DE69902485T3 - Verfahren zur herstellung von acylphosphinen und derivaten - Google Patents

Verfahren zur herstellung von acylphosphinen und derivaten Download PDF

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Publication number
DE69902485T3
DE69902485T3 DE69902485T DE69902485T DE69902485T3 DE 69902485 T3 DE69902485 T3 DE 69902485T3 DE 69902485 T DE69902485 T DE 69902485T DE 69902485 T DE69902485 T DE 69902485T DE 69902485 T3 DE69902485 T3 DE 69902485T3
Authority
DE
Germany
Prior art keywords
alkyl
phenyl
reaction
substituted
alkoxy
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
DE69902485T
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German (de)
English (en)
Other versions
DE69902485T2 (de
DE69902485D1 (de
Inventor
George David LEPPARD
Eugen Eichenberger
Rene Kaeser
Gebhard Hug
Urs 07590 Cala Ratjada SCHWENDIMANN
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
BASF Schweiz AG
Original Assignee
Ciba Spezialitaetenchemie Holding AG
Ciba SC Holding AG
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
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First worldwide family litigation filed litigation Critical https://patents.darts-ip.com/?family=25690294&utm_source=google_patent&utm_medium=platform_link&utm_campaign=public_patent_search&patent=DE69902485(T3) "Global patent litigation dataset” by Darts-ip is licensed under a Creative Commons Attribution 4.0 International License.
Application filed by Ciba Spezialitaetenchemie Holding AG, Ciba SC Holding AG filed Critical Ciba Spezialitaetenchemie Holding AG
Application granted granted Critical
Publication of DE69902485D1 publication Critical patent/DE69902485D1/de
Publication of DE69902485T2 publication Critical patent/DE69902485T2/de
Publication of DE69902485T3 publication Critical patent/DE69902485T3/de
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

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Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F9/00—Compounds containing elements of Groups 5 or 15 of the Periodic Table
    • C07F9/02—Phosphorus compounds
    • C07F9/28—Phosphorus compounds with one or more P—C bonds
    • C07F9/50—Organo-phosphines
    • C07F9/53—Organo-phosphine oxides; Organo-phosphine thioxides
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F9/00—Compounds containing elements of Groups 5 or 15 of the Periodic Table
    • C07F9/02—Phosphorus compounds
    • C07F9/28—Phosphorus compounds with one or more P—C bonds
    • C07F9/50—Organo-phosphines
    • C07F9/5036—Phosphines containing the structure -C(=X)-P or NC-P
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F9/00—Compounds containing elements of Groups 5 or 15 of the Periodic Table
    • C07F9/02—Phosphorus compounds
    • C07F9/28—Phosphorus compounds with one or more P—C bonds
    • C07F9/50—Organo-phosphines
    • C07F9/53—Organo-phosphine oxides; Organo-phosphine thioxides
    • C07F9/5337—Phosphine oxides or thioxides containing the structure -C(=X)-P(=X) or NC-P(=X) (X = O, S, Se)

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Biochemistry (AREA)
  • General Health & Medical Sciences (AREA)
  • Molecular Biology (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
  • Saccharide Compounds (AREA)
DE69902485T 1998-11-30 1999-11-20 Verfahren zur herstellung von acylphosphinen und derivaten Expired - Lifetime DE69902485T3 (de)

Applications Claiming Priority (5)

Application Number Priority Date Filing Date Title
CH237698 1998-11-30
CH237698 1998-11-30
CH243498 1998-12-08
CH243498 1998-12-08
PCT/EP1999/008968 WO2000032612A1 (en) 1998-11-30 1999-11-20 Process for preparing acylphosphines and derivatives

Publications (3)

Publication Number Publication Date
DE69902485D1 DE69902485D1 (de) 2002-09-12
DE69902485T2 DE69902485T2 (de) 2003-05-08
DE69902485T3 true DE69902485T3 (de) 2007-03-15

Family

ID=25690294

Family Applications (1)

Application Number Title Priority Date Filing Date
DE69902485T Expired - Lifetime DE69902485T3 (de) 1998-11-30 1999-11-20 Verfahren zur herstellung von acylphosphinen und derivaten

Country Status (14)

Country Link
US (3) US6888031B1 (enExample)
EP (1) EP1135399B2 (enExample)
JP (1) JP4265871B2 (enExample)
KR (1) KR100653117B1 (enExample)
CN (1) CN1211388C (enExample)
AT (1) ATE221893T1 (enExample)
AU (1) AU760237B2 (enExample)
CA (1) CA2349637C (enExample)
CZ (1) CZ302512B6 (enExample)
DE (1) DE69902485T3 (enExample)
ES (1) ES2180347T5 (enExample)
SK (1) SK286152B6 (enExample)
TW (1) TW492972B (enExample)
WO (1) WO2000032612A1 (enExample)

Families Citing this family (38)

* Cited by examiner, † Cited by third party
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AU760237B2 (en) * 1998-11-30 2003-05-08 Igm Group B.V. Process for preparing acylphosphines and derivatives
GB2360283B (en) 2000-02-08 2002-08-21 Ciba Sc Holding Ag Monoacylarylphosphines and acylphosphine oxides and sulphides
GB2365430B (en) 2000-06-08 2002-08-28 Ciba Sc Holding Ag Acylphosphine photoinitiators and intermediates
EP1423757B1 (en) * 2001-08-21 2009-04-29 Ciba Holding Inc. Bathochromic mono- and bis-acylphosphine oxides and sulfides and their use as photoinitiators
DE10206117A1 (de) 2002-02-13 2003-08-14 Basf Ag Acyl- und Bisacylphosphinderivate
DE10244684A1 (de) 2002-09-24 2004-04-01 Basf Ag Verfahren zur Herstellung von Acylphosphinoxiden
DE60328219D1 (de) * 2002-12-04 2009-08-13 Ciba Holding Inc Verfahren zur synthese von cycloorganylphosphanen und von di(alkali/erdalkalimetall)oligophosphandiiden
DE10315671A1 (de) * 2003-04-04 2004-10-14 Basf Ag Verfahren zur Herstellung von Acylphosphinoxid-Feststoffen
WO2005014605A1 (en) * 2003-07-18 2005-02-17 Ciba Specialty Chemicals Holding Inc. Process for preparing acylphosphanes and derivatives thereof
TW200523265A (en) * 2003-07-31 2005-07-16 Basf Ag A process for the preparation of acylphosphines
EP1814891B1 (en) 2004-11-23 2011-01-26 Basf Se Bisacylphosphanes and their use as photoinitiators; process for preparing acylphosphanes
WO2006074983A1 (en) * 2005-01-17 2006-07-20 Ciba Specialty Chemicals Holding Inc. Process for preparing acylphosphanes and their oxides and sulphides
DE102005005946A1 (de) * 2005-02-10 2006-08-17 Basf Ag Verfahren zur Herstellung tertiärer Phosphine
KR101648996B1 (ko) 2008-11-03 2016-08-17 바스프 에스이 광개시제 혼합물
EP2421903B1 (en) * 2009-04-20 2014-11-19 ETH Zurich Polymer nanoparticles
CN102875597B (zh) * 2011-07-11 2017-05-03 深圳市有为化学技术有限公司 芳香酮膦氧杂化型化合物
CN102875598B (zh) * 2011-07-11 2016-09-07 深圳市有为化学技术有限公司 (二苯膦氧基)(均三甲苯基)甲酮和(苯膦氧基)双(均三甲苯基甲酮)的制备方法
CN102675365A (zh) * 2012-05-16 2012-09-19 湖北固润科技股份有限公司 一种紫外光引发剂xbpo合成方法
GB201213163D0 (en) 2012-07-24 2012-09-05 Lambson Ltd Photopolymerisation processes and novel compounds therefor
CN108383874B (zh) 2012-10-01 2021-10-08 瑞士联邦苏黎世技术大学 用于制备酰基磷烷的方法
US10298846B2 (en) 2013-03-15 2019-05-21 Freefly Systems, Inc. Method and system for enabling pointing control of an actively stabilized camera
CN104592298B (zh) * 2014-12-31 2016-07-06 湖北固润科技股份有限公司 一种酰基膦高效光引发剂及其制备方法
CN105541913B (zh) * 2015-12-03 2017-08-25 天津久日新材料股份有限公司 一种2,4,6‑三甲基苯甲酰基二苯基氧化膦的制备方法
CN105732709A (zh) * 2016-03-16 2016-07-06 三峡大学 一种光引发剂2,4,6-三甲基苯甲酰二环己基氧膦，制备方法及其应用
CN105732710A (zh) * 2016-03-16 2016-07-06 三峡大学 一种光引发剂联苯基四(2,4,6-三甲基苯甲酰基)氧化膦的制备方法及其应用
CN107304220B (zh) * 2016-04-22 2020-03-31 江苏英力科技发展有限公司 一种“一锅法”合成2,4,6-三甲基苯甲酰基-二苯基氧化膦的方法
EP3296301A1 (en) 2016-09-19 2018-03-21 ETH Zürich A versatile process for the preparation of acylphosphines
JP6916484B2 (ja) * 2017-03-28 2021-08-11 国立大学法人千葉大学 アシルホスフィンの製造方法
EP3409680B1 (en) 2017-05-30 2021-01-06 IGM Group B.V. Synthesis of bis(acyl)phosphines by activation of unreactive metal phosphides
EP3539924A1 (en) 2018-03-14 2019-09-18 ETH Zurich Novel vinyl phosphines and photo-initiators obtainable therefrom
CN110734461A (zh) * 2018-07-20 2020-01-31 深圳市有为化学技术有限公司 化合物2,4,6-三甲基苯甲酰基二苯基氧化膦的制备
EP3892625A4 (en) * 2018-12-07 2021-11-24 Anqing Lighting Optoelectronics Technology Co., Ltd ACYLPHOSPHINE OXIDE COMPOUND AND MANUFACTURING METHOD FOR IT
CN111138491B (zh) * 2019-12-31 2022-08-05 天津久日新材料股份有限公司 一种制备光引发剂tpo同时副产氯苄的方法
CN111087425B (zh) 2020-01-10 2022-04-19 天津大学 一种大粒度苯基双(2,4,6-三甲基苯甲酰基)氧化膦晶型及其结晶方法
CN112279940B (zh) * 2020-04-17 2023-06-27 山东科技大学 一种酰基膦光引发剂及其制备方法
CN112159429B (zh) * 2020-10-29 2022-06-21 天津久日新材料股份有限公司 一种双(2,4,6-三甲基苯甲酰基)苯基氧化膦的制备方法
IT202300028218A1 (it) 2023-12-28 2025-06-28 Igm Resins Italia Srl Nuova forma solida di bis(2,4,6-trimetilbenzoil)-n-ottilfosfina ossido
JP7600464B1 (ja) * 2024-10-03 2024-12-16 サカタインクス株式会社 活性エネルギー線硬化型インクジェット印刷用インク

Family Cites Families (13)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE2909994A1 (de) 1979-03-14 1980-10-02 Basf Ag Acylphosphinoxidverbindungen, ihre herstellung und verwendung
EP0007086B1 (de) 1978-07-14 1982-02-10 BASF Aktiengesellschaft Lichthärtbare Form-, Tränk- und Überzugsmassen sowie daraus hergestellte Formkörper
DE3020092A1 (de) * 1980-05-27 1981-12-10 Basf Ag, 6700 Ludwigshafen Acylphosphinverbindungen und ihre verwendung
DE3034697A1 (de) 1980-09-15 1982-05-06 Basf Ag, 6700 Ludwigshafen Acylphosphinsulfidverbindungen, ihre herstellung und verwendung
DE3443221A1 (de) 1984-11-27 1986-06-05 ESPE Fabrik pharmazeutischer Präparate GmbH, 8031 Seefeld Bisacylphosphinoxide, ihre herstellung und verwendung
US5218009A (en) * 1989-08-04 1993-06-08 Ciba-Geigy Corporation Mono- and di-acylphosphine oxides
RU2091385C1 (ru) 1991-09-23 1997-09-27 Циба-Гейги АГ Бисацилфосфиноксиды, состав и способ нанесения покрытий
ZA941879B (en) 1993-03-18 1994-09-19 Ciba Geigy Curing compositions containing bisacylphosphine oxide photoinitiators
TW381106B (en) * 1994-09-02 2000-02-01 Ciba Sc Holding Ag Alkoxyphenyl-substituted bisacylphosphine oxides
AU682793B2 (en) * 1994-09-08 1997-10-16 Ciba Specialty Chemicals Holding Inc. Novel acylphosphine oxides
TW323274B (enExample) * 1994-10-13 1997-12-21 Ciba Sc Holding Ag
AU760237B2 (en) * 1998-11-30 2003-05-08 Igm Group B.V. Process for preparing acylphosphines and derivatives
GB2360283B (en) * 2000-02-08 2002-08-21 Ciba Sc Holding Ag Monoacylarylphosphines and acylphosphine oxides and sulphides

Also Published As

Publication number Publication date
ATE221893T1 (de) 2002-08-15
US7094931B2 (en) 2006-08-22
EP1135399B1 (en) 2002-08-07
CN1328564A (zh) 2001-12-26
SK7272001A3 (en) 2001-12-03
CA2349637C (en) 2008-12-23
KR100653117B1 (ko) 2006-12-21
WO2000032612A1 (en) 2000-06-08
AU1384500A (en) 2000-06-19
CN1211388C (zh) 2005-07-20
EP1135399B2 (en) 2006-08-09
CA2349637A1 (en) 2000-06-08
DE69902485T2 (de) 2003-05-08
CZ302512B6 (cs) 2011-06-29
AU760237B2 (en) 2003-05-08
US6888031B1 (en) 2005-05-03
US7214830B2 (en) 2007-05-08
KR20010093124A (ko) 2001-10-27
JP4265871B2 (ja) 2009-05-20
US20040248855A1 (en) 2004-12-09
TW492972B (en) 2002-07-01
EP1135399A1 (en) 2001-09-26
DE69902485D1 (de) 2002-09-12
US20060128959A1 (en) 2006-06-15
ES2180347T3 (es) 2003-02-01
ES2180347T5 (es) 2007-04-01
JP2002531460A (ja) 2002-09-24
SK286152B6 (sk) 2008-04-07
CZ20011875A3 (cs) 2001-09-12

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Legal Events

Date Code Title Description
8363 Opposition against the patent
8366 Restricted maintained after opposition proceedings
8328 Change in the person/name/address of the agent

Representative=s name: PFENNING MEINIG & PARTNER GBR, 80339 MUENCHEN

8327 Change in the person/name/address of the patent owner

Owner name: CIBA HOLDING INC., BASEL, CH

8328 Change in the person/name/address of the agent

Representative=s name: MAIWALD PATENTANWALTSGESELLSCHAFT MBH, 80335 MUENC