DE88557C - - Google Patents
Info
- Publication number
- DE88557C DE88557C DENDAT88557D DE88557DA DE88557C DE 88557 C DE88557 C DE 88557C DE NDAT88557 D DENDAT88557 D DE NDAT88557D DE 88557D A DE88557D A DE 88557DA DE 88557 C DE88557 C DE 88557C
- Authority
- DE
- Germany
- Prior art keywords
- amidophenyltrimethylammonium
- derivatives
- water
- alcohol
- prisms
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
- -1 alkyl halogens Chemical class 0.000 claims description 13
- 150000003839 salts Chemical class 0.000 claims description 10
- 239000002253 acid Substances 0.000 claims description 3
- 230000029936 alkylation Effects 0.000 claims description 2
- 238000005804 alkylation reaction Methods 0.000 claims description 2
- 125000003368 amide group Chemical group 0.000 claims description 2
- 150000004984 aromatic diamines Chemical class 0.000 claims description 2
- NYGZLYXAPMMJTE-UHFFFAOYSA-M metanil yellow Chemical group [Na+].[O-]S(=O)(=O)C1=CC=CC(N=NC=2C=CC(NC=3C=CC=CC=3)=CC=2)=C1 NYGZLYXAPMMJTE-UHFFFAOYSA-M 0.000 claims description 2
- 150000007513 acids Chemical class 0.000 claims 2
- 238000003776 cleavage reaction Methods 0.000 claims 2
- 238000000034 method Methods 0.000 claims 2
- 230000011987 methylation Effects 0.000 claims 2
- 238000007069 methylation reaction Methods 0.000 claims 2
- 230000007017 scission Effects 0.000 claims 2
- ZYDILTJZICMURJ-UHFFFAOYSA-N 1-(2,3-diaminophenyl)ethanone Chemical compound CC(=O)C1=CC=CC(N)=C1N ZYDILTJZICMURJ-UHFFFAOYSA-N 0.000 claims 1
- GGSUCNLOZRCGPQ-UHFFFAOYSA-N diethylaniline Chemical compound CCN(CC)C1=CC=CC=C1 GGSUCNLOZRCGPQ-UHFFFAOYSA-N 0.000 claims 1
- 229910052736 halogen Inorganic materials 0.000 claims 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 22
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 19
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 17
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 12
- UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 description 9
- VEXZGXHMUGYJMC-UHFFFAOYSA-M Chloride anion Chemical compound [Cl-] VEXZGXHMUGYJMC-UHFFFAOYSA-M 0.000 description 9
- 239000000243 solution Substances 0.000 description 7
- HCHKCACWOHOZIP-UHFFFAOYSA-N Zinc Chemical compound [Zn] HCHKCACWOHOZIP-UHFFFAOYSA-N 0.000 description 6
- 239000011701 zinc Substances 0.000 description 6
- 229910052725 zinc Inorganic materials 0.000 description 6
- JIAARYAFYJHUJI-UHFFFAOYSA-L zinc dichloride Chemical compound [Cl-].[Cl-].[Zn+2] JIAARYAFYJHUJI-UHFFFAOYSA-L 0.000 description 6
- 238000000354 decomposition reaction Methods 0.000 description 4
- XMBWDFGMSWQBCA-UHFFFAOYSA-N hydrogen iodide Chemical compound I XMBWDFGMSWQBCA-UHFFFAOYSA-N 0.000 description 4
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 3
- 239000013078 crystal Substances 0.000 description 3
- 238000010438 heat treatment Methods 0.000 description 3
- 235000005074 zinc chloride Nutrition 0.000 description 3
- 239000011592 zinc chloride Substances 0.000 description 3
- XZXYQEHISUMZAT-UHFFFAOYSA-N 2-[(2-hydroxy-5-methylphenyl)methyl]-4-methylphenol Chemical compound CC1=CC=C(O)C(CC=2C(=CC=C(C)C=2)O)=C1 XZXYQEHISUMZAT-UHFFFAOYSA-N 0.000 description 2
- QGZKDVFQNNGYKY-UHFFFAOYSA-O Ammonium Chemical compound [NH4+] QGZKDVFQNNGYKY-UHFFFAOYSA-O 0.000 description 2
- PAYRUJLWNCNPSJ-UHFFFAOYSA-N Aniline Chemical compound NC1=CC=CC=C1 PAYRUJLWNCNPSJ-UHFFFAOYSA-N 0.000 description 2
- ICGLOTCMOYCOTB-UHFFFAOYSA-N [Cl].[Zn] Chemical compound [Cl].[Zn] ICGLOTCMOYCOTB-UHFFFAOYSA-N 0.000 description 2
- 229940107816 ammonium iodide Drugs 0.000 description 2
- 239000000987 azo dye Substances 0.000 description 2
- HUMNYLRZRPPJDN-UHFFFAOYSA-N benzaldehyde Chemical compound O=CC1=CC=CC=C1 HUMNYLRZRPPJDN-UHFFFAOYSA-N 0.000 description 2
- 238000009835 boiling Methods 0.000 description 2
- 238000010992 reflux Methods 0.000 description 2
- ZYDVNTYVDVZMKF-UHFFFAOYSA-N [Cl].[Ag] Chemical compound [Cl].[Ag] ZYDVNTYVDVZMKF-UHFFFAOYSA-N 0.000 description 1
- ZXYNGLRGFYLTQZ-UHFFFAOYSA-M [Zn]Cl Chemical compound [Zn]Cl ZXYNGLRGFYLTQZ-UHFFFAOYSA-M 0.000 description 1
- 125000002777 acetyl group Chemical group [H]C([H])([H])C(*)=O 0.000 description 1
- 239000007864 aqueous solution Substances 0.000 description 1
- 125000005998 bromoethyl group Chemical group 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- 150000004985 diamines Chemical class 0.000 description 1
- 150000004694 iodide salts Chemical class 0.000 description 1
- HWSZZLVAJGOAAY-UHFFFAOYSA-L lead(II) chloride Chemical compound Cl[Pb]Cl HWSZZLVAJGOAAY-UHFFFAOYSA-L 0.000 description 1
- 238000002844 melting Methods 0.000 description 1
- 230000008018 melting Effects 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- CJDICMLSLYHRPT-UHFFFAOYSA-N n,n-dimethyl-3-nitroaniline Chemical compound CN(C)C1=CC=CC([N+]([O-])=O)=C1 CJDICMLSLYHRPT-UHFFFAOYSA-N 0.000 description 1
- GNVRJGIVDSQCOP-UHFFFAOYSA-N n-ethyl-n-methylethanamine Chemical compound CCN(C)CC GNVRJGIVDSQCOP-UHFFFAOYSA-N 0.000 description 1
- SFDJOSRHYKHMOK-UHFFFAOYSA-N nitramide Chemical compound N[N+]([O-])=O SFDJOSRHYKHMOK-UHFFFAOYSA-N 0.000 description 1
- QNGNSVIICDLXHT-UHFFFAOYSA-N para-ethylbenzaldehyde Natural products CCC1=CC=C(C=O)C=C1 QNGNSVIICDLXHT-UHFFFAOYSA-N 0.000 description 1
- 238000001556 precipitation Methods 0.000 description 1
- 235000011121 sodium hydroxide Nutrition 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
- 239000006188 syrup Substances 0.000 description 1
- 235000020357 syrup Nutrition 0.000 description 1
Landscapes
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Publications (1)
| Publication Number | Publication Date |
|---|---|
| DE88557C true DE88557C (enrdf_load_html_response) |
Family
ID=360437
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DENDAT88557D Active DE88557C (enrdf_load_html_response) |
Country Status (1)
| Country | Link |
|---|---|
| DE (1) | DE88557C (enrdf_load_html_response) |
-
0
- DE DENDAT88557D patent/DE88557C/de active Active
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| DE2855764A1 (de) | Verfahren zur herstellung von nitrodiarylamin unter verwendung eines promotors | |
| EP0563747A2 (de) | Verfahren zur Herstellung von wässrigen Betainlösungen | |
| DE88557C (enrdf_load_html_response) | ||
| DE823294C (de) | Verfahren zur Herstellung von diquartaeren Salzen von Pyrimidylaminochinolinen | |
| DE2649530C3 (de) | Bis-isothiuronium-Salze, Verfahren zu ihrer Herstellung und Ihre Verwendung zur Reinigung von anionische Farbstoffe und/oder anionische Tenside enthaltenden Abwässern | |
| DE889447C (de) | Verfahren zur Herstellung diquarternaerer Salze des 4-Amino-6-(2'-aminopyrimidyl-4'-amino)-chinazolins | |
| DE530398C (de) | Verfahren zur Herstellung von Oxynaphthylguanidinen | |
| DE613516C (de) | Verfahren zur Darstellung von Kondensationsprodukten | |
| DE833818C (de) | Verfahren zur Herstellung von neuen mono- und diquartaeren Salzen von Pyrimidylaminocinnolinen | |
| DE128854C (enrdf_load_html_response) | ||
| DE69917163T2 (de) | Verfahren zur herstellung von l-valinbenzylester-p-toluolsufonaten | |
| AT162937B (de) | Verfahren zur Herstellung eines neuen substituierten 2,4-Diamino-1,3,5-triazins | |
| DE883883C (de) | Verfahren zum Behandeln von Wolle | |
| DE967826C (de) | Verfahren zur Herstellung von Aryloxyalkanol-schwefelsaeurehalbestersalzen | |
| DE831697C (de) | Verfahren zur Herstellung von neuen Pyrimidylaminochinolinderivaten | |
| DE615184C (de) | Verfahren zur Darstellung von Aminoverbindungen der Chinolinreihe | |
| DE586806C (de) | Verfahren zur Darstellung von symmetrischen Di-(arylamino)-oxybenzolen | |
| DE484664C (de) | Verfahren zur Darstellung von Sulfoderivaten der Oxyarylcarbonsaeurearylide | |
| AT85299B (de) | Verfahren zur Darstellung komplexer Silberverbindungen von α-Aminosäuren. | |
| DE746576C (de) | Verfahren zur Darstellung von 2,4-Diamino-1,3,5-triazinen. | |
| DE681684C (de) | Verfahren zur Herstellung von Abkoemmlingen von cyclischen Aminosulfonsaeureamiden | |
| DE657118C (de) | Verfahren zur Darstellung von Abkoemmlingen des p-Phenanthrolins | |
| DE553074C (de) | Verfahren zur Darstellung von Aminosulfonsaeuren | |
| AT156476B (de) | Verfahren zur Herstellung von Guajacolverbindungen. | |
| DE66361C (de) | Verfahren zur Darstellung eines am Azinstickstoff alkylirten Indulins und von Sulfosäuren desselben |