DE60334637D1 - Verfahren zur quantitativen herstellung von ammoniak aus harnstoff - Google Patents
Verfahren zur quantitativen herstellung von ammoniak aus harnstoffInfo
- Publication number
- DE60334637D1 DE60334637D1 DE60334637T DE60334637T DE60334637D1 DE 60334637 D1 DE60334637 D1 DE 60334637D1 DE 60334637 T DE60334637 T DE 60334637T DE 60334637 T DE60334637 T DE 60334637T DE 60334637 D1 DE60334637 D1 DE 60334637D1
- Authority
- DE
- Germany
- Prior art keywords
- urea
- ammonia
- quantitative preparation
- quantitative
- preparation
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01C—AMMONIA; CYANOGEN; COMPOUNDS THEREOF
- C01C1/00—Ammonia; Compounds thereof
- C01C1/02—Preparation, purification or separation of ammonia
- C01C1/08—Preparation of ammonia from nitrogenous organic substances
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P20/00—Technologies relating to chemical industry
- Y02P20/50—Improvements relating to the production of bulk chemicals
- Y02P20/52—Improvements relating to the production of bulk chemicals using catalysts, e.g. selective catalysts
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Analytical Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Catalysts (AREA)
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US10/302,531 US6887449B2 (en) | 2002-11-21 | 2002-11-21 | Method of quantitatively producing ammonia from urea |
PCT/US2003/035640 WO2004048268A1 (en) | 2002-11-21 | 2003-11-07 | Method of quantitatively producing ammonia from urea |
Publications (1)
Publication Number | Publication Date |
---|---|
DE60334637D1 true DE60334637D1 (de) | 2010-12-02 |
Family
ID=32324809
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
DE60334637T Expired - Lifetime DE60334637D1 (de) | 2002-11-21 | 2003-11-07 | Verfahren zur quantitativen herstellung von ammoniak aus harnstoff |
Country Status (10)
Country | Link |
---|---|
US (1) | US6887449B2 (de) |
EP (1) | EP1562858B1 (de) |
JP (1) | JP2006507209A (de) |
CN (1) | CN1319858C (de) |
AR (1) | AR042121A1 (de) |
AU (1) | AU2003285166A1 (de) |
CA (1) | CA2502379C (de) |
DE (1) | DE60334637D1 (de) |
TW (1) | TWI338673B (de) |
WO (1) | WO2004048268A1 (de) |
Families Citing this family (19)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US20030211024A1 (en) * | 2002-05-10 | 2003-11-13 | Wojichowski David Lee | Methods of converting urea to ammonia for SCR, SNCR and flue gas conditioning |
US7682586B2 (en) * | 2006-08-22 | 2010-03-23 | Babcock Power Environmental, Inc. | Thermal decomposition of urea in a side stream of combustion flue gas using a regenerative heat exchanger |
US20080267837A1 (en) * | 2007-04-27 | 2008-10-30 | Phelps Calvin E | Conversion of urea to reactants for NOx reduction |
US20090148370A1 (en) * | 2007-12-06 | 2009-06-11 | Spencer Iii Herbert W | Process to produce ammonia from urea |
US9266709B2 (en) * | 2009-11-20 | 2016-02-23 | Jack R. BRAMMELL | Systems and methods for on-site mixing and dispensing of a reducing agent solution for use with a diesel catalytic converter |
AU2013213700B2 (en) * | 2012-08-31 | 2017-08-17 | China Petroleum & Chemical Corporation | Apparatus for producing aqueous urea solution used in vehicles and method of using the same |
ITMI20130679A1 (it) * | 2013-04-24 | 2014-10-25 | Termokimik Corp Impianti E P Rocedimenti In | Fast feeder - gruppo e metodo per la generazione e l'immissione di una miscela gassosa controllata di ammoniaca in un flusso di fumi di combustione |
ITMI20130680A1 (it) * | 2013-04-24 | 2014-10-25 | Termokimik Corp Impianti E P Rocedimenti In | Fast aig - gruppo e relativo impianto per l'iniezione di una miscela gassosa di ammoniaca o urea in un flusso di fumi di combustione |
CN103395801B (zh) * | 2013-08-08 | 2016-03-09 | 大唐环境产业集团股份有限公司 | 一种尿素催化水解的方法及装置 |
FR3015454B1 (fr) * | 2013-12-20 | 2016-01-01 | Aaqius & Aaqius Sa | Dispositif et procede de rechargement de cartouche d'ammoniac pour reduction des oxydes d'azote par reduction catalytique selective dans un vehicule |
US9586831B2 (en) * | 2014-06-09 | 2017-03-07 | Wahlco, Inc. | Urea to ammonia process |
US10330654B2 (en) * | 2014-07-20 | 2019-06-25 | Sabic Global Technologies B.V. | Methods for determining low sulfate concentrations in synthetic urea samples, produced in a manufacturing process and containing high levels of impurities |
CN104876242B (zh) * | 2015-05-11 | 2017-03-22 | 北京新叶能源科技有限公司 | 一种三相流态化尿素催化水解制氨设备及方法 |
KR102113792B1 (ko) * | 2015-05-27 | 2020-05-22 | 현대중공업파워시스템 주식회사 | 복합 화력발전 시스템 |
TW202306432A (zh) * | 2016-04-26 | 2023-02-01 | 丹麥商托普索公司 | 用於氨合成轉換器之起動加熱的方法 |
WO2018128902A1 (en) * | 2017-01-05 | 2018-07-12 | Fuel Tech, Inc. | Controlled, compact, on-demand ammonia gas generation process and apparatus |
CN110775986B (zh) * | 2019-11-20 | 2024-05-28 | 南通市新叶能源科技有限公司 | 一种尿素催化水解制氨设备及其制备方法 |
CN111408389A (zh) * | 2020-04-22 | 2020-07-14 | 江苏中立环保科技有限公司 | 用于尿素催化水解反应的复合催化剂 |
CN115057454B (zh) * | 2022-06-28 | 2023-06-23 | 江苏国瑞特环保工程技术有限公司 | 一种强碱性环境改良型尿素水解制氨系统 |
Family Cites Families (74)
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DE154442C (de) | ||||
GB896660A (en) | 1959-07-13 | 1962-05-16 | Thorn Electrical Ind Ltd | Improvements in the preparation of phosphates of bivalent metals |
IL23001A (en) | 1964-02-17 | 1968-09-26 | Allied Chem | Method for decomposing ammonium carbamates |
US3826815A (en) * | 1972-06-21 | 1974-07-30 | I Mavrovic | Recovery of residual ammonia from weak aqueous solutions thereof |
US3922222A (en) | 1973-02-20 | 1975-11-25 | Cf Ind | Method for treatment of urea crystallizer condensate |
US3900544A (en) * | 1973-11-28 | 1975-08-19 | Arco Polymers Inc | Method for the continuous extrusion of multiple small cross-section thermoplastic polymeric resinous foam profiles |
US4220632A (en) * | 1974-09-10 | 1980-09-02 | The United States Of America As Represented By The United States Department Of Energy | Reduction of nitrogen oxides with catalytic acid resistant aluminosilicate molecular sieves and ammonia |
US4208386A (en) * | 1976-03-03 | 1980-06-17 | Electric Power Research Institute, Inc. | Urea reduction of NOx in combustion effluents |
IT1068268B (it) * | 1976-09-09 | 1985-03-21 | Snam Progetti | Procedimento per la produzione di urea e purificazione delle acque |
US4341640A (en) * | 1976-09-27 | 1982-07-27 | Standard Oil Company | Urea hydrolysis |
JPS5352274A (en) | 1976-10-25 | 1978-05-12 | Mitsui Toatsu Chem Inc | Treating method for aqueous solution containing urea, ammonia and carbondioxide |
AT351135B (de) * | 1977-06-08 | 1979-07-10 | Oemv Ag | Verfahren und vorrichtung zur reinigung von harnstoffloesungen |
US4087513A (en) * | 1977-08-12 | 1978-05-02 | Olin Corporation | Method of hydrolyzing urea contained in waste water streams |
US4325924A (en) * | 1977-10-25 | 1982-04-20 | Electric Power Research Institute, Inc. | Urea reduction of NOx in fuel rich combustion effluents |
US4168299A (en) * | 1978-03-20 | 1979-09-18 | Olin Corporation | Catalytic method for hydrolyzing urea |
US4220635A (en) * | 1978-03-20 | 1980-09-02 | Olin Corporation | Catalytic method for hydrolyzing urea |
NL7903623A (nl) * | 1979-05-09 | 1980-11-11 | Stamicarbon | Werkwijze voor het zuiveren van ureumhoudend afvalwater en werkwijze voor het bereiden van melamine. |
NL8006477A (nl) * | 1980-11-28 | 1982-06-16 | Unie Van Kunstmestfab Bv | Werkwijze voor het verwijderen van ureum, ammoniak en kooldioxide uit verdunde waterige oplossing. |
NL8100989A (nl) * | 1981-02-28 | 1982-09-16 | Unie Van Kunstmestfab Bv | Werkwijze voor het verwijderen van ureum, ammoniak en kooldioxide uit verdunde waterige oplossingen. |
NL8102391A (nl) * | 1981-05-15 | 1982-12-01 | Unie Van Kunstmestfab Bv | Werkwijze voor het winnen van waardevolle bestanddelen uit de afvalstromen verkregen bij de ureumbereiding. |
JPS57188560A (en) | 1981-05-18 | 1982-11-19 | Toyo Eng Corp | Method and apparatus for preparation of urea |
NL8105027A (nl) | 1981-11-06 | 1983-06-01 | Stamicarbon | Werkwijze voor het omzetten in ammoniak en kooldioxide van gasvormige verbindingen die stikstof- en koolstofatomen bevatten. |
JPS5982987A (ja) | 1982-11-05 | 1984-05-14 | Toyo Eng Corp | 尿素を含有する希水溶液の処理方法 |
US4533364A (en) * | 1983-02-01 | 1985-08-06 | Electric Power Research Institute, Inc. | Method for flue gas conditioning with the decomposition products of ammonium sulfate or ammonium bisulfate |
DE3422175A1 (de) | 1984-06-04 | 1985-12-19 | Julius Dr. 8000 München Kern | Verfahren zur beimischung von ammoniak zu saure schadstoffe enthaltenden abgasen oder luft |
US4552979A (en) * | 1984-08-27 | 1985-11-12 | James Chemical Engineering Inc. | Process for treatment of urea plant process condensate |
US4731233A (en) * | 1986-01-09 | 1988-03-15 | Thompson Richard E | Method and composition for utilizing lime-urea hydrates to simultaneously reduce NOx and SOx in combustion effluents |
JPS63198713A (ja) | 1987-02-13 | 1988-08-17 | Hino Motors Ltd | デイ−ゼルエンジンの窒素酸化物除去方法 |
JPH0691987B2 (ja) | 1987-03-13 | 1994-11-16 | 東洋エンジニアリング株式会社 | 尿素の加水分解方法 |
WO1989007004A1 (en) | 1988-02-02 | 1989-08-10 | Dale Gordon Jones | Process and apparatus using two-stage boiler injection for reduction of oxides of nitrogen |
AT390208B (de) | 1988-05-09 | 1990-04-10 | Waagner Biro Ag | Verfahren zur entfernung von stickoxiden |
JPH02191528A (ja) | 1989-01-20 | 1990-07-27 | Babcock Hitachi Kk | 固体還元剤を用いた脱硝装置 |
JPH02268811A (ja) | 1989-04-10 | 1990-11-02 | Hitachi Zosen Corp | 尿素の加水分解によるアンモニアを用いる脱硝方法 |
US5034030A (en) * | 1989-07-03 | 1991-07-23 | The University Of North Dakota School Of Engineering & Mines Foundation (Und-Sem Foundation) | Process of flue gas conditioning applied to fabric filtration |
US5262138A (en) * | 1989-08-31 | 1993-11-16 | Union Oil Company Of California | Process for NOx abatement |
IT1232670B (it) * | 1989-09-15 | 1992-03-02 | Snam Progetti | Procedimento per la purificazione delle acque reflue prodotte dagli impianti di produzione dell'urea. |
US5058514A (en) * | 1989-10-18 | 1991-10-22 | Mozes Miriam S | Process for controlling acid gas emissions in power plant flue gases |
US5240688A (en) | 1990-08-01 | 1993-08-31 | Fuel Tech Gmbh | Process for the in-line hydrolysis of urea |
US5543123A (en) * | 1990-08-01 | 1996-08-06 | Nalco Fuel Tech | Low pressure formation of a urea hydrolysate for nitrogen oxides reduction |
US5098680A (en) * | 1990-10-15 | 1992-03-24 | Exxon Research & Engineering Company | Aqueous ammonia injection scheme |
DE4038054A1 (de) | 1990-11-29 | 1992-06-04 | Man Technologie Gmbh | Verfahren und vorrichtung zur selektiven katalytischen no(pfeil abwaerts)x(pfeil abwaerts)-reduktion in sauerstoffhaltigen abgasen |
US5281403B1 (en) * | 1991-09-27 | 1996-06-11 | Noell Inc | Method for converting urea to ammonia |
RU2056408C1 (ru) * | 1991-10-23 | 1996-03-20 | Уриа Казале С.А. | Способ гидролиза мочевины, содержащейся в отработанной воде с установок синтеза мочевины, и колонный аппарат для его осуществления |
US5233238A (en) * | 1991-12-20 | 1993-08-03 | Vlsi Technology, Inc. | High power buffer with increased current stability |
US5252308A (en) * | 1991-12-31 | 1993-10-12 | Union Oil Company Of California | Transporting urea for quantitative conversion into ammonia |
US5223238A (en) | 1992-01-16 | 1993-06-29 | The M. W. Kellogg Company | Method for treating ammonia and urea condensates |
EP0582022A1 (de) | 1992-08-03 | 1994-02-09 | Paul Scherrer Institut | Verfahren zum Herstellen von gasförmigem Ammoniak aus Harnstoff |
US5567226A (en) * | 1992-10-09 | 1996-10-22 | Lookman; Aziz A. | Apparatus and method for enhancing the performance of a particulate collection device |
WO1994013391A1 (en) | 1992-12-08 | 1994-06-23 | Nalco Fuel Tech | Process for improving the performance of an electrostatic precipitator |
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NO950854L (no) | 1995-03-03 | 1996-09-04 | Norsk Hydro As | Selektiv katalytisk reduksjon av nitrogenoksider |
DE19510804A1 (de) | 1995-03-24 | 1996-09-26 | Dornier Gmbh | Verfahren und Vorrichtung zur Stickoxidminderung in Abgasen von Verbrennungsmaschinen |
DE19531028A1 (de) | 1995-08-23 | 1997-02-27 | Siemens Ag | Verfahren zur Abgasreinigung und Abgas-Reinigungseinrichtung für einen Verbrennungsmotor |
JP3368371B2 (ja) | 1996-05-07 | 2003-01-20 | 日立造船株式会社 | 排煙脱硝装置 |
US5985222A (en) * | 1996-11-01 | 1999-11-16 | Noxtech, Inc. | Apparatus and method for reducing NOx from exhaust gases produced by industrial processes |
DE19651212C3 (de) | 1996-12-10 | 2003-10-30 | Bosch Gmbh Robert | Verfahren und Vorrichtung zur Minderung von Stickoxiden in Gasgemischen |
US6077491A (en) | 1997-03-21 | 2000-06-20 | Ec&C Technologies | Methods for the production of ammonia from urea and/or biuret, and uses for NOx and/or particulate matter removal |
DE19719998C2 (de) * | 1997-05-13 | 2003-10-30 | Daimler Chrysler Ag | Verfahren und Vorrichtung zur Stickoxidreduktion im Abgas einer Verbrennungseinrichtung |
JPH11171535A (ja) | 1997-12-05 | 1999-06-29 | Mitsubishi Heavy Ind Ltd | アンモニア発生方法及び排ガス処理方法 |
US6120580A (en) * | 1998-04-15 | 2000-09-19 | Hera, Llc | Method for testing systems designed for NOx reduction in the combustion of carbonaceous fuels |
ITMI981155A1 (it) * | 1998-05-25 | 1999-11-25 | Siirtec Nigi S P A | Processo per la produzione di ammoniaca mediante idrolisi dell'urea |
DE19834980A1 (de) | 1998-08-03 | 1999-12-30 | Siemens Ag | Mikrowellen-Hydrolyse-Reaktor |
US6093380A (en) * | 1998-10-16 | 2000-07-25 | Siirtec Nigi, S.P.A. | Method and apparatus for pollution control in exhaust gas streams from fossil fuel burning facilities |
US6146605A (en) * | 1999-07-26 | 2000-11-14 | Hera, Llc | Combined SCR/SNCR process |
US6511644B1 (en) * | 2000-08-28 | 2003-01-28 | The Chemithon Corporation | Method for removing contaminants in reactors |
US6436359B1 (en) * | 2000-10-25 | 2002-08-20 | Ec&C Technologies, Inc. | Method for controlling the production of ammonia from urea for NOx scrubbing |
US6761868B2 (en) * | 2001-05-16 | 2004-07-13 | The Chemithon Corporation | Process for quantitatively converting urea to ammonia on demand |
-
2002
- 2002-11-21 US US10/302,531 patent/US6887449B2/en not_active Expired - Lifetime
-
2003
- 2003-11-07 EP EP03779490A patent/EP1562858B1/de not_active Expired - Lifetime
- 2003-11-07 CA CA002502379A patent/CA2502379C/en not_active Expired - Fee Related
- 2003-11-07 JP JP2004555395A patent/JP2006507209A/ja active Pending
- 2003-11-07 DE DE60334637T patent/DE60334637D1/de not_active Expired - Lifetime
- 2003-11-07 AU AU2003285166A patent/AU2003285166A1/en not_active Abandoned
- 2003-11-07 CN CNB2003801022794A patent/CN1319858C/zh not_active Expired - Lifetime
- 2003-11-07 WO PCT/US2003/035640 patent/WO2004048268A1/en active Application Filing
- 2003-11-18 TW TW092132291A patent/TWI338673B/zh not_active IP Right Cessation
- 2003-11-21 AR ARP030104315A patent/AR042121A1/es not_active Application Discontinuation
Also Published As
Publication number | Publication date |
---|---|
CN1708456A (zh) | 2005-12-14 |
WO2004048268A1 (en) | 2004-06-10 |
CA2502379A1 (en) | 2004-06-10 |
TW200417515A (en) | 2004-09-16 |
AR042121A1 (es) | 2005-06-08 |
US6887449B2 (en) | 2005-05-03 |
AU2003285166A1 (en) | 2004-06-18 |
CA2502379C (en) | 2009-06-02 |
JP2006507209A (ja) | 2006-03-02 |
CN1319858C (zh) | 2007-06-06 |
US20040101464A1 (en) | 2004-05-27 |
EP1562858B1 (de) | 2010-10-20 |
TWI338673B (en) | 2011-03-11 |
EP1562858A1 (de) | 2005-08-17 |
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