CN1211388C - 酰基膦和其衍生物的制备方法 - Google Patents

酰基膦和其衍生物的制备方法 Download PDF

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Publication number
CN1211388C
CN1211388C CNB998137138A CN99813713A CN1211388C CN 1211388 C CN1211388 C CN 1211388C CN B998137138 A CNB998137138 A CN B998137138A CN 99813713 A CN99813713 A CN 99813713A CN 1211388 C CN1211388 C CN 1211388C
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CN
China
Prior art keywords
alkyl
phenyl
reaction
xenyl
alkoxyl group
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Expired - Lifetime
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CNB998137138A
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English (en)
Chinese (zh)
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CN1328564A (zh
Inventor
D·G·莱帕德
E·艾兴贝格尔
R·凯泽
G·胡格
U·施温迪曼
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IGM Group BV
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Ciba Spezialitaetenchemie Holding AG
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    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F9/00—Compounds containing elements of Groups 5 or 15 of the Periodic Table
    • C07F9/02—Phosphorus compounds
    • C07F9/28—Phosphorus compounds with one or more P—C bonds
    • C07F9/50—Organo-phosphines
    • C07F9/53—Organo-phosphine oxides; Organo-phosphine thioxides
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F9/00—Compounds containing elements of Groups 5 or 15 of the Periodic Table
    • C07F9/02—Phosphorus compounds
    • C07F9/28—Phosphorus compounds with one or more P—C bonds
    • C07F9/50—Organo-phosphines
    • C07F9/5036—Phosphines containing the structure -C(=X)-P or NC-P
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F9/00—Compounds containing elements of Groups 5 or 15 of the Periodic Table
    • C07F9/02—Phosphorus compounds
    • C07F9/28—Phosphorus compounds with one or more P—C bonds
    • C07F9/50—Organo-phosphines
    • C07F9/53—Organo-phosphine oxides; Organo-phosphine thioxides
    • C07F9/5337—Phosphine oxides or thioxides containing the structure -C(=X)-P(=X) or NC-P(=X) (X = O, S, Se)

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Biochemistry (AREA)
  • General Health & Medical Sciences (AREA)
  • Molecular Biology (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Saccharide Compounds (AREA)
  • Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
CNB998137138A 1998-11-30 1999-11-20 酰基膦和其衍生物的制备方法 Expired - Lifetime CN1211388C (zh)

Applications Claiming Priority (4)

Application Number Priority Date Filing Date Title
CH237698 1998-11-30
CH2376/1998 1998-11-30
CH2434/1998 1998-12-08
CH243498 1998-12-08

Publications (2)

Publication Number Publication Date
CN1328564A CN1328564A (zh) 2001-12-26
CN1211388C true CN1211388C (zh) 2005-07-20

Family

ID=25690294

Family Applications (1)

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CNB998137138A Expired - Lifetime CN1211388C (zh) 1998-11-30 1999-11-20 酰基膦和其衍生物的制备方法

Country Status (14)

Country Link
US (3) US6888031B1 (enExample)
EP (1) EP1135399B2 (enExample)
JP (1) JP4265871B2 (enExample)
KR (1) KR100653117B1 (enExample)
CN (1) CN1211388C (enExample)
AT (1) ATE221893T1 (enExample)
AU (1) AU760237B2 (enExample)
CA (1) CA2349637C (enExample)
CZ (1) CZ302512B6 (enExample)
DE (1) DE69902485T3 (enExample)
ES (1) ES2180347T5 (enExample)
SK (1) SK286152B6 (enExample)
TW (1) TW492972B (enExample)
WO (1) WO2000032612A1 (enExample)

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SK286152B6 (sk) * 1998-11-30 2008-04-07 Ciba Specialty Chemicals Holding Inc. Spôsob prípravy acylfosfínov, acylfosfínoxidov a acylfosfínsulfidov
GB2360283B (en) * 2000-02-08 2002-08-21 Ciba Sc Holding Ag Monoacylarylphosphines and acylphosphine oxides and sulphides
GB2365430B (en) 2000-06-08 2002-08-28 Ciba Sc Holding Ag Acylphosphine photoinitiators and intermediates
JP4225898B2 (ja) * 2001-08-21 2009-02-18 チバ ホールディング インコーポレーテッド 深色モノ−及びビス−アシルホスフィンオキシド及びスルフィド並びに光開始剤としてのこれらの使用
DE10206117A1 (de) 2002-02-13 2003-08-14 Basf Ag Acyl- und Bisacylphosphinderivate
DE10244684A1 (de) 2002-09-24 2004-04-01 Basf Ag Verfahren zur Herstellung von Acylphosphinoxiden
WO2004050668A1 (en) * 2002-12-04 2004-06-17 Ciba Specialty Chemicals Holding Inc. Process for the synthesis of cycloorganylphosphanes and di(alkali metal/alkaline earth metal) oligophosphanediides
DE10315671A1 (de) * 2003-04-04 2004-10-14 Basf Ag Verfahren zur Herstellung von Acylphosphinoxid-Feststoffen
CA2531318A1 (en) * 2003-07-18 2005-02-17 Ciba Specialty Chemicals Holding Inc. Process for preparing acylphosphanes and derivatives thereof
TW200523265A (en) * 2003-07-31 2005-07-16 Basf Ag A process for the preparation of acylphosphines
JP5148283B2 (ja) * 2004-11-23 2013-02-20 チバ ホールディング インコーポレーテッド アシルホスファン及びその誘導体の製造方法
US7470819B2 (en) 2005-01-17 2008-12-30 Ciba Specialty Chemicals Corporation Process for preparing acylphosphanes and their oxides and sulphides
DE102005005946A1 (de) * 2005-02-10 2006-08-17 Basf Ag Verfahren zur Herstellung tertiärer Phosphine
EP2342237B1 (en) 2008-11-03 2014-04-23 Basf Se Photoinitiator mixtures
CN102405239B (zh) * 2009-04-20 2014-10-15 瑞士联邦苏黎世技术大学 聚合物纳米颗粒
CN102875598B (zh) * 2011-07-11 2016-09-07 深圳市有为化学技术有限公司 (二苯膦氧基)(均三甲苯基)甲酮和(苯膦氧基)双(均三甲苯基甲酮)的制备方法
CN102875597B (zh) * 2011-07-11 2017-05-03 深圳市有为化学技术有限公司 芳香酮膦氧杂化型化合物
CN102675365A (zh) * 2012-05-16 2012-09-19 湖北固润科技股份有限公司 一种紫外光引发剂xbpo合成方法
GB201213163D0 (en) 2012-07-24 2012-09-05 Lambson Ltd Photopolymerisation processes and novel compounds therefor
WO2014053455A1 (en) 2012-10-01 2014-04-10 ETH Zürich A process for the preparation of acylphosphanes
WO2014140357A1 (en) 2013-03-15 2014-09-18 Freefly Systems Inc. Method and system for enabling pointing control of an actively stabilized camera
CN104592298B (zh) * 2014-12-31 2016-07-06 湖北固润科技股份有限公司 一种酰基膦高效光引发剂及其制备方法
CN105541913B (zh) * 2015-12-03 2017-08-25 天津久日新材料股份有限公司 一种2,4,6‑三甲基苯甲酰基二苯基氧化膦的制备方法
CN105732710A (zh) * 2016-03-16 2016-07-06 三峡大学 一种光引发剂联苯基四(2,4,6-三甲基苯甲酰基)氧化膦的制备方法及其应用
CN105732709A (zh) * 2016-03-16 2016-07-06 三峡大学 一种光引发剂2,4,6-三甲基苯甲酰二环己基氧膦，制备方法及其应用
CN107304220B (zh) * 2016-04-22 2020-03-31 江苏英力科技发展有限公司 一种“一锅法”合成2,4,6-三甲基苯甲酰基-二苯基氧化膦的方法
EP3296301A1 (en) * 2016-09-19 2018-03-21 ETH Zürich A versatile process for the preparation of acylphosphines
JP6916484B2 (ja) * 2017-03-28 2021-08-11 国立大学法人千葉大学 アシルホスフィンの製造方法
EP3409680B1 (en) 2017-05-30 2021-01-06 IGM Group B.V. Synthesis of bis(acyl)phosphines by activation of unreactive metal phosphides
EP3539924A1 (en) * 2018-03-14 2019-09-18 ETH Zurich Novel vinyl phosphines and photo-initiators obtainable therefrom
CN110734461A (zh) * 2018-07-20 2020-01-31 深圳市有为化学技术有限公司 化合物2,4,6-三甲基苯甲酰基二苯基氧化膦的制备
JP7432616B2 (ja) * 2018-12-07 2024-02-16 アンチン ライティング オプトエレクトロニクス テクノロジー カンパニー リミテッド アシルホスフィンオキシド化合物及びその調製方法
CN111138491B (zh) * 2019-12-31 2022-08-05 天津久日新材料股份有限公司 一种制备光引发剂tpo同时副产氯苄的方法
CN111087425B (zh) 2020-01-10 2022-04-19 天津大学 一种大粒度苯基双(2,4,6-三甲基苯甲酰基)氧化膦晶型及其结晶方法
CN112279940B (zh) * 2020-04-17 2023-06-27 山东科技大学 一种酰基膦光引发剂及其制备方法
CN112159429B (zh) * 2020-10-29 2022-06-21 天津久日新材料股份有限公司 一种双(2,4,6-三甲基苯甲酰基)苯基氧化膦的制备方法
WO2025140854A2 (en) 2023-12-28 2025-07-03 Igm Resins Italia S.R.L. NOVEL SOLID FORM OF BIS(2,4,6-TRIMETHYLBENZOYL)-n-OCTYL-PHOSPHINE OXIDE
JP7600464B1 (ja) * 2024-10-03 2024-12-16 サカタインクス株式会社 活性エネルギー線硬化型インクジェット印刷用インク

Family Cites Families (13)

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DE2909994A1 (de) 1979-03-14 1980-10-02 Basf Ag Acylphosphinoxidverbindungen, ihre herstellung und verwendung
EP0007086B1 (de) 1978-07-14 1982-02-10 BASF Aktiengesellschaft Lichthärtbare Form-, Tränk- und Überzugsmassen sowie daraus hergestellte Formkörper
DE3020092A1 (de) * 1980-05-27 1981-12-10 Basf Ag, 6700 Ludwigshafen Acylphosphinverbindungen und ihre verwendung
DE3034697A1 (de) 1980-09-15 1982-05-06 Basf Ag, 6700 Ludwigshafen Acylphosphinsulfidverbindungen, ihre herstellung und verwendung
DE3443221A1 (de) 1984-11-27 1986-06-05 ESPE Fabrik pharmazeutischer Präparate GmbH, 8031 Seefeld Bisacylphosphinoxide, ihre herstellung und verwendung
US5218009A (en) * 1989-08-04 1993-06-08 Ciba-Geigy Corporation Mono- and di-acylphosphine oxides
RU2091385C1 (ru) 1991-09-23 1997-09-27 Циба-Гейги АГ Бисацилфосфиноксиды, состав и способ нанесения покрытий
ZA941879B (en) 1993-03-18 1994-09-19 Ciba Geigy Curing compositions containing bisacylphosphine oxide photoinitiators
TW381106B (en) * 1994-09-02 2000-02-01 Ciba Sc Holding Ag Alkoxyphenyl-substituted bisacylphosphine oxides
MX9701734A (es) * 1994-09-08 1997-06-28 Ciba Sc Holding Ag Novedosos oxidos de acilfosfina.
TW323274B (enExample) * 1994-10-13 1997-12-21 Ciba Sc Holding Ag
SK286152B6 (sk) * 1998-11-30 2008-04-07 Ciba Specialty Chemicals Holding Inc. Spôsob prípravy acylfosfínov, acylfosfínoxidov a acylfosfínsulfidov
GB2360283B (en) * 2000-02-08 2002-08-21 Ciba Sc Holding Ag Monoacylarylphosphines and acylphosphine oxides and sulphides

Also Published As

Publication number Publication date
ATE221893T1 (de) 2002-08-15
JP2002531460A (ja) 2002-09-24
KR100653117B1 (ko) 2006-12-21
WO2000032612A1 (en) 2000-06-08
JP4265871B2 (ja) 2009-05-20
DE69902485T3 (de) 2007-03-15
DE69902485T2 (de) 2003-05-08
ES2180347T5 (es) 2007-04-01
US7094931B2 (en) 2006-08-22
SK286152B6 (sk) 2008-04-07
AU1384500A (en) 2000-06-19
KR20010093124A (ko) 2001-10-27
US20040248855A1 (en) 2004-12-09
CA2349637A1 (en) 2000-06-08
SK7272001A3 (en) 2001-12-03
EP1135399B2 (en) 2006-08-09
CN1328564A (zh) 2001-12-26
US20060128959A1 (en) 2006-06-15
CZ20011875A3 (cs) 2001-09-12
EP1135399B1 (en) 2002-08-07
CA2349637C (en) 2008-12-23
CZ302512B6 (cs) 2011-06-29
TW492972B (en) 2002-07-01
AU760237B2 (en) 2003-05-08
DE69902485D1 (de) 2002-09-12
EP1135399A1 (en) 2001-09-26
US6888031B1 (en) 2005-05-03
ES2180347T3 (es) 2003-02-01
US7214830B2 (en) 2007-05-08

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