DE69724147T2 - Herstellung von mit einer beschichtung aus bornitrid umhüllten faserigen vorformen, und von kompositen, die diese enthalten - Google Patents
Herstellung von mit einer beschichtung aus bornitrid umhüllten faserigen vorformen, und von kompositen, die diese enthalten Download PDFInfo
- Publication number
- DE69724147T2 DE69724147T2 DE69724147T DE69724147T DE69724147T2 DE 69724147 T2 DE69724147 T2 DE 69724147T2 DE 69724147 T DE69724147 T DE 69724147T DE 69724147 T DE69724147 T DE 69724147T DE 69724147 T2 DE69724147 T2 DE 69724147T2
- Authority
- DE
- Germany
- Prior art keywords
- borazine
- polycondensed
- preforms
- fiber preforms
- coating
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
- 238000000576 coating method Methods 0.000 title claims description 48
- 239000011248 coating agent Substances 0.000 title claims description 42
- 239000002131 composite material Substances 0.000 title claims description 19
- 238000004519 manufacturing process Methods 0.000 title claims description 19
- 239000000835 fiber Substances 0.000 claims description 72
- BGECDVWSWDRFSP-UHFFFAOYSA-N borazine Chemical compound B1NBNBN1 BGECDVWSWDRFSP-UHFFFAOYSA-N 0.000 claims description 61
- 229910052582 BN Inorganic materials 0.000 claims description 44
- PZNSFCLAULLKQX-UHFFFAOYSA-N Boron nitride Chemical compound N#B PZNSFCLAULLKQX-UHFFFAOYSA-N 0.000 claims description 44
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 claims description 37
- 230000016507 interphase Effects 0.000 claims description 36
- 238000000034 method Methods 0.000 claims description 31
- 238000006116 polymerization reaction Methods 0.000 claims description 26
- WYURNTSHIVDZCO-UHFFFAOYSA-N Tetrahydrofuran Chemical compound C1CCOC1 WYURNTSHIVDZCO-UHFFFAOYSA-N 0.000 claims description 22
- XTHFKEDIFFGKHM-UHFFFAOYSA-N Dimethoxyethane Chemical compound COCCOC XTHFKEDIFFGKHM-UHFFFAOYSA-N 0.000 claims description 21
- XKRFYHLGVUSROY-UHFFFAOYSA-N Argon Chemical compound [Ar] XKRFYHLGVUSROY-UHFFFAOYSA-N 0.000 claims description 20
- 238000005470 impregnation Methods 0.000 claims description 20
- 239000011159 matrix material Substances 0.000 claims description 20
- 238000000197 pyrolysis Methods 0.000 claims description 19
- 229910021529 ammonia Inorganic materials 0.000 claims description 17
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 claims description 16
- 230000006835 compression Effects 0.000 claims description 11
- 238000007906 compression Methods 0.000 claims description 11
- YLQBMQCUIZJEEH-UHFFFAOYSA-N tetrahydrofuran Natural products C=1C=COC=1 YLQBMQCUIZJEEH-UHFFFAOYSA-N 0.000 claims description 11
- 229910052786 argon Inorganic materials 0.000 claims description 10
- 239000012298 atmosphere Substances 0.000 claims description 8
- 229910052757 nitrogen Inorganic materials 0.000 claims description 8
- 230000008569 process Effects 0.000 claims description 7
- 239000000126 substance Substances 0.000 claims description 7
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 claims description 5
- 239000001301 oxygen Substances 0.000 claims description 5
- 229910052760 oxygen Inorganic materials 0.000 claims description 5
- 125000000217 alkyl group Chemical group 0.000 claims description 4
- 150000004985 diamines Chemical class 0.000 claims description 4
- 230000008595 infiltration Effects 0.000 claims description 3
- 238000001764 infiltration Methods 0.000 claims description 3
- 150000003141 primary amines Chemical group 0.000 claims description 3
- 150000003335 secondary amines Chemical class 0.000 claims description 3
- 125000004432 carbon atom Chemical group C* 0.000 claims description 2
- 201000006747 infectious mononucleosis Diseases 0.000 claims description 2
- 230000000379 polymerizing effect Effects 0.000 claims description 2
- 239000012783 reinforcing fiber Substances 0.000 claims description 2
- 239000003795 chemical substances by application Substances 0.000 claims 2
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- 239000000243 solution Substances 0.000 description 23
- HBMJWWWQQXIZIP-UHFFFAOYSA-N silicon carbide Chemical compound [Si+]#[C-] HBMJWWWQQXIZIP-UHFFFAOYSA-N 0.000 description 16
- 229910010271 silicon carbide Inorganic materials 0.000 description 14
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 13
- 238000006243 chemical reaction Methods 0.000 description 11
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- CVSVTCORWBXHQV-UHFFFAOYSA-N creatine Chemical compound NC(=[NH2+])N(C)CC([O-])=O CVSVTCORWBXHQV-UHFFFAOYSA-N 0.000 description 7
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- 239000012071 phase Substances 0.000 description 7
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- PIICEJLVQHRZGT-UHFFFAOYSA-N Ethylenediamine Chemical compound NCCN PIICEJLVQHRZGT-UHFFFAOYSA-N 0.000 description 5
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- 239000011347 resin Substances 0.000 description 3
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- UFWIBTONFRDIAS-UHFFFAOYSA-N Naphthalene Chemical compound C1=CC=CC2=CC=CC=C21 UFWIBTONFRDIAS-UHFFFAOYSA-N 0.000 description 2
- 239000011184 SiC–SiC matrix composite Substances 0.000 description 2
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 2
- TZCXTZWJZNENPQ-UHFFFAOYSA-L barium sulfate Chemical compound [Ba+2].[O-]S([O-])(=O)=O TZCXTZWJZNENPQ-UHFFFAOYSA-L 0.000 description 2
- 230000015572 biosynthetic process Effects 0.000 description 2
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- HPALAKNZSZLMCH-UHFFFAOYSA-M sodium;chloride;hydrate Chemical compound O.[Na+].[Cl-] HPALAKNZSZLMCH-UHFFFAOYSA-M 0.000 description 2
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- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 2
- 238000009941 weaving Methods 0.000 description 2
- WADSJYLPJPTMLN-UHFFFAOYSA-N 3-(cycloundecen-1-yl)-1,2-diazacycloundec-2-ene Chemical compound C1CCCCCCCCC=C1C1=NNCCCCCCCC1 WADSJYLPJPTMLN-UHFFFAOYSA-N 0.000 description 1
- HLJKQKZGVOYDJX-UHFFFAOYSA-N C1=CC=CC2=CC=NB=C21 Chemical compound C1=CC=CC2=CC=NB=C21 HLJKQKZGVOYDJX-UHFFFAOYSA-N 0.000 description 1
- 241000287828 Gallus gallus Species 0.000 description 1
- BAVYZALUXZFZLV-UHFFFAOYSA-N Methylamine Chemical compound NC BAVYZALUXZFZLV-UHFFFAOYSA-N 0.000 description 1
- ISWSIDIOOBJBQZ-UHFFFAOYSA-N Phenol Chemical compound OC1=CC=CC=C1 ISWSIDIOOBJBQZ-UHFFFAOYSA-N 0.000 description 1
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- 229920006362 Teflon® Polymers 0.000 description 1
- 238000002441 X-ray diffraction Methods 0.000 description 1
- 239000000443 aerosol Substances 0.000 description 1
- 150000001412 amines Chemical class 0.000 description 1
- TVJORGWKNPGCDW-UHFFFAOYSA-N aminoboron Chemical compound N[B] TVJORGWKNPGCDW-UHFFFAOYSA-N 0.000 description 1
- 230000003321 amplification Effects 0.000 description 1
- 238000005452 bending Methods 0.000 description 1
- KKAXNAVSOBXHTE-UHFFFAOYSA-N boranamine Chemical compound NB KKAXNAVSOBXHTE-UHFFFAOYSA-N 0.000 description 1
- KGBXLFKZBHKPEV-UHFFFAOYSA-N boric acid Chemical compound OB(O)O KGBXLFKZBHKPEV-UHFFFAOYSA-N 0.000 description 1
- 239000004327 boric acid Substances 0.000 description 1
- HQABUPZFAYXKJW-UHFFFAOYSA-N butan-1-amine Chemical compound CCCCN HQABUPZFAYXKJW-UHFFFAOYSA-N 0.000 description 1
- 238000004364 calculation method Methods 0.000 description 1
- 210000003850 cellular structure Anatomy 0.000 description 1
- 229910010293 ceramic material Inorganic materials 0.000 description 1
- 239000012700 ceramic precursor Substances 0.000 description 1
- 239000007795 chemical reaction product Substances 0.000 description 1
- 238000005056 compaction Methods 0.000 description 1
- 238000009833 condensation Methods 0.000 description 1
- 230000005494 condensation Effects 0.000 description 1
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- 238000000280 densification Methods 0.000 description 1
- 230000001419 dependent effect Effects 0.000 description 1
- 238000010790 dilution Methods 0.000 description 1
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- 238000001035 drying Methods 0.000 description 1
- 230000008030 elimination Effects 0.000 description 1
- 238000003379 elimination reaction Methods 0.000 description 1
- 230000007717 exclusion Effects 0.000 description 1
- 238000000605 extraction Methods 0.000 description 1
- 239000012634 fragment Substances 0.000 description 1
- 239000008187 granular material Substances 0.000 description 1
- 150000002431 hydrogen Chemical class 0.000 description 1
- 239000000411 inducer Substances 0.000 description 1
- 230000006698 induction Effects 0.000 description 1
- 239000011261 inert gas Substances 0.000 description 1
- 238000011835 investigation Methods 0.000 description 1
- JJWLVOIRVHMVIS-UHFFFAOYSA-N isopropylamine Chemical compound CC(C)N JJWLVOIRVHMVIS-UHFFFAOYSA-N 0.000 description 1
- 238000011068 loading method Methods 0.000 description 1
- 230000007774 longterm Effects 0.000 description 1
- 229920002521 macromolecule Polymers 0.000 description 1
- 238000004949 mass spectrometry Methods 0.000 description 1
- OETHQSJEHLVLGH-UHFFFAOYSA-N metformin hydrochloride Chemical compound Cl.CN(C)C(=N)N=C(N)N OETHQSJEHLVLGH-UHFFFAOYSA-N 0.000 description 1
- VNWKTOKETHGBQD-UHFFFAOYSA-N methane Chemical compound C VNWKTOKETHGBQD-UHFFFAOYSA-N 0.000 description 1
- 238000001000 micrograph Methods 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 150000004767 nitrides Chemical class 0.000 description 1
- 239000012299 nitrogen atmosphere Substances 0.000 description 1
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- 238000007142 ring opening reaction Methods 0.000 description 1
- 239000000377 silicon dioxide Substances 0.000 description 1
- DVQHRBFGRZHMSR-UHFFFAOYSA-N sodium methyl 2,2-dimethyl-4,6-dioxo-5-(N-prop-2-enoxy-C-propylcarbonimidoyl)cyclohexane-1-carboxylate Chemical compound [Na+].C=CCON=C(CCC)[C-]1C(=O)CC(C)(C)C(C(=O)OC)C1=O DVQHRBFGRZHMSR-UHFFFAOYSA-N 0.000 description 1
- 238000013517 stratification Methods 0.000 description 1
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- 150000003512 tertiary amines Chemical class 0.000 description 1
- 238000012360 testing method Methods 0.000 description 1
- 238000001149 thermolysis Methods 0.000 description 1
- 238000004804 winding Methods 0.000 description 1
Classifications
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- C04B35/00—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
- C04B35/622—Forming processes; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
- C04B35/626—Preparing or treating the powders individually or as batches ; preparing or treating macroscopic reinforcing agents for ceramic products, e.g. fibres; mechanical aspects section B
- C04B35/628—Coating the powders or the macroscopic reinforcing agents
- C04B35/62844—Coating fibres
- C04B35/62857—Coating fibres with non-oxide ceramics
- C04B35/62865—Nitrides
- C04B35/62868—Boron nitride
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- C04B35/515—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on non-oxide ceramics
- C04B35/56—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on non-oxide ceramics based on carbides or oxycarbides
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- C04B35/62897—Coatings characterised by their thickness
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- C04B35/00—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
- C04B35/71—Ceramic products containing macroscopic reinforcing agents
- C04B35/78—Ceramic products containing macroscopic reinforcing agents containing non-metallic materials
- C04B35/80—Fibres, filaments, whiskers, platelets, or the like
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- C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
- C04B41/009—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone characterised by the material treated
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- C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
- C04B41/45—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements
- C04B41/4584—Coating or impregnating of particulate or fibrous ceramic material
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- C04B41/45—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements
- C04B41/50—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements with inorganic materials
- C04B41/5053—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements with inorganic materials non-oxide ceramics
- C04B41/5062—Borides, Nitrides or Silicides
- C04B41/5064—Boron nitride
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- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
- C04B2235/30—Constituents and secondary phases not being of a fibrous nature
- C04B2235/48—Organic compounds becoming part of a ceramic after heat treatment, e.g. carbonising phenol resins
- C04B2235/486—Boron containing organic compounds, e.g. borazine, borane or boranyl
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- C04B2235/524—Non-oxidic, e.g. borides, carbides, silicides or nitrides
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- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/60—Aspects relating to the preparation, properties or mechanical treatment of green bodies or pre-forms
- C04B2235/614—Gas infiltration of green bodies or pre-forms
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- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/65—Aspects relating to heat treatments of ceramic bodies such as green ceramics or pre-sintered ceramics, e.g. burning, sintering or melting processes
- C04B2235/656—Aspects relating to heat treatments of ceramic bodies such as green ceramics or pre-sintered ceramics, e.g. burning, sintering or melting processes characterised by specific heating conditions during heat treatment
- C04B2235/6562—Heating rate
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
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- Y10T428/00—Stock material or miscellaneous articles
- Y10T428/249921—Web or sheet containing structurally defined element or component
- Y10T428/249924—Noninterengaged fiber-containing paper-free web or sheet which is not of specified porosity
- Y10T428/249928—Fiber embedded in a ceramic, glass, or carbon matrix
- Y10T428/249931—Free metal or alloy fiber
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- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Ceramic Engineering (AREA)
- Materials Engineering (AREA)
- Structural Engineering (AREA)
- Organic Chemistry (AREA)
- Manufacturing & Machinery (AREA)
- Inorganic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Ceramic Products (AREA)
- Chemical Or Physical Treatment Of Fibers (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| FR9616104 | 1996-12-27 | ||
| FR9616104A FR2757848B1 (fr) | 1996-12-27 | 1996-12-27 | Preformes fibreuses gainees d'un revetement bn original, composites les incorporant et leurs preparations |
| PCT/FR1997/002423 WO1998029355A1 (fr) | 1996-12-27 | 1997-12-24 | Preformes fibreuses gainees d'un revetement en nitrure de bore, composites les incorporant et leurs preparations |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| DE69724147D1 DE69724147D1 (de) | 2003-09-18 |
| DE69724147T2 true DE69724147T2 (de) | 2004-06-03 |
Family
ID=9499212
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE69724147T Expired - Fee Related DE69724147T2 (de) | 1996-12-27 | 1997-12-24 | Herstellung von mit einer beschichtung aus bornitrid umhüllten faserigen vorformen, und von kompositen, die diese enthalten |
Country Status (8)
| Country | Link |
|---|---|
| US (1) | US6284358B1 (enExample) |
| EP (1) | EP0952969B1 (enExample) |
| JP (1) | JP3987123B2 (enExample) |
| CA (1) | CA2279500C (enExample) |
| DE (1) | DE69724147T2 (enExample) |
| ES (1) | ES2205277T3 (enExample) |
| FR (1) | FR2757848B1 (enExample) |
| WO (1) | WO1998029355A1 (enExample) |
Families Citing this family (24)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US7150911B2 (en) * | 2001-02-08 | 2006-12-19 | Showa Denko Kabushiki Kaisha | Electrical insulating vapor grown carbon fiber and method for producing the same, and use thereof |
| JP3778045B2 (ja) * | 2001-10-09 | 2006-05-24 | 三菱電機株式会社 | 低誘電率材料の製造方法および低誘電率材料、並びにこの低誘電率材料を用いた絶縁膜および半導体装置 |
| JP4441617B2 (ja) * | 2004-08-09 | 2010-03-31 | 独立行政法人物質・材料研究機構 | 窒化アルミニウムナノチューブ及びその製造方法 |
| US7867554B2 (en) * | 2005-01-06 | 2011-01-11 | United Technologies Corporation | Boron nitride coated fibers and composite articles containing same |
| FR2882356B1 (fr) * | 2005-02-23 | 2008-08-15 | Snecma Propulsion Solide Sa | Procede de fabrication de piece en materiau composite a matrice ceramique et piece ainsi obtenue |
| JP4670100B2 (ja) * | 2006-03-01 | 2011-04-13 | 独立行政法人物質・材料研究機構 | 窒化ホウ素ナノチューブの精製方法 |
| JP4915929B2 (ja) * | 2007-03-27 | 2012-04-11 | 独立行政法人産業技術総合研究所 | ボラジン・ジアミン系重合体及びそのための重合性組成物、並びにその製造方法 |
| JP4915930B2 (ja) * | 2007-03-27 | 2012-04-11 | 独立行政法人産業技術総合研究所 | ボラジン・ジアミン系ポリマー薄膜形成用組成物及びボラジン・ジアミン系ポリマー薄膜の製造方法 |
| US20100192535A1 (en) * | 2009-02-04 | 2010-08-05 | Smith Michael W | Boron nitride nanotube fibrils and yarns |
| FR3008968B1 (fr) | 2013-07-23 | 2016-12-09 | Herakles | Procede de fabrication de pieces en materiau composite par impregnation a basse temperature de fusion |
| FR3037973B1 (fr) * | 2015-06-24 | 2019-09-06 | Safran Ceramics | Procede de traitement de fibres de carbure de silicium |
| FR3063725B1 (fr) | 2017-03-07 | 2019-04-12 | Safran Ceramics | Procede de realisation d'une preforme fibreuse consolidee |
| CN107353025B (zh) * | 2017-06-27 | 2020-10-20 | 中航复合材料有限责任公司 | 一种耐1200℃抗氧化的陶瓷基复合材料的制备方法 |
| WO2020025878A1 (fr) | 2018-08-03 | 2020-02-06 | Safran Ceramics | Procede de fabrication d'une piece en cmc |
| FR3120811B1 (fr) | 2021-03-18 | 2023-03-17 | Safran Ceram | Procédé amélioré de réalisation d'une préforme fibreuse consolidée |
| FR3124507B1 (fr) * | 2021-06-23 | 2023-10-27 | Safran Ceram | Procédé de revêtement d’au moins une fibre par une interphase de nitrure de bore |
| FR3130273B1 (fr) | 2021-12-10 | 2023-12-15 | Safran Ceram | Procédé de fabrication d’une pièce en matériau composite SiC/SiC |
| CN114804907A (zh) * | 2022-05-27 | 2022-07-29 | 陕西美兰德炭素有限责任公司 | 一种制备氮化硼改性的炭/炭复合材料制品的方法及制品 |
| FR3147804A1 (fr) | 2023-04-12 | 2024-10-18 | Safran Ceramics | Consolidation d’une préforme fibreuse |
| FR3147805A1 (fr) | 2023-04-12 | 2024-10-18 | Safran Ceramics | Consolidation d’une préforme fibreuse |
| CN117586034B (zh) * | 2023-11-08 | 2025-08-15 | 航天特种材料及工艺技术研究所 | 一种宽温域可重复使用高导热复合材料及其制备方法 |
| CN117645499B (zh) * | 2023-11-29 | 2025-08-08 | 西安理工大学 | 一种具有多层结构的bn纤维基多孔陶瓷的制备方法 |
| FR3157384A1 (fr) | 2023-12-21 | 2025-06-27 | Safran Ceramics | Procédé de fabrication d'une aube par infiltration chimique en phase vapeur |
| CN121673073B (zh) * | 2026-02-10 | 2026-04-14 | 江西昌兴航空装备股份有限公司 | 一种耐超高温抗磨损陶瓷基复合材料及其制备方法 |
Family Cites Families (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS6147735A (ja) * | 1984-08-11 | 1986-03-08 | Isoji Taniguchi | 有機窒化ホウ素重合体の製造法 |
| FR2640258B1 (fr) * | 1988-05-10 | 1991-06-07 | Europ Propulsion | Procede de fabrication de materiaux composites a renfort en fibres de carbure de silicium et a matrice ceramique |
| US5204295A (en) * | 1989-02-17 | 1993-04-20 | University Of New Mexico | Precursors for boron nitride coatings |
| US5502142A (en) * | 1990-03-09 | 1996-03-26 | The Trustees Of The University Of Pennsylvania | Direct thermal synthesis and ceramic applications of poly(borazylenes) |
| FR2659321B1 (fr) * | 1990-03-12 | 1992-05-22 | Rhone Poulenc Chimie | Procede de revetements en ceramique de pieces a base de carbone. |
-
1996
- 1996-12-27 FR FR9616104A patent/FR2757848B1/fr not_active Expired - Fee Related
-
1997
- 1997-12-24 JP JP52969698A patent/JP3987123B2/ja not_active Expired - Lifetime
- 1997-12-24 CA CA002279500A patent/CA2279500C/en not_active Expired - Fee Related
- 1997-12-24 EP EP97953947A patent/EP0952969B1/fr not_active Expired - Lifetime
- 1997-12-24 DE DE69724147T patent/DE69724147T2/de not_active Expired - Fee Related
- 1997-12-24 WO PCT/FR1997/002423 patent/WO1998029355A1/fr not_active Ceased
- 1997-12-24 ES ES97953947T patent/ES2205277T3/es not_active Expired - Lifetime
- 1997-12-24 US US09/331,726 patent/US6284358B1/en not_active Expired - Fee Related
Also Published As
| Publication number | Publication date |
|---|---|
| FR2757848A1 (fr) | 1998-07-03 |
| JP3987123B2 (ja) | 2007-10-03 |
| ES2205277T3 (es) | 2004-05-01 |
| FR2757848B1 (fr) | 1999-03-26 |
| EP0952969B1 (fr) | 2003-08-13 |
| DE69724147D1 (de) | 2003-09-18 |
| EP0952969A1 (fr) | 1999-11-03 |
| CA2279500C (en) | 2006-04-04 |
| JP2001507328A (ja) | 2001-06-05 |
| WO1998029355A1 (fr) | 1998-07-09 |
| US6284358B1 (en) | 2001-09-04 |
| CA2279500A1 (fr) | 1998-07-09 |
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| Date | Code | Title | Description |
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| 8364 | No opposition during term of opposition | ||
| 8339 | Ceased/non-payment of the annual fee |