004286178B2 (en) 2008-11-13
EP1689916A1 (en) 2006-08-16
CN100436660C (zh) 2008-11-26
RU2242545C1 (ru) 2004-12-20
EP1689916B1 (en) 2008-12-10

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