JP3987123B2 - 窒化ホウ素コーティングで被覆された布帛予備成形体、それを組み込んだ複合材料およびその製造方法 - Google Patents
窒化ホウ素コーティングで被覆された布帛予備成形体、それを組み込んだ複合材料およびその製造方法 Download PDFInfo
- Publication number
- JP3987123B2 JP3987123B2 JP52969698A JP52969698A JP3987123B2 JP 3987123 B2 JP3987123 B2 JP 3987123B2 JP 52969698 A JP52969698 A JP 52969698A JP 52969698 A JP52969698 A JP 52969698A JP 3987123 B2 JP3987123 B2 JP 3987123B2
- Authority
- JP
- Japan
- Prior art keywords
- fiber preform
- fiber
- preform
- coating
- boron nitride
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
- 238000000576 coating method Methods 0.000 title claims description 55
- 239000011248 coating agent Substances 0.000 title claims description 49
- 239000002131 composite material Substances 0.000 title claims description 20
- 229910052582 BN Inorganic materials 0.000 title claims description 18
- PZNSFCLAULLKQX-UHFFFAOYSA-N Boron nitride Chemical compound N#B PZNSFCLAULLKQX-UHFFFAOYSA-N 0.000 title claims description 17
- 238000004519 manufacturing process Methods 0.000 title claims description 8
- 239000004744 fabric Substances 0.000 title description 5
- 239000000835 fiber Substances 0.000 claims description 87
- 238000000034 method Methods 0.000 claims description 43
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 claims description 37
- BGECDVWSWDRFSP-UHFFFAOYSA-N borazine Chemical compound B1NBNBN1 BGECDVWSWDRFSP-UHFFFAOYSA-N 0.000 claims description 30
- 230000016507 interphase Effects 0.000 claims description 28
- 238000006116 polymerization reaction Methods 0.000 claims description 26
- WYURNTSHIVDZCO-UHFFFAOYSA-N Tetrahydrofuran Chemical compound C1CCOC1 WYURNTSHIVDZCO-UHFFFAOYSA-N 0.000 claims description 24
- XKRFYHLGVUSROY-UHFFFAOYSA-N Argon Chemical compound [Ar] XKRFYHLGVUSROY-UHFFFAOYSA-N 0.000 claims description 20
- HBMJWWWQQXIZIP-UHFFFAOYSA-N silicon carbide Chemical compound [Si+]#[C-] HBMJWWWQQXIZIP-UHFFFAOYSA-N 0.000 claims description 20
- 229910010271 silicon carbide Inorganic materials 0.000 claims description 18
- 239000011159 matrix material Substances 0.000 claims description 17
- 238000000197 pyrolysis Methods 0.000 claims description 17
- 229910021529 ammonia Inorganic materials 0.000 claims description 16
- 238000005470 impregnation Methods 0.000 claims description 15
- 239000000243 solution Substances 0.000 claims description 15
- 239000000126 substance Substances 0.000 claims description 13
- YLQBMQCUIZJEEH-UHFFFAOYSA-N tetrahydrofuran Natural products C=1C=COC=1 YLQBMQCUIZJEEH-UHFFFAOYSA-N 0.000 claims description 11
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 claims description 10
- 229910052786 argon Inorganic materials 0.000 claims description 10
- 239000007864 aqueous solution Substances 0.000 claims description 9
- 239000012298 atmosphere Substances 0.000 claims description 8
- 239000000411 inducer Substances 0.000 claims description 8
- 230000002787 reinforcement Effects 0.000 claims description 7
- 239000000919 ceramic Substances 0.000 claims description 6
- 238000009833 condensation Methods 0.000 claims description 6
- 230000005494 condensation Effects 0.000 claims description 6
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 claims description 5
- 239000000463 material Substances 0.000 claims description 5
- 229910052757 nitrogen Inorganic materials 0.000 claims description 5
- 239000001301 oxygen Substances 0.000 claims description 5
- 229910052760 oxygen Inorganic materials 0.000 claims description 5
- 229920000049 Carbon (fiber) Polymers 0.000 claims description 4
- 125000000217 alkyl group Chemical group 0.000 claims description 4
- 239000004917 carbon fiber Substances 0.000 claims description 4
- 150000004985 diamines Chemical class 0.000 claims description 3
- 239000006260 foam Substances 0.000 claims description 3
- 150000003335 secondary amines Chemical class 0.000 claims description 3
- 125000004432 carbon atom Chemical group C* 0.000 claims description 2
- 201000006747 infectious mononucleosis Diseases 0.000 claims description 2
- 150000004767 nitrides Chemical class 0.000 claims description 2
- 230000000379 polymerizing effect Effects 0.000 claims description 2
- 150000003141 primary amines Chemical class 0.000 claims description 2
- 239000004753 textile Substances 0.000 claims 3
- UZZWBUYVTBPQIV-UHFFFAOYSA-N dme dimethoxyethane Chemical compound COCCOC.COCCOC UZZWBUYVTBPQIV-UHFFFAOYSA-N 0.000 claims 2
- -1 carbide Substances 0.000 claims 1
- 238000001035 drying Methods 0.000 claims 1
- 230000008569 process Effects 0.000 description 16
- 229920000642 polymer Polymers 0.000 description 14
- XTHFKEDIFFGKHM-UHFFFAOYSA-N Dimethoxyethane Chemical compound COCCOC XTHFKEDIFFGKHM-UHFFFAOYSA-N 0.000 description 11
- 238000006243 chemical reaction Methods 0.000 description 11
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 10
- 238000009835 boiling Methods 0.000 description 10
- 239000012071 phase Substances 0.000 description 10
- 239000002243 precursor Substances 0.000 description 10
- 230000007246 mechanism Effects 0.000 description 9
- 239000000047 product Substances 0.000 description 8
- 229910052799 carbon Inorganic materials 0.000 description 7
- 238000000280 densification Methods 0.000 description 7
- 239000007789 gas Substances 0.000 description 6
- 238000010438 heat treatment Methods 0.000 description 6
- 230000003014 reinforcing effect Effects 0.000 description 6
- 239000002904 solvent Substances 0.000 description 6
- 239000007791 liquid phase Substances 0.000 description 5
- 238000002360 preparation method Methods 0.000 description 5
- PIICEJLVQHRZGT-UHFFFAOYSA-N Ethylenediamine Chemical compound NCCN PIICEJLVQHRZGT-UHFFFAOYSA-N 0.000 description 4
- 238000013459 approach Methods 0.000 description 4
- 230000001413 cellular effect Effects 0.000 description 4
- 239000003153 chemical reaction reagent Substances 0.000 description 4
- 229910002804 graphite Inorganic materials 0.000 description 4
- 239000010439 graphite Substances 0.000 description 4
- 239000001257 hydrogen Substances 0.000 description 4
- 229910052739 hydrogen Inorganic materials 0.000 description 4
- 230000006698 induction Effects 0.000 description 4
- 239000000543 intermediate Substances 0.000 description 4
- 239000007788 liquid Substances 0.000 description 4
- 239000000203 mixture Substances 0.000 description 4
- 239000002296 pyrolytic carbon Substances 0.000 description 4
- 238000005979 thermal decomposition reaction Methods 0.000 description 4
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical class O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 3
- 230000015572 biosynthetic process Effects 0.000 description 3
- 239000011153 ceramic matrix composite Substances 0.000 description 3
- 238000005516 engineering process Methods 0.000 description 3
- 238000001704 evaporation Methods 0.000 description 3
- 230000008020 evaporation Effects 0.000 description 3
- 238000001000 micrograph Methods 0.000 description 3
- 239000012783 reinforcing fiber Substances 0.000 description 3
- 239000011347 resin Substances 0.000 description 3
- 229920005989 resin Polymers 0.000 description 3
- 238000005728 strengthening Methods 0.000 description 3
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 description 2
- UFWIBTONFRDIAS-UHFFFAOYSA-N Naphthalene Chemical compound C1=CC=CC2=CC=CC=C21 UFWIBTONFRDIAS-UHFFFAOYSA-N 0.000 description 2
- 238000004132 cross linking Methods 0.000 description 2
- 238000000151 deposition Methods 0.000 description 2
- 238000007598 dipping method Methods 0.000 description 2
- 239000008187 granular material Substances 0.000 description 2
- 150000002431 hydrogen Chemical class 0.000 description 2
- 239000011261 inert gas Substances 0.000 description 2
- 230000008595 infiltration Effects 0.000 description 2
- 238000001764 infiltration Methods 0.000 description 2
- VNWKTOKETHGBQD-UHFFFAOYSA-N methane Chemical compound C VNWKTOKETHGBQD-UHFFFAOYSA-N 0.000 description 2
- 239000000178 monomer Substances 0.000 description 2
- 230000000750 progressive effect Effects 0.000 description 2
- 239000000376 reactant Substances 0.000 description 2
- 238000003756 stirring Methods 0.000 description 2
- 238000012360 testing method Methods 0.000 description 2
- 238000012546 transfer Methods 0.000 description 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 2
- 238000009941 weaving Methods 0.000 description 2
- WADSJYLPJPTMLN-UHFFFAOYSA-N 3-(cycloundecen-1-yl)-1,2-diazacycloundec-2-ene Chemical compound C1CCCCCCCCC=C1C1=NNCCCCCCCC1 WADSJYLPJPTMLN-UHFFFAOYSA-N 0.000 description 1
- HLJKQKZGVOYDJX-UHFFFAOYSA-N C1=CC=CC2=CC=NB=C21 Chemical compound C1=CC=CC2=CC=NB=C21 HLJKQKZGVOYDJX-UHFFFAOYSA-N 0.000 description 1
- BAVYZALUXZFZLV-UHFFFAOYSA-N Methylamine Chemical compound NC BAVYZALUXZFZLV-UHFFFAOYSA-N 0.000 description 1
- 239000011184 SiC–SiC matrix composite Substances 0.000 description 1
- 239000004809 Teflon Substances 0.000 description 1
- 229920006362 Teflon® Polymers 0.000 description 1
- 230000009471 action Effects 0.000 description 1
- 239000000443 aerosol Substances 0.000 description 1
- 150000001412 amines Chemical class 0.000 description 1
- TVJORGWKNPGCDW-UHFFFAOYSA-N aminoboron Chemical compound N[B] TVJORGWKNPGCDW-UHFFFAOYSA-N 0.000 description 1
- 239000012300 argon atmosphere Substances 0.000 description 1
- 238000005452 bending Methods 0.000 description 1
- 230000002457 bidirectional effect Effects 0.000 description 1
- KGBXLFKZBHKPEV-UHFFFAOYSA-N boric acid Chemical compound OB(O)O KGBXLFKZBHKPEV-UHFFFAOYSA-N 0.000 description 1
- 239000004327 boric acid Substances 0.000 description 1
- 229910010293 ceramic material Inorganic materials 0.000 description 1
- 239000012700 ceramic precursor Substances 0.000 description 1
- 238000005229 chemical vapour deposition Methods 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 238000007796 conventional method Methods 0.000 description 1
- 230000008021 deposition Effects 0.000 description 1
- 238000001212 derivatisation Methods 0.000 description 1
- 150000002170 ethers Chemical class 0.000 description 1
- 238000011049 filling Methods 0.000 description 1
- 239000012467 final product Substances 0.000 description 1
- 239000012210 heat-resistant fiber Substances 0.000 description 1
- 230000007062 hydrolysis Effects 0.000 description 1
- 238000006460 hydrolysis reaction Methods 0.000 description 1
- 238000007689 inspection Methods 0.000 description 1
- 238000011068 loading method Methods 0.000 description 1
- 238000004949 mass spectrometry Methods 0.000 description 1
- 239000002184 metal Substances 0.000 description 1
- 239000011859 microparticle Substances 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- 239000010413 mother solution Substances 0.000 description 1
- 230000003647 oxidation Effects 0.000 description 1
- 238000007254 oxidation reaction Methods 0.000 description 1
- ISWSIDIOOBJBQZ-UHFFFAOYSA-N phenol group Chemical group C1(=CC=CC=C1)O ISWSIDIOOBJBQZ-UHFFFAOYSA-N 0.000 description 1
- 229920003203 poly(dimethylsilylene-co-phenylmethyl- silylene) polymer Polymers 0.000 description 1
- 239000011148 porous material Substances 0.000 description 1
- 239000002244 precipitate Substances 0.000 description 1
- 238000012545 processing Methods 0.000 description 1
- 239000012495 reaction gas Substances 0.000 description 1
- 239000011541 reaction mixture Substances 0.000 description 1
- 230000009257 reactivity Effects 0.000 description 1
- 238000010992 reflux Methods 0.000 description 1
- 230000000717 retained effect Effects 0.000 description 1
- 230000000630 rising effect Effects 0.000 description 1
- 238000013207 serial dilution Methods 0.000 description 1
- 239000000377 silicon dioxide Substances 0.000 description 1
- 229910052814 silicon oxide Inorganic materials 0.000 description 1
- DVQHRBFGRZHMSR-UHFFFAOYSA-N sodium methyl 2,2-dimethyl-4,6-dioxo-5-(N-prop-2-enoxy-C-propylcarbonimidoyl)cyclohexane-1-carboxylate Chemical compound [Na+].C=CCON=C(CCC)[C-]1C(=O)CC(C)(C)C(C(=O)OC)C1=O DVQHRBFGRZHMSR-UHFFFAOYSA-N 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 238000003786 synthesis reaction Methods 0.000 description 1
- 230000002194 synthesizing effect Effects 0.000 description 1
- 150000003512 tertiary amines Chemical class 0.000 description 1
Images
Classifications
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B35/00—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
- C04B35/622—Forming processes; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
- C04B35/626—Preparing or treating the powders individually or as batches ; preparing or treating macroscopic reinforcing agents for ceramic products, e.g. fibres; mechanical aspects section B
- C04B35/628—Coating the powders or the macroscopic reinforcing agents
- C04B35/62844—Coating fibres
- C04B35/62857—Coating fibres with non-oxide ceramics
- C04B35/62865—Nitrides
- C04B35/62868—Boron nitride
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B35/00—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
- C04B35/515—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on non-oxide ceramics
- C04B35/56—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on non-oxide ceramics based on carbides or oxycarbides
- C04B35/565—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on non-oxide ceramics based on carbides or oxycarbides based on silicon carbide
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B35/00—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
- C04B35/622—Forming processes; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
- C04B35/626—Preparing or treating the powders individually or as batches ; preparing or treating macroscopic reinforcing agents for ceramic products, e.g. fibres; mechanical aspects section B
- C04B35/628—Coating the powders or the macroscopic reinforcing agents
- C04B35/62897—Coatings characterised by their thickness
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B35/00—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
- C04B35/71—Ceramic products containing macroscopic reinforcing agents
- C04B35/78—Ceramic products containing macroscopic reinforcing agents containing non-metallic materials
- C04B35/80—Fibres, filaments, whiskers, platelets, or the like
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
- C04B41/009—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone characterised by the material treated
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
- C04B41/45—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements
- C04B41/4584—Coating or impregnating of particulate or fibrous ceramic material
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
- C04B41/45—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements
- C04B41/50—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements with inorganic materials
- C04B41/5053—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements with inorganic materials non-oxide ceramics
- C04B41/5062—Borides, Nitrides or Silicides
- C04B41/5064—Boron nitride
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
- C04B2235/30—Constituents and secondary phases not being of a fibrous nature
- C04B2235/48—Organic compounds becoming part of a ceramic after heat treatment, e.g. carbonising phenol resins
- C04B2235/486—Boron containing organic compounds, e.g. borazine, borane or boranyl
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
- C04B2235/50—Constituents or additives of the starting mixture chosen for their shape or used because of their shape or their physical appearance
- C04B2235/52—Constituents or additives characterised by their shapes
- C04B2235/5208—Fibers
- C04B2235/5216—Inorganic
- C04B2235/524—Non-oxidic, e.g. borides, carbides, silicides or nitrides
- C04B2235/5244—Silicon carbide
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
- C04B2235/50—Constituents or additives of the starting mixture chosen for their shape or used because of their shape or their physical appearance
- C04B2235/52—Constituents or additives characterised by their shapes
- C04B2235/5208—Fibers
- C04B2235/5216—Inorganic
- C04B2235/524—Non-oxidic, e.g. borides, carbides, silicides or nitrides
- C04B2235/5248—Carbon, e.g. graphite
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/60—Aspects relating to the preparation, properties or mechanical treatment of green bodies or pre-forms
- C04B2235/614—Gas infiltration of green bodies or pre-forms
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/60—Aspects relating to the preparation, properties or mechanical treatment of green bodies or pre-forms
- C04B2235/616—Liquid infiltration of green bodies or pre-forms
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/65—Aspects relating to heat treatments of ceramic bodies such as green ceramics or pre-sintered ceramics, e.g. burning, sintering or melting processes
- C04B2235/656—Aspects relating to heat treatments of ceramic bodies such as green ceramics or pre-sintered ceramics, e.g. burning, sintering or melting processes characterised by specific heating conditions during heat treatment
- C04B2235/6562—Heating rate
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
- Y10T428/00—Stock material or miscellaneous articles
- Y10T428/249921—Web or sheet containing structurally defined element or component
- Y10T428/249924—Noninterengaged fiber-containing paper-free web or sheet which is not of specified porosity
- Y10T428/249928—Fiber embedded in a ceramic, glass, or carbon matrix
- Y10T428/249931—Free metal or alloy fiber
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Ceramic Engineering (AREA)
- Materials Engineering (AREA)
- Structural Engineering (AREA)
- Organic Chemistry (AREA)
- Manufacturing & Machinery (AREA)
- Inorganic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Chemical Or Physical Treatment Of Fibers (AREA)
- Ceramic Products (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| FR96/16104 | 1996-12-27 | ||
| FR9616104A FR2757848B1 (fr) | 1996-12-27 | 1996-12-27 | Preformes fibreuses gainees d'un revetement bn original, composites les incorporant et leurs preparations |
| PCT/FR1997/002423 WO1998029355A1 (fr) | 1996-12-27 | 1997-12-24 | Preformes fibreuses gainees d'un revetement en nitrure de bore, composites les incorporant et leurs preparations |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| JP2001507328A JP2001507328A (ja) | 2001-06-05 |
| JP2001507328A5 JP2001507328A5 (enExample) | 2005-04-07 |
| JP3987123B2 true JP3987123B2 (ja) | 2007-10-03 |
Family
ID=9499212
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP52969698A Expired - Lifetime JP3987123B2 (ja) | 1996-12-27 | 1997-12-24 | 窒化ホウ素コーティングで被覆された布帛予備成形体、それを組み込んだ複合材料およびその製造方法 |
Country Status (8)
| Country | Link |
|---|---|
| US (1) | US6284358B1 (enExample) |
| EP (1) | EP0952969B1 (enExample) |
| JP (1) | JP3987123B2 (enExample) |
| CA (1) | CA2279500C (enExample) |
| DE (1) | DE69724147T2 (enExample) |
| ES (1) | ES2205277T3 (enExample) |
| FR (1) | FR2757848B1 (enExample) |
| WO (1) | WO1998029355A1 (enExample) |
Families Citing this family (23)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US7150911B2 (en) * | 2001-02-08 | 2006-12-19 | Showa Denko Kabushiki Kaisha | Electrical insulating vapor grown carbon fiber and method for producing the same, and use thereof |
| JP3778045B2 (ja) * | 2001-10-09 | 2006-05-24 | 三菱電機株式会社 | 低誘電率材料の製造方法および低誘電率材料、並びにこの低誘電率材料を用いた絶縁膜および半導体装置 |
| JP4441617B2 (ja) * | 2004-08-09 | 2010-03-31 | 独立行政法人物質・材料研究機構 | 窒化アルミニウムナノチューブ及びその製造方法 |
| US7867554B2 (en) * | 2005-01-06 | 2011-01-11 | United Technologies Corporation | Boron nitride coated fibers and composite articles containing same |
| FR2882356B1 (fr) * | 2005-02-23 | 2008-08-15 | Snecma Propulsion Solide Sa | Procede de fabrication de piece en materiau composite a matrice ceramique et piece ainsi obtenue |
| JP4670100B2 (ja) * | 2006-03-01 | 2011-04-13 | 独立行政法人物質・材料研究機構 | 窒化ホウ素ナノチューブの精製方法 |
| JP4915930B2 (ja) * | 2007-03-27 | 2012-04-11 | 独立行政法人産業技術総合研究所 | ボラジン・ジアミン系ポリマー薄膜形成用組成物及びボラジン・ジアミン系ポリマー薄膜の製造方法 |
| JP4915929B2 (ja) * | 2007-03-27 | 2012-04-11 | 独立行政法人産業技術総合研究所 | ボラジン・ジアミン系重合体及びそのための重合性組成物、並びにその製造方法 |
| US20100192535A1 (en) * | 2009-02-04 | 2010-08-05 | Smith Michael W | Boron nitride nanotube fibrils and yarns |
| FR3008968B1 (fr) | 2013-07-23 | 2016-12-09 | Herakles | Procede de fabrication de pieces en materiau composite par impregnation a basse temperature de fusion |
| FR3037973B1 (fr) * | 2015-06-24 | 2019-09-06 | Safran Ceramics | Procede de traitement de fibres de carbure de silicium |
| FR3063725B1 (fr) | 2017-03-07 | 2019-04-12 | Safran Ceramics | Procede de realisation d'une preforme fibreuse consolidee |
| CN107353025B (zh) * | 2017-06-27 | 2020-10-20 | 中航复合材料有限责任公司 | 一种耐1200℃抗氧化的陶瓷基复合材料的制备方法 |
| WO2020025878A1 (fr) | 2018-08-03 | 2020-02-06 | Safran Ceramics | Procede de fabrication d'une piece en cmc |
| FR3120811B1 (fr) | 2021-03-18 | 2023-03-17 | Safran Ceram | Procédé amélioré de réalisation d'une préforme fibreuse consolidée |
| FR3124507B1 (fr) * | 2021-06-23 | 2023-10-27 | Safran Ceram | Procédé de revêtement d’au moins une fibre par une interphase de nitrure de bore |
| FR3130273B1 (fr) | 2021-12-10 | 2023-12-15 | Safran Ceram | Procédé de fabrication d’une pièce en matériau composite SiC/SiC |
| CN114804907A (zh) * | 2022-05-27 | 2022-07-29 | 陕西美兰德炭素有限责任公司 | 一种制备氮化硼改性的炭/炭复合材料制品的方法及制品 |
| FR3147805A1 (fr) | 2023-04-12 | 2024-10-18 | Safran Ceramics | Consolidation d’une préforme fibreuse |
| FR3147804A1 (fr) | 2023-04-12 | 2024-10-18 | Safran Ceramics | Consolidation d’une préforme fibreuse |
| CN117586034B (zh) * | 2023-11-08 | 2025-08-15 | 航天特种材料及工艺技术研究所 | 一种宽温域可重复使用高导热复合材料及其制备方法 |
| CN117645499B (zh) * | 2023-11-29 | 2025-08-08 | 西安理工大学 | 一种具有多层结构的bn纤维基多孔陶瓷的制备方法 |
| FR3157384A1 (fr) | 2023-12-21 | 2025-06-27 | Safran Ceramics | Procédé de fabrication d'une aube par infiltration chimique en phase vapeur |
Family Cites Families (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS6147735A (ja) * | 1984-08-11 | 1986-03-08 | Isoji Taniguchi | 有機窒化ホウ素重合体の製造法 |
| FR2640258B1 (fr) * | 1988-05-10 | 1991-06-07 | Europ Propulsion | Procede de fabrication de materiaux composites a renfort en fibres de carbure de silicium et a matrice ceramique |
| US5204295A (en) * | 1989-02-17 | 1993-04-20 | University Of New Mexico | Precursors for boron nitride coatings |
| US5502142A (en) * | 1990-03-09 | 1996-03-26 | The Trustees Of The University Of Pennsylvania | Direct thermal synthesis and ceramic applications of poly(borazylenes) |
| FR2659321B1 (fr) * | 1990-03-12 | 1992-05-22 | Rhone Poulenc Chimie | Procede de revetements en ceramique de pieces a base de carbone. |
-
1996
- 1996-12-27 FR FR9616104A patent/FR2757848B1/fr not_active Expired - Fee Related
-
1997
- 1997-12-24 DE DE69724147T patent/DE69724147T2/de not_active Expired - Fee Related
- 1997-12-24 US US09/331,726 patent/US6284358B1/en not_active Expired - Fee Related
- 1997-12-24 EP EP97953947A patent/EP0952969B1/fr not_active Expired - Lifetime
- 1997-12-24 ES ES97953947T patent/ES2205277T3/es not_active Expired - Lifetime
- 1997-12-24 JP JP52969698A patent/JP3987123B2/ja not_active Expired - Lifetime
- 1997-12-24 WO PCT/FR1997/002423 patent/WO1998029355A1/fr not_active Ceased
- 1997-12-24 CA CA002279500A patent/CA2279500C/en not_active Expired - Fee Related
Also Published As
| Publication number | Publication date |
|---|---|
| CA2279500A1 (fr) | 1998-07-09 |
| DE69724147T2 (de) | 2004-06-03 |
| DE69724147D1 (de) | 2003-09-18 |
| ES2205277T3 (es) | 2004-05-01 |
| FR2757848B1 (fr) | 1999-03-26 |
| US6284358B1 (en) | 2001-09-04 |
| WO1998029355A1 (fr) | 1998-07-09 |
| FR2757848A1 (fr) | 1998-07-03 |
| EP0952969B1 (fr) | 2003-08-13 |
| JP2001507328A (ja) | 2001-06-05 |
| EP0952969A1 (fr) | 1999-11-03 |
| CA2279500C (en) | 2006-04-04 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| JP3987123B2 (ja) | 窒化ホウ素コーティングで被覆された布帛予備成形体、それを組み込んだ複合材料およびその製造方法 | |
| CN100572327C (zh) | 带有陶瓷基体的复合材料部件的制造方法和所得部件 | |
| US5459114A (en) | Method for producing ceramic products | |
| Chawla | Ceramic matrix composites | |
| US5067999A (en) | Method for providing a silicon carbide matrix in carbon-fiber reinforced composites | |
| JP2000169249A (ja) | セラミック複合材料 | |
| EP0891956B2 (en) | Silicon-silicon carbide material and silicon carbide fiber-reinforced silicon-silicon carbide composite material | |
| CA2960342A1 (en) | Ceramic matrix composites having monomodal pore size distribution and low fiber volume fraction | |
| JP2007535461A (ja) | 炭素繊維強化のセラミックの複合体の製造方法 | |
| Suttor et al. | Fiber‐reinforced ceramic‐matrix composites with a polysiloxane/boron‐derived matrix | |
| JP2011190169A (ja) | 炭素繊維複合材、及びこの炭素繊維複合材を用いたブレーキ用部材、半導体用構造部材、耐熱性パネル、ヒートシンク | |
| US20130029127A1 (en) | Inorganic fiber for fiber bundles, process for producing the same, inorganic fiber bundle for composite material comprising the inorganic fiber for fiber bundles, and ceramic-based composite material reinforced with the fiber bundle | |
| EP1594627A2 (en) | Ceramic forming polymer derived ceramic composite and methods | |
| JPH03285877A (ja) | 繊維強化セラミックス複合材料及び強化用繊維 | |
| JPH07197264A (ja) | 繊維の表面処理方法、強化繊維及び応用 | |
| CN112266258B (zh) | 一种碳陶材料及其制备方法和应用 | |
| JPH0292886A (ja) | 耐酸化性を有する炭素繊維強化複合材料の製造法 | |
| Kajii et al. | A new type of fiber-bonded-ceramic material synthesized from pre-oxidized Si-Ti-CO fiber | |
| CN117447217B (zh) | 一种可室温浸渍C/SiAlC陶瓷基复合材料及其制备方法 | |
| JPH107472A (ja) | 繊維強化セラミックスの製造方法 | |
| JP2000160474A (ja) | 被覆セラミック繊維 | |
| JP3461424B2 (ja) | 耐酸化性c/c複合材の製造方法 | |
| JPH11130553A (ja) | 炭素/炭素複合材料 | |
| JP3154360B2 (ja) | 無機繊維強化セラミック複合材料 | |
| JPH1045480A (ja) | 繊維強化複合材用無機質繊維を被覆するためのコーティング並びにこれを含む無機質繊維及び繊維強化複合材 |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| A521 | Request for written amendment filed |
Free format text: JAPANESE INTERMEDIATE CODE: A523 Effective date: 20040707 |
|
| A621 | Written request for application examination |
Free format text: JAPANESE INTERMEDIATE CODE: A621 Effective date: 20040707 |
|
| A131 | Notification of reasons for refusal |
Free format text: JAPANESE INTERMEDIATE CODE: A131 Effective date: 20070123 |
|
| A521 | Request for written amendment filed |
Free format text: JAPANESE INTERMEDIATE CODE: A523 Effective date: 20070417 |
|
| TRDD | Decision of grant or rejection written | ||
| A01 | Written decision to grant a patent or to grant a registration (utility model) |
Free format text: JAPANESE INTERMEDIATE CODE: A01 Effective date: 20070612 |
|
| A61 | First payment of annual fees (during grant procedure) |
Free format text: JAPANESE INTERMEDIATE CODE: A61 Effective date: 20070712 |
|
| R150 | Certificate of patent or registration of utility model |
Free format text: JAPANESE INTERMEDIATE CODE: R150 |
|
| FPAY | Renewal fee payment (event date is renewal date of database) |
Free format text: PAYMENT UNTIL: 20100720 Year of fee payment: 3 |