DE602004003071D1 - Verfahren zur herstellung von ammoniak aus wasser und stickstoff am einsatzort - Google Patents

Verfahren zur herstellung von ammoniak aus wasser und stickstoff am einsatzort

Info

Publication number
DE602004003071D1
DE602004003071D1 DE602004003071T DE602004003071T DE602004003071D1 DE 602004003071 D1 DE602004003071 D1 DE 602004003071D1 DE 602004003071 T DE602004003071 T DE 602004003071T DE 602004003071 T DE602004003071 T DE 602004003071T DE 602004003071 D1 DE602004003071 D1 DE 602004003071D1
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DE
Germany
Prior art keywords
ammonia
nitrogen
production
water
field
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
DE602004003071T
Other languages
English (en)
Other versions
DE602004003071T2 (de
Inventor
J Spiegelman
Daniel Alvarez
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Entegris Inc
Original Assignee
Entegris Inc
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Entegris Inc filed Critical Entegris Inc
Publication of DE602004003071D1 publication Critical patent/DE602004003071D1/de
Application granted granted Critical
Publication of DE602004003071T2 publication Critical patent/DE602004003071T2/de
Anticipated expiration legal-status Critical
Expired - Fee Related legal-status Critical Current

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B3/00Hydrogen; Gaseous mixtures containing hydrogen; Separation of hydrogen from mixtures containing it; Purification of hydrogen
    • C01B3/02Production of hydrogen or of gaseous mixtures containing a substantial proportion of hydrogen
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B21/00Nitrogen; Compounds thereof
    • C01B21/04Purification or separation of nitrogen
    • C01B21/0405Purification or separation processes
    • C01B21/0433Physical processing only
    • C01B21/045Physical processing only by adsorption in solids
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B3/00Hydrogen; Gaseous mixtures containing hydrogen; Separation of hydrogen from mixtures containing it; Purification of hydrogen
    • C01B3/02Production of hydrogen or of gaseous mixtures containing a substantial proportion of hydrogen
    • C01B3/025Preparation or purification of gas mixtures for ammonia synthesis
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B3/00Hydrogen; Gaseous mixtures containing hydrogen; Separation of hydrogen from mixtures containing it; Purification of hydrogen
    • C01B3/02Production of hydrogen or of gaseous mixtures containing a substantial proportion of hydrogen
    • C01B3/04Production of hydrogen or of gaseous mixtures containing a substantial proportion of hydrogen by decomposition of inorganic compounds, e.g. ammonia
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B3/00Hydrogen; Gaseous mixtures containing hydrogen; Separation of hydrogen from mixtures containing it; Purification of hydrogen
    • C01B3/50Separation of hydrogen or hydrogen containing gases from gaseous mixtures, e.g. purification
    • C01B3/56Separation of hydrogen or hydrogen containing gases from gaseous mixtures, e.g. purification by contacting with solids; Regeneration of used solids
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01CAMMONIA; CYANOGEN; COMPOUNDS THEREOF
    • C01C1/00Ammonia; Compounds thereof
    • C01C1/02Preparation, purification or separation of ammonia
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01CAMMONIA; CYANOGEN; COMPOUNDS THEREOF
    • C01C1/00Ammonia; Compounds thereof
    • C01C1/02Preparation, purification or separation of ammonia
    • C01C1/024Purification
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01CAMMONIA; CYANOGEN; COMPOUNDS THEREOF
    • C01C1/00Ammonia; Compounds thereof
    • C01C1/02Preparation, purification or separation of ammonia
    • C01C1/04Preparation of ammonia by synthesis in the gas phase
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01CAMMONIA; CYANOGEN; COMPOUNDS THEREOF
    • C01C1/00Ammonia; Compounds thereof
    • C01C1/02Preparation, purification or separation of ammonia
    • C01C1/04Preparation of ammonia by synthesis in the gas phase
    • C01C1/0405Preparation of ammonia by synthesis in the gas phase from N2 and H2 in presence of a catalyst
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B2203/00Integrated processes for the production of hydrogen or synthesis gas
    • C01B2203/04Integrated processes for the production of hydrogen or synthesis gas containing a purification step for the hydrogen or the synthesis gas
    • C01B2203/042Purification by adsorption on solids
    • C01B2203/043Regenerative adsorption process in two or more beds, one for adsorption, the other for regeneration
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B2203/00Integrated processes for the production of hydrogen or synthesis gas
    • C01B2203/04Integrated processes for the production of hydrogen or synthesis gas containing a purification step for the hydrogen or the synthesis gas
    • C01B2203/0465Composition of the impurity
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B2203/00Integrated processes for the production of hydrogen or synthesis gas
    • C01B2203/04Integrated processes for the production of hydrogen or synthesis gas containing a purification step for the hydrogen or the synthesis gas
    • C01B2203/0465Composition of the impurity
    • C01B2203/047Composition of the impurity the impurity being carbon monoxide
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B2203/00Integrated processes for the production of hydrogen or synthesis gas
    • C01B2203/04Integrated processes for the production of hydrogen or synthesis gas containing a purification step for the hydrogen or the synthesis gas
    • C01B2203/0465Composition of the impurity
    • C01B2203/0475Composition of the impurity the impurity being carbon dioxide
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B2203/00Integrated processes for the production of hydrogen or synthesis gas
    • C01B2203/04Integrated processes for the production of hydrogen or synthesis gas containing a purification step for the hydrogen or the synthesis gas
    • C01B2203/0465Composition of the impurity
    • C01B2203/048Composition of the impurity the impurity being an organic compound
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B2203/00Integrated processes for the production of hydrogen or synthesis gas
    • C01B2203/04Integrated processes for the production of hydrogen or synthesis gas containing a purification step for the hydrogen or the synthesis gas
    • C01B2203/0465Composition of the impurity
    • C01B2203/0495Composition of the impurity the impurity being water
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02EREDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
    • Y02E60/00Enabling technologies; Technologies with a potential or indirect contribution to GHG emissions mitigation
    • Y02E60/30Hydrogen technology
    • Y02E60/36Hydrogen production from non-carbon containing sources, e.g. by water electrolysis
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02PCLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00Technologies relating to chemical industry
    • Y02P20/50Improvements relating to the production of bulk chemicals
    • Y02P20/52Improvements relating to the production of bulk chemicals using catalysts, e.g. selective catalysts

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Analytical Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Combustion & Propulsion (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Health & Medical Sciences (AREA)
  • General Health & Medical Sciences (AREA)
  • Hydrogen, Water And Hydrids (AREA)
  • Physical Water Treatments (AREA)
  • Treatment Of Water By Oxidation Or Reduction (AREA)
DE602004003071T 2003-07-23 2004-07-22 Verfahren zur herstellung von ammoniak aus wasser und stickstoff am einsatzort Expired - Fee Related DE602004003071T2 (de)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
US10/626,266 US20050019244A1 (en) 2003-07-23 2003-07-23 Method for the point of use production of ammonia from water and nitrogen
US626266 2003-07-23
PCT/US2004/023594 WO2005009894A1 (en) 2003-07-23 2004-07-22 Method for the point of use production of ammonia from water and nitrogen

Publications (2)

Publication Number Publication Date
DE602004003071D1 true DE602004003071D1 (de) 2006-12-14
DE602004003071T2 DE602004003071T2 (de) 2007-05-31

Family

ID=34080395

Family Applications (1)

Application Number Title Priority Date Filing Date
DE602004003071T Expired - Fee Related DE602004003071T2 (de) 2003-07-23 2004-07-22 Verfahren zur herstellung von ammoniak aus wasser und stickstoff am einsatzort

Country Status (8)

Country Link
US (2) US20050019244A1 (de)
EP (1) EP1654192B1 (de)
JP (1) JP2006528128A (de)
KR (1) KR20060040713A (de)
CN (1) CN1852861A (de)
DE (1) DE602004003071T2 (de)
TW (1) TW200510249A (de)
WO (1) WO2005009894A1 (de)

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US7402292B2 (en) * 2005-09-19 2008-07-22 Delphi Technologies, Inc. Device and methods of ammonia generation for NOx abatement
CN1907855A (zh) * 2006-08-16 2007-02-07 武汉华灿光电有限公司 高纯氨的合成方法
US20080311022A1 (en) * 2007-06-14 2008-12-18 Battelle Energy Alliance, Llc Methods and apparatuses for ammonia production
JP4512151B2 (ja) * 2007-09-28 2010-07-28 トヨタ自動車株式会社 水素発生方法、水素発生材料の製造方法、水素製造装置、及び、燃料電池システム
US8272216B2 (en) * 2008-02-22 2012-09-25 Toyota Jidosha Kabushiki Kaisha Method for converting solar thermal energy
US20100003184A1 (en) * 2008-02-22 2010-01-07 Toyota Jidosha Kabushiki Kaisha Method for storing solar thermal energy
JP5012559B2 (ja) * 2008-02-22 2012-08-29 トヨタ自動車株式会社 太陽熱エネルギー貯蔵及び移送方法
JP5365037B2 (ja) * 2008-03-18 2013-12-11 トヨタ自動車株式会社 水素生成装置、アンモニア燃焼内燃機関、及び燃料電池
JP5373410B2 (ja) 2009-01-09 2013-12-18 トヨタ自動車株式会社 アンモニア合成方法
CN101575102B (zh) 2009-06-12 2012-09-05 武汉高安新材料有限公司 氨催化裂解、氢氮气纯化和氨合成三步集成制备高纯氨的方法
IL207178A0 (en) * 2010-07-25 2010-12-30 Meyer Fitoussi Hydrogen generating system and apparatuses thereof
TWI427035B (zh) 2011-08-02 2014-02-21 Univ Nat Pingtung Sci & Tech 氨製備裝置
US8992842B2 (en) * 2012-04-17 2015-03-31 Roger Gordon Systems and methods of making ammonia using hydrogen and nitrogen gases
KR101200561B1 (ko) * 2012-04-27 2012-11-13 주식회사 엑스에프씨 해수전해설비를 이용한 연료전지, 해수전해설비를 이용하여 가성소다, 암모니아, 요소, pvc의 제조방법 및 그 통합시스템
JP2014047089A (ja) * 2012-08-30 2014-03-17 Japan Pionics Co Ltd 精製アンモニアの供給装置
CN105264118B (zh) * 2013-03-26 2019-01-18 俄亥俄州立大学 在碱性介质中的氨的电化学合成
US20150203359A1 (en) * 2014-01-17 2015-07-23 Air Products And Chemicals, Inc. System and Process for Producing Ammonia Using an Ion Transport Membrane, Gasifier, and Ammonia Synthesis Unit
CN105692653A (zh) * 2014-11-28 2016-06-22 中国科学院大连化学物理研究所 制备氨的系统及方法
GB2544485B (en) * 2015-11-16 2018-09-19 Siemens Ag Electrochemical cell comprising a steam inlet and a solid oxide layer
GB2544486C (en) 2015-11-16 2018-07-25 Siemens Ag Synthesis of Ammonia
CN106480469A (zh) * 2016-07-14 2017-03-08 张国权 小型制氨机的制造方法
CN106185984B (zh) * 2016-07-23 2021-06-29 陈志强 基于水蒸汽电解法联合生产氨与硝酸的系统
JP2022526821A (ja) * 2019-04-08 2022-05-26 エムケイエス インストゥルメンツ, インコーポレイテッド 溶存キャリアガス及び酸素含有量が低減されたアンモニア溶液を生成するためのシステムおよび方法
KR102306626B1 (ko) * 2019-12-19 2021-09-30 한국에너지기술연구원 흡착부과 공정을 이용한 고순도 암모니아 생산 방법
CN111394740B (zh) * 2020-03-11 2021-07-27 南京航空航天大学 一种提高电催化氮还原合成氨反应效率的方法
WO2021226275A1 (en) * 2020-05-05 2021-11-11 Enviro Water Minerals Company, Inc. Sustainable desalination systems and methods
CA3227905A1 (en) * 2021-08-19 2023-02-23 Topsoe A/S Process for the preparation of green ammonia synthesis gas

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Also Published As

Publication number Publication date
US20050019244A1 (en) 2005-01-27
EP1654192B1 (de) 2006-11-02
US20060243585A1 (en) 2006-11-02
JP2006528128A (ja) 2006-12-14
CN1852861A (zh) 2006-10-25
DE602004003071T2 (de) 2007-05-31
KR20060040713A (ko) 2006-05-10
WO2005009894A1 (en) 2005-02-03
EP1654192A1 (de) 2006-05-10
TW200510249A (en) 2005-03-16

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