DE602005026166D1 - Verzweigtes und sulfoniertes mehrblockcopolymer und elektrolytmembran damit - Google Patents
Verzweigtes und sulfoniertes mehrblockcopolymer und elektrolytmembran damitInfo
- Publication number
- DE602005026166D1 DE602005026166D1 DE602005026166T DE602005026166T DE602005026166D1 DE 602005026166 D1 DE602005026166 D1 DE 602005026166D1 DE 602005026166 T DE602005026166 T DE 602005026166T DE 602005026166 T DE602005026166 T DE 602005026166T DE 602005026166 D1 DE602005026166 D1 DE 602005026166D1
- Authority
- DE
- Germany
- Prior art keywords
- branched
- electrolyte membrane
- block copolymer
- sulphonated
- multi block
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
Classifications
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G61/00—Macromolecular compounds obtained by reactions forming a carbon-to-carbon link in the main chain of the macromolecule
- C08G61/12—Macromolecular compounds containing atoms other than carbon in the main chain of the macromolecule
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G65/00—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule
- C08G65/002—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from unsaturated compounds
- C08G65/005—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from unsaturated compounds containing halogens
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G65/00—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule
- C08G65/34—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from hydroxy compounds or their metallic derivatives
- C08G65/38—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from hydroxy compounds or their metallic derivatives derived from phenols
- C08G65/40—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from hydroxy compounds or their metallic derivatives derived from phenols from phenols (I) and other compounds (II), e.g. OH-Ar-OH + X-Ar-X, where X is halogen atom, i.e. leaving group
- C08G65/4012—Other compound (II) containing a ketone group, e.g. X-Ar-C(=O)-Ar-X for polyetherketones
- C08G65/4056—(I) or (II) containing sulfur
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G65/00—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule
- C08G65/34—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from hydroxy compounds or their metallic derivatives
- C08G65/48—Polymers modified by chemical after-treatment
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G75/00—Macromolecular compounds obtained by reactions forming a linkage containing sulfur with or without nitrogen, oxygen, or carbon in the main chain of the macromolecule
- C08G75/20—Polysulfones
- C08G75/23—Polyethersulfones
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
- C08J5/00—Manufacture of articles or shaped materials containing macromolecular substances
- C08J5/20—Manufacture of shaped structures of ion-exchange resins
- C08J5/22—Films, membranes or diaphragms
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L71/00—Compositions of polyethers obtained by reactions forming an ether link in the main chain; Compositions of derivatives of such polymers
- C08L71/08—Polyethers derived from hydroxy compounds or from their metallic derivatives
- C08L71/10—Polyethers derived from hydroxy compounds or from their metallic derivatives from phenols
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L81/00—Compositions of macromolecular compounds obtained by reactions forming in the main chain of the macromolecule a linkage containing sulfur with or without nitrogen, oxygen or carbon only; Compositions of polysulfones; Compositions of derivatives of such polymers
- C08L81/06—Polysulfones; Polyethersulfones
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- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
- H01M8/00—Fuel cells; Manufacture thereof
- H01M8/10—Fuel cells with solid electrolytes
- H01M8/1016—Fuel cells with solid electrolytes characterised by the electrolyte material
- H01M8/1018—Polymeric electrolyte materials
- H01M8/102—Polymeric electrolyte materials characterised by the chemical structure of the main chain of the ion-conducting polymer
- H01M8/1025—Polymeric electrolyte materials characterised by the chemical structure of the main chain of the ion-conducting polymer having only carbon and oxygen, e.g. polyethers, sulfonated polyetheretherketones [S-PEEK], sulfonated polysaccharides, sulfonated celluloses or sulfonated polyesters
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- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
- H01M8/00—Fuel cells; Manufacture thereof
- H01M8/10—Fuel cells with solid electrolytes
- H01M8/1016—Fuel cells with solid electrolytes characterised by the electrolyte material
- H01M8/1018—Polymeric electrolyte materials
- H01M8/102—Polymeric electrolyte materials characterised by the chemical structure of the main chain of the ion-conducting polymer
- H01M8/1027—Polymeric electrolyte materials characterised by the chemical structure of the main chain of the ion-conducting polymer having carbon, oxygen and other atoms, e.g. sulfonated polyethersulfones [S-PES]
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- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
- H01M8/00—Fuel cells; Manufacture thereof
- H01M8/10—Fuel cells with solid electrolytes
- H01M8/1016—Fuel cells with solid electrolytes characterised by the electrolyte material
- H01M8/1018—Polymeric electrolyte materials
- H01M8/102—Polymeric electrolyte materials characterised by the chemical structure of the main chain of the ion-conducting polymer
- H01M8/103—Polymeric electrolyte materials characterised by the chemical structure of the main chain of the ion-conducting polymer having nitrogen, e.g. sulfonated polybenzimidazoles [S-PBI], polybenzimidazoles with phosphoric acid, sulfonated polyamides [S-PA] or sulfonated polyphosphazenes [S-PPh]
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- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
- H01M8/00—Fuel cells; Manufacture thereof
- H01M8/10—Fuel cells with solid electrolytes
- H01M8/1016—Fuel cells with solid electrolytes characterised by the electrolyte material
- H01M8/1018—Polymeric electrolyte materials
- H01M8/102—Polymeric electrolyte materials characterised by the chemical structure of the main chain of the ion-conducting polymer
- H01M8/1032—Polymeric electrolyte materials characterised by the chemical structure of the main chain of the ion-conducting polymer having sulfur, e.g. sulfonated-polyethersulfones [S-PES]
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
- H01M8/00—Fuel cells; Manufacture thereof
- H01M8/10—Fuel cells with solid electrolytes
- H01M8/1016—Fuel cells with solid electrolytes characterised by the electrolyte material
- H01M8/1018—Polymeric electrolyte materials
- H01M8/102—Polymeric electrolyte materials characterised by the chemical structure of the main chain of the ion-conducting polymer
- H01M8/1037—Polymeric electrolyte materials characterised by the chemical structure of the main chain of the ion-conducting polymer having silicon, e.g. sulfonated crosslinked polydimethylsiloxanes
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- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
- H01M8/00—Fuel cells; Manufacture thereof
- H01M8/10—Fuel cells with solid electrolytes
- H01M8/1016—Fuel cells with solid electrolytes characterised by the electrolyte material
- H01M8/1018—Polymeric electrolyte materials
- H01M8/1039—Polymeric electrolyte materials halogenated, e.g. sulfonated polyvinylidene fluorides
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- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
- H01M8/00—Fuel cells; Manufacture thereof
- H01M8/10—Fuel cells with solid electrolytes
- H01M8/1016—Fuel cells with solid electrolytes characterised by the electrolyte material
- H01M8/1018—Polymeric electrolyte materials
- H01M8/1069—Polymeric electrolyte materials characterised by the manufacturing processes
- H01M8/1081—Polymeric electrolyte materials characterised by the manufacturing processes starting from solutions, dispersions or slurries exclusively of polymers
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G2261/00—Macromolecular compounds obtained by reactions forming a carbon-to-carbon link in the main chain of the macromolecule
- C08G2261/10—Definition of the polymer structure
- C08G2261/12—Copolymers
- C08G2261/126—Copolymers block
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
- Y02E60/00—Enabling technologies; Technologies with a potential or indirect contribution to GHG emissions mitigation
- Y02E60/30—Hydrogen technology
- Y02E60/50—Fuel cells
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P70/00—Climate change mitigation technologies in the production process for final industrial or consumer products
- Y02P70/50—Manufacturing or production processes characterised by the final manufactured product
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
KR1020040110487A KR100657740B1 (ko) | 2004-12-22 | 2004-12-22 | 브랜치된 술폰화 멀티 블록 공중합체 및 이를 이용한전해질막 |
PCT/KR2005/003939 WO2006068369A1 (en) | 2004-12-22 | 2005-11-22 | Branched and sulphonated multi block copolymer and electrolyte membrane using the same |
Publications (1)
Publication Number | Publication Date |
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DE602005026166D1 true DE602005026166D1 (de) | 2011-03-10 |
Family
ID=36596268
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
DE602005026166T Active DE602005026166D1 (de) | 2004-12-22 | 2005-11-22 | Verzweigtes und sulfoniertes mehrblockcopolymer und elektrolytmembran damit |
Country Status (10)
Country | Link |
---|---|
US (1) | US7807759B2 (de) |
EP (1) | EP1828278B8 (de) |
JP (1) | JP5101889B2 (de) |
KR (1) | KR100657740B1 (de) |
CN (1) | CN100556931C (de) |
AT (1) | ATE496955T1 (de) |
CA (1) | CA2549841C (de) |
DE (1) | DE602005026166D1 (de) |
TW (1) | TWI294889B (de) |
WO (1) | WO2006068369A1 (de) |
Families Citing this family (40)
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TWI326691B (en) * | 2005-07-22 | 2010-07-01 | Kraton Polymers Res Bv | Sulfonated block copolymers, method for making same, and various uses for such block copolymers |
JP2007126645A (ja) * | 2005-10-04 | 2007-05-24 | Sumitomo Chemical Co Ltd | イオン交換性基を有する重合体およびその用途 |
KR100634551B1 (ko) * | 2005-10-12 | 2006-10-16 | 삼성에스디아이 주식회사 | 이온전도성 가교 공중합체 및 이를 포함하는 연료전지 |
KR100794466B1 (ko) * | 2005-11-30 | 2008-01-16 | 주식회사 엘지화학 | 브랜치된 술폰화 멀티 블록 공중합체 및 이를 이용한전해질막 |
KR100884959B1 (ko) * | 2006-03-20 | 2009-02-23 | 주식회사 엘지화학 | 탄화수소계 고분자 전해질막 연료전지용 막-전극 접합체의제조방법 |
US7851557B2 (en) * | 2006-06-20 | 2010-12-14 | Lg Chem, Ltd. | Organic/inorganic composite electrolyte membranes using zeolite and fuel cell comprising the same |
US20080004443A1 (en) * | 2006-07-03 | 2008-01-03 | General Electric Company | Sulfonated polyaryletherketone-block-polyethersulfone copolymers |
KR100903613B1 (ko) * | 2006-11-16 | 2009-06-18 | 삼성에스디아이 주식회사 | 연료 전지용 고분자 전해질 막 및 이를 포함하는 연료 전지시스템 |
JP4986219B2 (ja) * | 2006-12-28 | 2012-07-25 | 日東電工株式会社 | 電解質膜 |
JP2008308683A (ja) * | 2007-05-17 | 2008-12-25 | Sumitomo Chemical Co Ltd | 架橋芳香族ポリマー、高分子電解質、触媒インク、高分子電解質膜、膜−電極接合体及び燃料電池 |
US8436118B2 (en) * | 2007-06-11 | 2013-05-07 | The Hong Kong University Of Science And Technology | Synthesis of acylarylenes and hyperbranched poly(aclarylene)s by metal-free cyclotrimerization of alkynes |
KR101127320B1 (ko) * | 2008-02-13 | 2012-04-12 | 주식회사 엘지화학 | 술폰화 멀티 블록 공중합체 및 브랜치된 술폰화 멀티 블록공중합체의 제조방법 |
KR101132558B1 (ko) * | 2008-02-13 | 2012-04-03 | 주식회사 엘지화학 | 3가 방향족 불소계 화합물의 제조방법 및 이를 이용한브랜치된 술폰화 멀티 블록 공중합체의 제조방법 |
JP5262227B2 (ja) * | 2008-03-26 | 2013-08-14 | Jsr株式会社 | 芳香族化合物、分岐状ポリアリーレン系共重合体およびそれを用いた固体高分子電解質膜 |
US8012539B2 (en) | 2008-05-09 | 2011-09-06 | Kraton Polymers U.S. Llc | Method for making sulfonated block copolymers, method for making membranes from such block copolymers and membrane structures |
US7829652B2 (en) * | 2008-07-31 | 2010-11-09 | General Electric Company | Polyarylether composition and membrane |
KR101190913B1 (ko) * | 2008-08-28 | 2012-10-12 | 주식회사 엘지화학 | 브랜치된 술폰화 멀티 블록 공중합체의 제조방법 |
BRPI0920638A2 (pt) * | 2008-10-23 | 2016-01-12 | Basf Se | composto, processo para preparar compostos, material de moldagem termoplastico, uso dos materias de moldagem termoplasticos, e, corpo moldado |
JP5542833B2 (ja) * | 2008-11-04 | 2014-07-09 | エルジー・ケム・リミテッド | 高分子電解質膜 |
KR101064986B1 (ko) * | 2009-06-04 | 2011-09-15 | 강원대학교산학협력단 | 세라믹 다공성 지지체, 그를 이용한 강화 복합 전해질 막 및 그를 구비한 막-전극 어셈블리 |
US20110033776A1 (en) * | 2009-08-10 | 2011-02-10 | Board of regents of the Nevada System of Higher Education, on Behalf of the University of | Proton exchange membranes |
US8263713B2 (en) | 2009-10-13 | 2012-09-11 | Kraton Polymers U.S. Llc | Amine neutralized sulfonated block copolymers and method for making same |
US8445631B2 (en) | 2009-10-13 | 2013-05-21 | Kraton Polymers U.S. Llc | Metal-neutralized sulfonated block copolymers, process for making them and their use |
KR101223708B1 (ko) * | 2010-09-14 | 2013-01-18 | 주식회사 엘지화학 | 트리 블록 공중합체, 및 그로부터 제조되는 전해질 막 |
US9429366B2 (en) | 2010-09-29 | 2016-08-30 | Kraton Polymers U.S. Llc | Energy recovery ventilation sulfonated block copolymer laminate membrane |
US9394414B2 (en) | 2010-09-29 | 2016-07-19 | Kraton Polymers U.S. Llc | Elastic, moisture-vapor permeable films, their preparation and their use |
CN103201298B (zh) | 2010-10-18 | 2015-06-24 | 科腾聚合物美国有限责任公司 | 生产磺化的嵌段共聚物组合物的方法 |
US9861941B2 (en) | 2011-07-12 | 2018-01-09 | Kraton Polymers U.S. Llc | Modified sulfonated block copolymers and the preparation thereof |
WO2013137691A1 (ko) | 2012-03-16 | 2013-09-19 | 주식회사 엘지화학 | 고분자 전해질 조성물, 전해질 막, 막-전극 접합체 및 연료전지 |
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WO2014200286A2 (ko) * | 2013-06-14 | 2014-12-18 | 주식회사 엘지화학 | 술포네이트계 화합물 및 이를 이용한 고분자 전해질막 |
KR101546370B1 (ko) * | 2014-05-13 | 2015-08-28 | 한국에너지기술연구원 | 높은 이온전도성을 보이는 술폰산화 멀티블록형 고분자 및 이를 포함하는 전기화학 시스템 |
KR20160067720A (ko) * | 2014-12-04 | 2016-06-14 | 주식회사 엘지화학 | 중합체 및 이를 포함하는 고분자 전해질막 |
CN107004880B (zh) | 2014-12-04 | 2020-07-28 | 株式会社Lg化学 | 聚合物电解质膜 |
WO2016089154A1 (ko) * | 2014-12-04 | 2016-06-09 | 주식회사 엘지화학 | 중합체 및 이를 포함하는 고분자 전해질막 |
EP3228613B1 (de) | 2014-12-04 | 2020-06-17 | LG Chem, Ltd. | Halogenierte verbindung, polymer damit und polymerelektrolytmembran damit |
US10407521B2 (en) | 2014-12-04 | 2019-09-10 | Lg Chem, Ltd. | Polymer and polymer electrolyte membrane comprising same |
CN104389173B (zh) * | 2014-12-05 | 2016-06-29 | 重庆理工大学 | 一种结构仿生的聚合物致动器及其制备方法 |
KR101812274B1 (ko) | 2015-06-01 | 2017-12-26 | 한국에너지기술연구원 | 과불소화 연결제를 사용하지 않는 고이온성 술폰산화 멀티블록형 고분자의 제조방법, 이를 포함하는 전기화학 시스템 |
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2004
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- 2005-11-03 TW TW094138560A patent/TWI294889B/zh active
- 2005-11-21 US US11/282,488 patent/US7807759B2/en active Active
- 2005-11-22 WO PCT/KR2005/003939 patent/WO2006068369A1/en active Application Filing
- 2005-11-22 CA CA2549841A patent/CA2549841C/en active Active
- 2005-11-22 DE DE602005026166T patent/DE602005026166D1/de active Active
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Publication number | Publication date |
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US7807759B2 (en) | 2010-10-05 |
JP5101889B2 (ja) | 2012-12-19 |
EP1828278B8 (de) | 2011-03-09 |
ATE496955T1 (de) | 2011-02-15 |
US20060134494A1 (en) | 2006-06-22 |
EP1828278B1 (de) | 2011-01-26 |
EP1828278A4 (de) | 2008-09-24 |
TWI294889B (en) | 2008-03-21 |
CN1898293A (zh) | 2007-01-17 |
TW200621846A (en) | 2006-07-01 |
CN100556931C (zh) | 2009-11-04 |
EP1828278A1 (de) | 2007-09-05 |
CA2549841A1 (en) | 2006-06-22 |
KR100657740B1 (ko) | 2006-12-14 |
KR20060071690A (ko) | 2006-06-27 |
WO2006068369A1 (en) | 2006-06-29 |
JP2007523230A (ja) | 2007-08-16 |
CA2549841C (en) | 2010-01-26 |
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