EA200600835A1 - Сцинтилляционное вещество (варианты) - Google Patents

Сцинтилляционное вещество (варианты)

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Publication number
EA200600835A1
EA200600835A1 EA200600835A EA200600835A EA200600835A1 EA 200600835 A1 EA200600835 A1 EA 200600835A1 EA 200600835 A EA200600835 A EA 200600835A EA 200600835 A EA200600835 A EA 200600835A EA 200600835 A1 EA200600835 A1 EA 200600835A1
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EA
Eurasian Patent Office
Prior art keywords
units
value
exceeding
ray
scintillating
Prior art date
Application number
EA200600835A
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English (en)
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EA009436B1 (ru
Inventor
Александр Иосифович Загуменный
Юрий Дмитриевич Заварцев
Сергей Александрович Кутовой
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Зекотек Медикэл Системс Инк.
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Publication of EA200600835A1 publication Critical patent/EA200600835A1/ru
Publication of EA009436B1 publication Critical patent/EA009436B1/ru

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    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B35/00—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
    • C04B35/01—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics
    • C04B35/16—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics based on silicates other than clay
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09K—MATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
    • C09K11/00—Luminescent, e.g. electroluminescent, chemiluminescent materials
    • C09K11/08—Luminescent, e.g. electroluminescent, chemiluminescent materials containing inorganic luminescent materials
    • C09K11/77—Luminescent, e.g. electroluminescent, chemiluminescent materials containing inorganic luminescent materials containing rare earth metals
    • C09K11/7766—Luminescent, e.g. electroluminescent, chemiluminescent materials containing inorganic luminescent materials containing rare earth metals containing two or more rare earth metals
    • C09K11/77742—Silicates
    • C—CHEMISTRY; METALLURGY
    • C30—CRYSTAL GROWTH
    • C30B—SINGLE-CRYSTAL GROWTH; UNIDIRECTIONAL SOLIDIFICATION OF EUTECTIC MATERIAL OR UNIDIRECTIONAL DEMIXING OF EUTECTOID MATERIAL; REFINING BY ZONE-MELTING OF MATERIAL; PRODUCTION OF A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; SINGLE CRYSTALS OR HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; AFTER-TREATMENT OF SINGLE CRYSTALS OR A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; APPARATUS THEREFOR
    • C30B11/00—Single-crystal growth by normal freezing or freezing under temperature gradient, e.g. Bridgman-Stockbarger method
    • C—CHEMISTRY; METALLURGY
    • C30—CRYSTAL GROWTH
    • C30B—SINGLE-CRYSTAL GROWTH; UNIDIRECTIONAL SOLIDIFICATION OF EUTECTIC MATERIAL OR UNIDIRECTIONAL DEMIXING OF EUTECTOID MATERIAL; REFINING BY ZONE-MELTING OF MATERIAL; PRODUCTION OF A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; SINGLE CRYSTALS OR HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; AFTER-TREATMENT OF SINGLE CRYSTALS OR A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; APPARATUS THEREFOR
    • C30B15/00—Single-crystal growth by pulling from a melt, e.g. Czochralski method
    • C—CHEMISTRY; METALLURGY
    • C30—CRYSTAL GROWTH
    • C30B—SINGLE-CRYSTAL GROWTH; UNIDIRECTIONAL SOLIDIFICATION OF EUTECTIC MATERIAL OR UNIDIRECTIONAL DEMIXING OF EUTECTOID MATERIAL; REFINING BY ZONE-MELTING OF MATERIAL; PRODUCTION OF A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; SINGLE CRYSTALS OR HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; AFTER-TREATMENT OF SINGLE CRYSTALS OR A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; APPARATUS THEREFOR
    • C30B29/00—Single crystals or homogeneous polycrystalline material with defined structure characterised by the material or by their shape
    • C30B29/10—Inorganic compounds or compositions
    • C30B29/34—Silicates
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
    • C04B2235/30—Constituents and secondary phases not being of a fibrous nature
    • C04B2235/32—Metal oxides, mixed metal oxides, or oxide-forming salts thereof, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
    • C04B2235/3201—Alkali metal oxides or oxide-forming salts thereof
    • C04B2235/3203—Lithium oxide or oxide-forming salts thereof
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    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
    • C04B2235/30—Constituents and secondary phases not being of a fibrous nature
    • C04B2235/32—Metal oxides, mixed metal oxides, or oxide-forming salts thereof, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
    • C04B2235/3205—Alkaline earth oxides or oxide forming salts thereof, e.g. beryllium oxide
    • C04B2235/3208—Calcium oxide or oxide-forming salts thereof, e.g. lime
    • C—CHEMISTRY; METALLURGY
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    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
    • C04B2235/30—Constituents and secondary phases not being of a fibrous nature
    • C04B2235/32—Metal oxides, mixed metal oxides, or oxide-forming salts thereof, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
    • C04B2235/3224—Rare earth oxide or oxide forming salts thereof, e.g. scandium oxide
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    • C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
    • C04B2235/30—Constituents and secondary phases not being of a fibrous nature
    • C04B2235/32—Metal oxides, mixed metal oxides, or oxide-forming salts thereof, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
    • C04B2235/3224—Rare earth oxide or oxide forming salts thereof, e.g. scandium oxide
    • C04B2235/3225—Yttrium oxide or oxide-forming salts thereof
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
    • C04B2235/30—Constituents and secondary phases not being of a fibrous nature
    • C04B2235/32—Metal oxides, mixed metal oxides, or oxide-forming salts thereof, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
    • C04B2235/3224—Rare earth oxide or oxide forming salts thereof, e.g. scandium oxide
    • C04B2235/3227—Lanthanum oxide or oxide-forming salts thereof
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
    • C04B2235/30—Constituents and secondary phases not being of a fibrous nature
    • C04B2235/32—Metal oxides, mixed metal oxides, or oxide-forming salts thereof, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
    • C04B2235/3224—Rare earth oxide or oxide forming salts thereof, e.g. scandium oxide
    • C04B2235/3229—Cerium oxides or oxide-forming salts thereof

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  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Organic Chemistry (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Metallurgy (AREA)
  • Inorganic Chemistry (AREA)
  • Ceramic Engineering (AREA)
  • Manufacturing & Machinery (AREA)
  • Structural Engineering (AREA)
  • Luminescent Compositions (AREA)
  • Crystals, And After-Treatments Of Crystals (AREA)
  • Measurement Of Radiation (AREA)

Abstract

Изобретение относится к сцинтилляционным материалам и может быть использовано в ядерной физике, медицине и нефтяной промышленности для регистрации и измерения рентгеновского, гамма- и альфа-излучений; неразрушающего контроля структуры твердых тел; трехмерной позитрон-электронной и рентгеновской компьютерной томографии и флюорографии. Сцинтилляционные вещества на основе силиката, содержащего лютеций Lu и церий Се, имеют состав, который выражается химическими формуламиCeLiSiO,CeLiLuASiO,CeLiLudASiO,где А - по крайней мере один из элементов группы Gd, Sc, Y, La, Eu, Tb; x - от 1х10ф.ед. до 0,02 ф.ед, y - от 0,024 ф.ед. до 0,09 ф.ед, z не более чем 0,05 ф.ед; q не более чем 0,2 ф.ед, р не более чем 0,05 ф.ед.CeLiLuASiO,z не более чем 8,9 ф.ед. Получаемые сцинтилляционные вещества обладают большой плотностью, высоким световым выходом, малым временем послесвечения и малым процентом потерь при изготовлении сцинтилляционных элементов для трехмерных томографов (PET).
EA200600835A 2003-11-04 2004-03-12 Сцинтилляционное вещество (варианты) EA009436B1 (ru)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
RU2003132127/15A RU2242545C1 (ru) 2003-11-04 2003-11-04 Сцинтиляционное вещество (варианты)
PCT/RU2004/000094 WO2005042812A1 (en) 2003-11-04 2004-03-12 Scintillation substances (variants)

Publications (2)

Publication Number Publication Date
EA200600835A1 true EA200600835A1 (ru) 2007-02-27
EA009436B1 EA009436B1 (ru) 2007-12-28

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EP (1) EP1689916B1 (ru)
JP (1) JP4115503B2 (ru)
CN (1) CN100436660C (ru)
AT (1) ATE417145T1 (ru)
AU (1) AU2004286178B2 (ru)
CA (1) CA2555754C (ru)
DE (1) DE602004018378D1 (ru)
EA (1) EA009436B1 (ru)
RU (1) RU2242545C1 (ru)
WO (1) WO2005042812A1 (ru)

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JP5055910B2 (ja) * 2006-06-02 2012-10-24 日立化成工業株式会社 単結晶の熱処理方法
JP5027463B2 (ja) * 2006-09-06 2012-09-19 株式会社日立製作所 画像表示装置
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US20090136731A1 (en) * 2007-10-23 2009-05-28 Saint-Gobain Ceramics & Plastics, Inc. Scintillator crystals and methods of forming
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EP2597133B1 (en) * 2010-07-19 2016-12-07 Ocean's King Lighting Science&Technology Co., Ltd. Luminescent material of silicate and preparing method thereof
RU2466428C2 (ru) * 2010-08-17 2012-11-10 Учреждение Российской академии наук Институт синтетических полимерных материалов им. Н.С. Ениколопова РАН (ИСПМ РАН) Металлосодержащий пластмассовый сцинтиллятор
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JP5926449B2 (ja) * 2012-05-08 2016-05-25 ▲海▼洋王照明科技股▲ふん▼有限公司 コア−シェル構造のケイ酸塩発光材料およびその製造方法
RU2564038C1 (ru) * 2014-04-03 2015-09-27 Общество с ограниченной ответственностью"НеоСцинт" Сцинтилляционное вещество
RU2564037C1 (ru) * 2014-04-03 2015-09-27 Общество с ограниченной ответственностью "НеоСцинт" Способ стабилизации редкоземельных ионов в трехвалентном состоянии в силикатных стеклах и композитах
CN103951206B (zh) * 2014-05-08 2016-05-04 宁波大学 稀土离子掺杂的BaGdBr5微晶玻璃及其制备方法
WO2015185988A1 (en) * 2014-06-03 2015-12-10 Zecotek Imaging Systems Singapore Pte. Ltd Cerium doped rare-earth ortosilicate materials having defects for improvement or scintillation parameters
RU2579135C1 (ru) * 2014-12-09 2016-03-27 Федеральное государственное бюджетное учреждение науки Институт химии твердого тела Уральского Отделения РАН Силикат редкоземельных элементов в наноаморфном состоянии
US10274616B2 (en) 2015-02-26 2019-04-30 Saint-Gobain Cristaux & Detecteurs Scintillation crystal including a co-doped rare earth silicate, a radiation detection apparatus including the scintillation crystal, and a process of forming the same
CN105986320A (zh) * 2016-02-16 2016-10-05 安徽火天晶体科技有限公司 Sc,Ce共掺杂的硅酸镥、硅酸钇镥晶体及其熔体法生长方法
JP6451700B2 (ja) * 2016-06-29 2019-01-16 住友金属鉱山株式会社 酸化物単結晶の育成方法
RU2627573C1 (ru) * 2016-09-02 2017-08-08 Федеральное государственное бюджетное учреждение "Национальный исследовательский центр "Курчатовский институт" Сцинтилляционный материал для регистрации ионизирующего излучения (варианты)
CN108059957A (zh) * 2016-11-07 2018-05-22 上海新漫晶体材料科技有限公司 阴阳离子共掺杂高光输出低余辉闪烁体材料
CN108585853B (zh) * 2017-12-11 2021-12-24 上海大学 一种铕掺杂氧化钪闪烁体及其制备方法和用途
RU2693875C1 (ru) * 2018-04-05 2019-07-08 Сергей Александрович Кутовой Химическое соединение на основе оксиортосиликатов, содержащих иттрий и скандий, для квантовой электроники
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AU2004286178A1 (en) 2005-05-12
CA2555754A1 (en) 2005-05-12
EP1689916A1 (en) 2006-08-16
CN100436660C (zh) 2008-11-26
EP1689916B1 (en) 2008-12-10
JP4115503B2 (ja) 2008-07-09
EA009436B1 (ru) 2007-12-28
CN1902341A (zh) 2007-01-24
JP2007514631A (ja) 2007-06-07
WO2005042812A1 (en) 2005-05-12
RU2242545C1 (ru) 2004-12-20
ATE417145T1 (de) 2008-12-15
CA2555754C (en) 2009-06-02
DE602004018378D1 (de) 2009-01-22
AU2004286178B2 (en) 2008-11-13
EP1689916A4 (en) 2008-02-27

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