DK2982709T3 - Hærdbar sammensætning og støbt artikel, der omfatter sammensætningen - Google Patents

Hærdbar sammensætning og støbt artikel, der omfatter sammensætningen Download PDF

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DK2982709T3
DK2982709T3 DK14306252.9T DK14306252T DK2982709T3 DK 2982709 T3 DK2982709 T3 DK 2982709T3 DK 14306252 T DK14306252 T DK 14306252T DK 2982709 T3 DK2982709 T3 DK 2982709T3
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composition
molded article
compound
article according
weight
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DK14306252.9T
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Matusiak Renata Drozdzak
Gilles Recher
Alexander Daemen
Jacob Cornelis Dijt
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Telene Sas
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    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J5/00—Manufacture of articles or shaped materials containing macromolecular substances
    • C08J5/04—Reinforcing macromolecular compounds with loose or coherent fibrous material
    • C08J5/06—Reinforcing macromolecular compounds with loose or coherent fibrous material using pretreated fibrous materials
    • C08J5/08—Reinforcing macromolecular compounds with loose or coherent fibrous material using pretreated fibrous materials glass fibres
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    • C08L65/00—Compositions of macromolecular compounds obtained by reactions forming a carbon-to-carbon link in the main chain; Compositions of derivatives of such polymers
    • C—CHEMISTRY; METALLURGY
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    • C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
    • C08F2/00—Processes of polymerisation
    • C08F2/38—Polymerisation using regulators, e.g. chain terminating agents, e.g. telomerisation
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
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    • C08F283/00—Macromolecular compounds obtained by polymerising monomers on to polymers provided for in subclass C08G
    • C08F283/14—Macromolecular compounds obtained by polymerising monomers on to polymers provided for in subclass C08G on to polymers obtained by ring-opening polymerisation of carbocyclic compounds having one or more carbon-to-carbon double bonds in the carbocyclic ring, i.e. polyalkeneamers
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    • C08G61/00—Macromolecular compounds obtained by reactions forming a carbon-to-carbon link in the main chain of the macromolecule
    • C08G61/02—Macromolecular compounds containing only carbon atoms in the main chain of the macromolecule, e.g. polyxylylenes
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    • C08G61/00—Macromolecular compounds obtained by reactions forming a carbon-to-carbon link in the main chain of the macromolecule
    • C08G61/02—Macromolecular compounds containing only carbon atoms in the main chain of the macromolecule, e.g. polyxylylenes
    • C08G61/04—Macromolecular compounds containing only carbon atoms in the main chain of the macromolecule, e.g. polyxylylenes only aliphatic carbon atoms
    • C08G61/06—Macromolecular compounds containing only carbon atoms in the main chain of the macromolecule, e.g. polyxylylenes only aliphatic carbon atoms prepared by ring-opening of carbocyclic compounds
    • C08G61/08—Macromolecular compounds containing only carbon atoms in the main chain of the macromolecule, e.g. polyxylylenes only aliphatic carbon atoms prepared by ring-opening of carbocyclic compounds of carbocyclic compounds containing one or more carbon-to-carbon double bonds in the ring
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    • C08J5/00—Manufacture of articles or shaped materials containing macromolecular substances
    • C08J5/04—Reinforcing macromolecular compounds with loose or coherent fibrous material
    • C08J5/0405—Reinforcing macromolecular compounds with loose or coherent fibrous material with inorganic fibres
    • C08J5/043—Reinforcing macromolecular compounds with loose or coherent fibrous material with inorganic fibres with glass fibres
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    • C08K5/00—Use of organic ingredients
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    • C08K5/00—Use of organic ingredients
    • C08K5/54—Silicon-containing compounds
    • C08K5/541—Silicon-containing compounds containing oxygen
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    • C08L23/00—Compositions of homopolymers or copolymers of unsaturated aliphatic hydrocarbons having only one carbon-to-carbon double bond; Compositions of derivatives of such polymers
    • C08L23/02—Compositions of homopolymers or copolymers of unsaturated aliphatic hydrocarbons having only one carbon-to-carbon double bond; Compositions of derivatives of such polymers not modified by chemical after-treatment
    • C08L23/18—Homopolymers or copolymers of hydrocarbons having four or more carbon atoms
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    • C08L91/00—Compositions of oils, fats or waxes; Compositions of derivatives thereof
    • C08L91/06—Waxes
    • C08L91/08—Mineral waxes
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    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
    • C09J4/00—Adhesives based on organic non-macromolecular compounds having at least one polymerisable carbon-to-carbon unsaturated bond ; adhesives, based on monomers of macromolecular compounds of groups C09J183/00 - C09J183/16
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    • C08F4/00—Polymerisation catalysts
    • C08F4/42—Metals; Metal hydrides; Metallo-organic compounds; Use thereof as catalyst precursors
    • C08F4/44—Metals; Metal hydrides; Metallo-organic compounds; Use thereof as catalyst precursors selected from light metals, zinc, cadmium, mercury, copper, silver, gold, boron, gallium, indium, thallium, rare earths or actinides
    • C08F4/60—Metals; Metal hydrides; Metallo-organic compounds; Use thereof as catalyst precursors selected from light metals, zinc, cadmium, mercury, copper, silver, gold, boron, gallium, indium, thallium, rare earths or actinides together with refractory metals, iron group metals, platinum group metals, manganese, rhenium technetium or compounds thereof
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    • C08G2261/00—Macromolecular compounds obtained by reactions forming a carbon-to-carbon link in the main chain of the macromolecule
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    • C08G2261/00—Macromolecular compounds obtained by reactions forming a carbon-to-carbon link in the main chain of the macromolecule
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    • C08G2261/135—Cross-linked structures
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    • C08G2261/00—Macromolecular compounds obtained by reactions forming a carbon-to-carbon link in the main chain of the macromolecule
    • C08G2261/30—Monomer units or repeat units incorporating structural elements in the main chain
    • C08G2261/33—Monomer units or repeat units incorporating structural elements in the main chain incorporating non-aromatic structural elements in the main chain
    • C08G2261/332—Monomer units or repeat units incorporating structural elements in the main chain incorporating non-aromatic structural elements in the main chain containing only carbon atoms
    • C08G2261/3325—Monomer units or repeat units incorporating structural elements in the main chain incorporating non-aromatic structural elements in the main chain containing only carbon atoms derived from other polycyclic systems
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    • C08G2261/00—Macromolecular compounds obtained by reactions forming a carbon-to-carbon link in the main chain of the macromolecule
    • C08G2261/40—Polymerisation processes
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    • C08G2261/418—Ring opening metathesis polymerisation [ROMP]
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    • C08G2261/00—Macromolecular compounds obtained by reactions forming a carbon-to-carbon link in the main chain of the macromolecule
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    • C08L2205/00—Polymer mixtures characterised by other features
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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Manufacturing & Machinery (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Inorganic Chemistry (AREA)
  • Reinforced Plastic Materials (AREA)
  • Compositions Of Macromolecular Compounds (AREA)
  • Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
  • Polyoxymethylene Polymers And Polymers With Carbon-To-Carbon Bonds (AREA)

Claims (19)

1. Støbt artikel af et kompositmateriale, der omfatter (a) en matrixpolymer, som er fremstillet ved polymerisering af en hærdbar sammensætning, der omfatter: (A) en cyklisk olefin; (B) en metatesekatalysator til polymerisering af den cykliske olefin; (C) 0,1 - 30 vægt-% af en forbindelse, der omfatter mindst en vinylgruppe; og (D) 0,1 -10 vægt-% af et hærdemiddel for forbindelsen (C), hvor vægt-% er i forhold til den samlede vægt af sammensætningen, og (b) forstærkende fibre, der er forsynet med en limningsmiddelsammensætning.
2. Støbt artikel ifølge krav 1, hvor forbindelsen (C) har en Hildebrandt-opløselighedsparameter δτ på mellem 15,4 og 19,8 MPa1/2.
3. Støbt artikel ifølge krav 1 eller 2, der omfatter 3 - 20 vægt-% af forbindelsen (C).
4. Støbt artikel ifølge et hvilket som helst af de foregående krav, hvor forbindelsen (C) omfatter en (meth)acrylatforbindelse.
5. Støbt artikel ifølge et hvilket som helst af de foregående krav, der omfatter 0,2 -1 vægt-% af det hærdende middel.
6. Støbt artikel ifølge et hvilket som helst af de foregående krav, hvor det hærdende middel omfatter en radikalinitiator.
7. Støbt artikel ifølge krav 6, hvor radikalinitiatoren omfatter et ikke-cyklisk peroxid.
8. Støbt artikel ifølge et hvilket som helst af de foregående krav, hvor den cykliske olefin omfatter en dicyclopentadien.
9. Støbt artikel ifølge et hvilket som helst af de foregående krav, hvor en filmdanner for limningsmidlet har en Hildebrandt-opløselighedsparameter δτ, der er omfattet mellem 15,9 og 19,9 MPa1/2.
10. Støbt artikel ifølge et hvilket som helst af de foregående krav, hvor en filmdanner for limningsmidlet omfatter en (co)polymer af monomere enheder, der har fra fire til seks carbonatomer og en carbon-carbon-dobbeltbinding.
11. Støbt artikel ifølge krav 10, hvorfilmdanneren omfatter polybutadien.
12. Støbt artikel ifølge et hvilket som helst af de foregående krav, hvor en filmdanner for limningsmidlet omfatter paraffinvoks.
13. Støbt artikel ifølge et hvilket som helst af de foregående krav, hvor et koblingsmiddel for limningsmidlet omfatter en silanforbindelse, der har umættethed.
14. Fremgangsmåde til fremstilling af en støbt artikel ifølge et hvilket som helst af de foregående krav, hvilken fremgangsmåde omfatter: - at kombinerer mindst forbindelserne (A) til (D) for at danne den hærdbare sammensætning; - at kontakte sammensætningen med de forstærkende fibre; og - at udsætte sammensætningen for betingelser, der er effektive til at fremme en olefin-metathese-reaktion af den cykliske olefin og en radikalpolymerisation af forbindelsen (C).
15. Fremgangsmåden ifølge krav 14, hvilken fremgangsmåde yderligere omfatter følgende trin: - at kontakte den hærdbare sammensætning med et klæbende substrat; og - at udsætte den hærdbare sammensætning for betingelser for at tilvejebringe en binding mellem sammensætningen og det klæbende substrat.
16. Fremgangsmåde ifølge krav 14 eller 15, hvilken fremgangsmåde omfatter trinnet at injicere sammensætningen i en lukket støbeform, hvilken støbeform er tilvejebragt med forstærkningsfibre forud for indsprøjtning af sammensætningen.
17. Fremgangsmåde ifølge et hvilket som helst af kravene 14-16, hvor betingelserne omfatter opvarmning ved en temperatur på mellem 120 °C til 150 °C i løbet af højst 60 minutter.
18. Støbt artikel ifølge et hvilket som helst af de foregående krav 1-13, hvor matrixpolymeren har et flygtigt indhold på mindre end 3 vægt-% i forhold til den samlede vægt af matrixpolymeren.
19. Støbt artikel ifølge et hvilket som helst af de foregående krav 1-13, hvor kompositmaterialets egenskaber mindst opfylder en af følgende: - en glasovergangstemperatur Tg ifølge ASTM D7028-07e1, der er over 180 °C; - en tværgående 3-punktsbøjningsstyrke ifølge ISO 14125, der er over 50 MPa; og - en G1c ifølge ISO 15024, der er over 800 J/m2.
DK14306252.9T 2014-08-07 2014-08-07 Hærdbar sammensætning og støbt artikel, der omfatter sammensætningen DK2982709T3 (da)

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US (2) US10017615B2 (da)
EP (3) EP2982709B1 (da)
JP (2) JP2017525836A (da)
KR (2) KR20170047260A (da)
CN (2) CN107109034B (da)
DK (2) DK2982709T3 (da)
ES (2) ES2639302T3 (da)
PL (2) PL2982709T3 (da)
TR (1) TR201904749T4 (da)
WO (2) WO2016020261A1 (da)

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US9856352B2 (en) 2014-08-07 2018-01-02 Ppg Industries Ohio, Inc. Glass fiber sizing compositions, sized glass fibers, and polyolefin composites
EP2982709B1 (en) * 2014-08-07 2017-06-28 Telene SAS Curable composition and molded article comprising the composition
EP3202813A1 (en) * 2016-02-05 2017-08-09 Telene SAS Curable composition and molded article comprising the composition
US10487446B2 (en) * 2016-03-18 2019-11-26 The Board Of Trustees Of The University Of Illinois Frontal polymerization for fiber-reinforced composites
DE102016217735A1 (de) * 2016-09-16 2018-03-22 Carl Zeiss Smt Gmbh Komponente für eine Spiegelanordnung für die EUV-Lithographie
CN110023358B (zh) * 2016-12-07 2022-07-08 Dic株式会社 VaRTM成型用树脂组合物、成型材料、成型品和成型品的制造方法
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