DK2399977T3 - Fraktioneringsfremgangsmåde til 1,3-dimættet-2-umættet triglycerid - Google Patents

Fraktioneringsfremgangsmåde til 1,3-dimættet-2-umættet triglycerid Download PDF

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Publication number
DK2399977T3
DK2399977T3 DK11168991.5T DK11168991T DK2399977T3 DK 2399977 T3 DK2399977 T3 DK 2399977T3 DK 11168991 T DK11168991 T DK 11168991T DK 2399977 T3 DK2399977 T3 DK 2399977T3
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DK
Denmark
Prior art keywords
fatty acid
triglycerides
fat
solid
mass
Prior art date
Application number
DK11168991.5T
Other languages
English (en)
Inventor
Shin Arimoto
Hidetaka Uehara
Tomomi Suganuma
Kinya Tsuchiya
Satoshi Negishi
Original Assignee
Nisshin Oillio Group Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
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Application filed by Nisshin Oillio Group Ltd filed Critical Nisshin Oillio Group Ltd
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Publication of DK2399977T3 publication Critical patent/DK2399977T3/da

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    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B7/00—Separation of mixtures of fats or fatty oils into their constituents, e.g. saturated oils from unsaturated oils
    • C11B7/0075—Separation of mixtures of fats or fatty oils into their constituents, e.g. saturated oils from unsaturated oils by differences of melting or solidifying points
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B7/00—Separation of mixtures of fats or fatty oils into their constituents, e.g. saturated oils from unsaturated oils
    • C11B7/0008—Separation of mixtures of fats or fatty oils into their constituents, e.g. saturated oils from unsaturated oils by differences of solubilities, e.g. by extraction, by separation from a solution by means of anti-solvents
    • C11B7/0025—Separation of mixtures of fats or fatty oils into their constituents, e.g. saturated oils from unsaturated oils by differences of solubilities, e.g. by extraction, by separation from a solution by means of anti-solvents in solvents containing oxygen in their molecule
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11C—FATTY ACIDS FROM FATS, OILS OR WAXES; CANDLES; FATS, OILS OR FATTY ACIDS BY CHEMICAL MODIFICATION OF FATS, OILS, OR FATTY ACIDS OBTAINED THEREFROM
    • C11C1/00—Preparation of fatty acids from fats, fatty oils, or waxes; Refining the fatty acids
    • C11C1/08—Refining
    • C11C1/10—Refining by distillation
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11C—FATTY ACIDS FROM FATS, OILS OR WAXES; CANDLES; FATS, OILS OR FATTY ACIDS BY CHEMICAL MODIFICATION OF FATS, OILS, OR FATTY ACIDS OBTAINED THEREFROM
    • C11C3/00—Fats, oils, or fatty acids by chemical modification of fats, oils, or fatty acids obtained therefrom
    • C11C3/04—Fats, oils, or fatty acids by chemical modification of fats, oils, or fatty acids obtained therefrom by esterification of fats or fatty oils
    • C11C3/10—Ester interchange

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  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Wood Science & Technology (AREA)
  • Organic Chemistry (AREA)
  • General Chemical & Material Sciences (AREA)
  • Analytical Chemistry (AREA)
  • Microbiology (AREA)
  • Fats And Perfumes (AREA)
  • Edible Oils And Fats (AREA)

Claims (5)

1. Fremgangsmåde til fremstilling af triglycerider, der er rige på XLX-fedt, hvilken fremgangsmåde omfatter trinnene med at opvarme og opløse triglycerider, som omfatter 20 til 60 masseprocent af en triglycerid (XLX-fedt) med en mættet fedtsyrerest i hver af den første og tredje position og en linoleoyl-gruppe i den anden position i det samlede antal triglycerider i nærvær af 1 til 30 masseprocent af en lavere fedtsyrealkylester med alkylgruppe med 1 til 6 carbonatomer; og derefter afkøling af blandingen til udfældning af krystaller og udførelse af fast-flydende-separering.
2. Fremgangsmåde ifølge krav 1, hvor fast-flydende-separeringen udføres ved at tilsætte 1 til 50 vægtdele af en lavere fedtsyrealkylester med alkylgruppe med 1 til 6 carbonatomer pr. 100 vægtdele af de udfældede krystaller og knuse blandingen; eller knuse krystallerne og derefter tilsætte den lavere fedtsyrealkylester dertil; og derefter filtrere blandingen ved komprimering til opnåelse af et fast indhold.
3. Fremgangsmåde ifølge et af kravene 1 til 2, der omfatter trinnene med at opvarme og opløse triglycerider, der omfatter 20 til 60 masseprocent XLX-fedt i det samlede antal triglycerider i nærvær af 1 til 30 masseprocent af en lavere fedtsyrealkylester med alkylgruppe med 1 til 6 carbonatomer; derefter afkøling af blandingen og fjernelse, ved krystallisering, af en triglycerid (XXX-fedt), som kun består af mættede fedtsyrerester, og/eller en diglycerid (XX), der kun består af mættede fedtsyrerester; og yderligere afkøling af reaktanten ved omrøring til krystallisering af XLX-fedt og udførelse af fast-flydende-separering.
4. Fremgangsmåde ifølge et af kravene 1 til 2, der omfatter trinnene med at opvarme og opløse triglycerider, der omfatter 20 til 60 masseprocent XLX-fedt i det samlede antal triglycerider i nærvær af 1 til 30 masseprocent en lavere fedtsyrealkylester med alkylgruppe med 1 til 6 carbonatomer; derefter afkøling af blandingen og fjernelse, ved krystallisering, af en triglycerid (XXX-fedt), der kun består af mættede fedtsyrerester, og/eller en diglycerid (XX), der kun består af mættede fedtsyrerester; og yderligere fraktionering af reaktanten med en eller flere opløsningsmidler til krystallisering af XLX-fedt og udførelse af fast-flydende-separering.
5. Fremgangsmåde ifølge et af kravene 1 til 4, der omfatter trinnet med at oprense det opnåede faste indhold.
DK11168991.5T 2007-09-07 2008-09-08 Fraktioneringsfremgangsmåde til 1,3-dimættet-2-umættet triglycerid DK2399977T3 (da)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
JP2007232567 2007-09-07
JP2008053465 2008-03-04
EP08829341.0A EP2213712B1 (en) 2007-09-07 2008-09-08 Method for separation of 1,3-disaturated-2-unsaturated triglyceride

Publications (1)

Publication Number Publication Date
DK2399977T3 true DK2399977T3 (da) 2014-02-24

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Family Applications (3)

Application Number Title Priority Date Filing Date
DK11168989.9T DK2388306T3 (da) 2007-09-07 2008-09-08 Fraktioneringsfremgangsmåde til 1,3-dimættet-2-umættet triglycerid
DK11168991.5T DK2399977T3 (da) 2007-09-07 2008-09-08 Fraktioneringsfremgangsmåde til 1,3-dimættet-2-umættet triglycerid
DK08829341.0T DK2213712T3 (da) 2007-09-07 2008-09-08 Fremgangsmåde til separering af 1,3-dimættet-2-umættet triglycerid

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DK11168989.9T DK2388306T3 (da) 2007-09-07 2008-09-08 Fraktioneringsfremgangsmåde til 1,3-dimættet-2-umættet triglycerid

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DK08829341.0T DK2213712T3 (da) 2007-09-07 2008-09-08 Fremgangsmåde til separering af 1,3-dimættet-2-umættet triglycerid

Country Status (11)

Country Link
US (1) US8389754B2 (da)
EP (4) EP2388306B1 (da)
JP (1) JP4352103B2 (da)
KR (1) KR101010572B1 (da)
CN (1) CN101848981B (da)
DK (3) DK2388306T3 (da)
ES (3) ES2437927T3 (da)
MY (1) MY147857A (da)
RU (1) RU2431654C1 (da)
TW (1) TWI441915B (da)
WO (1) WO2009031680A1 (da)

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Also Published As

Publication number Publication date
ES2437849T3 (es) 2014-01-14
WO2009031680A1 (ja) 2009-03-12
KR20100043111A (ko) 2010-04-27
CN101848981A (zh) 2010-09-29
RU2431654C1 (ru) 2011-10-20
TW200920840A (en) 2009-05-16
EP2399977B1 (en) 2013-11-27
DK2388306T3 (da) 2014-02-24
KR101010572B1 (ko) 2011-01-24
DK2213712T3 (da) 2014-01-20
JP4352103B2 (ja) 2009-10-28
MY147857A (en) 2013-01-31
EP2388307A1 (en) 2011-11-23
TWI441915B (zh) 2014-06-21
ES2438170T3 (es) 2014-01-16
EP2213712A1 (en) 2010-08-04
US8389754B2 (en) 2013-03-05
CN101848981B (zh) 2014-06-11
EP2213712B1 (en) 2013-11-27
EP2388306A1 (en) 2011-11-23
EP2399977A1 (en) 2011-12-28
US20100222607A1 (en) 2010-09-02
EP2213712A4 (en) 2012-02-22
EP2388306B1 (en) 2013-11-27
ES2437927T3 (es) 2014-01-15
JPWO2009031680A1 (ja) 2010-12-16

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