DE60008933T2 - Aktivierung und regenerierung eines hydro-oxydierungskatalysators - Google Patents

Aktivierung und regenerierung eines hydro-oxydierungskatalysators Download PDF

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Publication number
DE60008933T2
DE60008933T2 DE60008933T DE60008933T DE60008933T2 DE 60008933 T2 DE60008933 T2 DE 60008933T2 DE 60008933 T DE60008933 T DE 60008933T DE 60008933 T DE60008933 T DE 60008933T DE 60008933 T2 DE60008933 T2 DE 60008933T2
Authority
DE
Germany
Prior art keywords
catalyst
hydro
oxidation
titanium
olefin
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
DE60008933T
Other languages
German (de)
English (en)
Other versions
DE60008933D1 (de
Inventor
H. Deborah PARKER
G. Robert BOWMAN
W. Howard CLARK
E. George HARTWELL
Alex Kuperman
R. Garmt MEIMA
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Dow Global Technologies LLC
Original Assignee
Dow Global Technologies LLC
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Dow Global Technologies LLC filed Critical Dow Global Technologies LLC
Application granted granted Critical
Publication of DE60008933D1 publication Critical patent/DE60008933D1/de
Publication of DE60008933T2 publication Critical patent/DE60008933T2/de
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

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Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/12—Oxidising
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D301/00—Preparation of oxiranes
    • C07D301/02—Synthesis of the oxirane ring
    • C07D301/03—Synthesis of the oxirane ring by oxidation of unsaturated compounds, or of mixtures of unsaturated and saturated compounds
    • C07D301/04—Synthesis of the oxirane ring by oxidation of unsaturated compounds, or of mixtures of unsaturated and saturated compounds with air or molecular oxygen
    • C07D301/08—Synthesis of the oxirane ring by oxidation of unsaturated compounds, or of mixtures of unsaturated and saturated compounds with air or molecular oxygen in the gaseous phase
    • C07D301/10—Synthesis of the oxirane ring by oxidation of unsaturated compounds, or of mixtures of unsaturated and saturated compounds with air or molecular oxygen in the gaseous phase with catalysts containing silver or gold
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/38—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of noble metals
    • B01J23/48—Silver or gold
    • B01J23/50—Silver
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/38—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of noble metals
    • B01J23/48—Silver or gold
    • B01J23/52—Gold
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/90—Regeneration or reactivation
    • B01J23/96—Regeneration or reactivation of catalysts comprising metals, oxides or hydroxides of the noble metals
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J38/00—Regeneration or reactivation of catalysts, in general
    • B01J38/04—Gas or vapour treating; Treating by using liquids vaporisable upon contacting spent catalyst
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J38/00—Regeneration or reactivation of catalysts, in general
    • B01J38/04—Gas or vapour treating; Treating by using liquids vaporisable upon contacting spent catalyst
    • B01J38/12—Treating with free oxygen-containing gas
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00—Technologies relating to chemical industry
    • Y02P20/50—Improvements relating to the production of bulk chemicals
    • Y02P20/584—Recycling of catalysts

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Catalysts (AREA)
  • Epoxy Compounds (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
DE60008933T 1999-12-09 2000-12-07 Aktivierung und regenerierung eines hydro-oxydierungskatalysators Expired - Lifetime DE60008933T2 (de)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
US16986299P 1999-12-09 1999-12-09
US169862P 1999-12-09
PCT/US2000/033385 WO2001041926A1 (en) 1999-12-09 2000-12-07 Activation and regeneration of a hydro-oxidation catalyst

Publications (2)

Publication Number Publication Date
DE60008933D1 DE60008933D1 (de) 2004-04-15
DE60008933T2 true DE60008933T2 (de) 2005-01-05

Family

ID=22617503

Family Applications (1)

Application Number Title Priority Date Filing Date
DE60008933T Expired - Lifetime DE60008933T2 (de) 1999-12-09 2000-12-07 Aktivierung und regenerierung eines hydro-oxydierungskatalysators

Country Status (11)

Country Link
US (1) US7018948B2 (enExample)
EP (1) EP1283747B1 (enExample)
JP (1) JP2003519560A (enExample)
KR (1) KR20030003219A (enExample)
CN (1) CN1151891C (enExample)
AT (1) ATE261341T1 (enExample)
AU (1) AU770334B2 (enExample)
BR (1) BR0016486A (enExample)
DE (1) DE60008933T2 (enExample)
ES (1) ES2213064T3 (enExample)
WO (1) WO2001041926A1 (enExample)

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US6562986B2 (en) * 1997-06-30 2003-05-13 Dow Global Technologies, Inc. Process for the direct oxidation of olefins to olefin oxides
ES2190280T3 (es) 1998-12-16 2003-07-16 Dow Global Technologies Inc Procedimiento para la oxidacion directa de olefinas a oxidos de olefina.
US6821923B1 (en) 1999-04-08 2004-11-23 Dow Global Technologies Inc. Method of preparing a catalyst containing gold and titanium
BR0211796A (pt) 2001-08-01 2004-08-03 Dow Global Technologies Inc Método para aumentar a vida útil de um catalisador de hidro-oxidação
WO2004090937A2 (en) * 2003-04-10 2004-10-21 Technion Research & Development Foundation Ltd Copper cmp slurry composition
US7541012B2 (en) 2004-07-07 2009-06-02 The Hong Kong University Of Science And Technology Catalytic material and method of production thereof
DE102004059375A1 (de) 2004-12-09 2006-06-22 Consortium für elektrochemische Industrie GmbH Auf nanoskaligem Titandioxid geträgerte Platin-Katalysatoren, deren Verwendung in der Hydrosilylierung, ein Hydrosilylierungsverfahren mit solchen Katalysatoren und Zusammensetzungen enthaltend solche Katalysatoren
US7494610B2 (en) * 2005-08-30 2009-02-24 The Hong Kong University Of Science And Technology Methods for fabricating zeolite micromembranes
US7704908B2 (en) 2005-12-22 2010-04-27 Shell Oil Company Method for reusing rhenium from a donor spent epoxidation catalyst
US7459589B2 (en) 2005-12-22 2008-12-02 Shell Oil Company Process for the preparation of an alkylene glycol
US8357812B2 (en) 2005-12-22 2013-01-22 Shell Oil Company Process for preparing a rejuvenated epoxidation catalyst
US20090325783A1 (en) * 2008-06-30 2009-12-31 Myers Daniel N Oto quench tower catalyst recovery system utilizing a low temperature fluidized drying chamber
JP5933445B2 (ja) 2009-11-27 2016-06-08 ビーエーエスエフ ソシエタス・ヨーロピアＢａｓｆ Ｓｅ チタンゼオライト触媒の製造方法
EP2600971A4 (en) 2010-08-03 2014-12-24 Aditya Birla Science And Technology Company Ltd PROCESS FOR REGENERATING A CATALYST OF TITANOSILICATE
US8742147B2 (en) * 2010-12-08 2014-06-03 Shell Oil Company Process for improving the selectivity of an EO catalyst
US8742146B2 (en) * 2010-12-08 2014-06-03 Shell Oil Company Process for improving the selectivity of an EO catalyst
CN102133547B (zh) * 2011-03-02 2013-03-20 华南理工大学 一种钒钛基烟气脱硝催化剂的臭氧处理再生方法及装置
US10598599B2 (en) 2015-11-03 2020-03-24 Savannah River Nuclear Solutions, Llc Methods and materials for determination of distribution coefficients for separation materials
WO2017127728A1 (en) * 2016-01-20 2017-07-27 President And Fellows Of Harvard College Ozone-activated nanoporous gold and methods of its use
US10994268B2 (en) * 2017-05-03 2021-05-04 Exxonmobil Chemical Patents Inc. Processes for rejuvenating catalysts
CN109174075A (zh) * 2018-09-04 2019-01-11 中国科学院上海硅酸盐研究所 一种用于光催化降解VOCs的稀土元素改性二氧化钛纳米光催化材料及其制备方法

Family Cites Families (24)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB2029719B (en) 1978-09-01 1982-12-08 Mitsubishi Rayon Co Method of regenerating an oxidized catalyst
AU641571B2 (en) * 1990-11-28 1993-09-23 Sumitomo Seika Chemicals Co., Ltd. Method for treating gas and apparatus used therefor
US5183789A (en) * 1991-03-11 1993-02-02 Exxon Research And Engineering Company Ozone regeneration of platinum, and polymetallic platinum reforming catalysts
US5365009A (en) * 1993-04-14 1994-11-15 Exxon Research And Engineering Company Heterogeneous alkylation and regeneration of alkylation catalysts
DE4425672A1 (de) 1994-07-20 1996-01-25 Basf Ag Oxidationskatalysator, Verfahren zu seiner Herstellung und Oxidationsverfahren unter Verwendung des Oxidationskatalysators
JP2615432B2 (ja) * 1994-10-28 1997-05-28 工業技術院長 金−酸化チタン含有触媒による炭化水素の部分酸化方法
US5753576A (en) 1995-05-18 1998-05-19 Arco Chemical Technology, L.P. Regeneration of a titanium-containing molecular sieve
DE19528220C1 (de) 1995-08-01 1997-01-09 Degussa Verfahren zur Regenerierung eines Katalysators und Verfahren zur Herstellung eines Epoxids in Gegenwart des Katalysators
DE19600708A1 (de) 1996-01-11 1997-07-17 Basf Ag Oxidationskatalysator mit einem Gehalt an Lanthanoidmetallen, Verfahren zu seiner Herstellung und Oxidationsverfahren unter Verwendung des Oxidationskatalysators
US5681789A (en) 1996-02-12 1997-10-28 Arco Chemical Technology, L.P. Activation of as-synthesized titanium-containing zeolites
JP4135818B2 (ja) * 1997-03-03 2008-08-20 株式会社日本触媒 炭化水素の部分酸化用触媒および炭化水素の部分酸化方法
US5932750A (en) 1996-03-21 1999-08-03 Agency Of Industrial Science And Technology Catalysts for partial oxidation of hydrocarbons and method of partial oxidation of hydrocarbons
DE69708880T2 (de) 1996-07-01 2002-04-11 The Dow Chemical Co., Midland Verfahren zur direkten oxidation von olefinen zu olefinoxiden
BE1010717A3 (fr) 1996-10-25 1998-12-01 Solvay Procede de regeneration de catalyseurs.
US5798313A (en) 1996-12-20 1998-08-25 Arco Chemical Technology, L.P. Heterogeneous catalyst regeneration
DE19723949A1 (de) * 1997-06-06 1998-12-10 Basf Ag Verfahren zur Regenerierung eines Zeolith-Katalysators
DE19723950A1 (de) * 1997-06-06 1998-12-10 Basf Ag Verfahren zur Oxidation einer mindestens eine C-C-Doppelbindung aufweisenden organischen Verbindung
BR9714951A (pt) 1997-06-30 2000-10-17 Dow Chemical Co Processo para preparar um óxido de olefina, composição de catalisador e processo para regenerar um composição.
DE19804711A1 (de) 1998-02-06 1999-08-12 Bayer Ag Verfahren zur Regenerierung von mit Goldteilchen belegten Trägerkatalysatoren für die Oxidation ungesättigter Kohlenwasserstoffe
DE19804712A1 (de) 1998-02-06 1999-08-12 Bayer Ag Verfahren zur Standzeitverlängerung von mit Goldteilen belegten Trägerkatalysatoren für die Oxidation ungesättigter Kohlenwasserstoffe
US5939569A (en) 1998-03-10 1999-08-17 Jones; C. Andrew Epoxidation process
ES2190280T3 (es) 1998-12-16 2003-07-16 Dow Global Technologies Inc Procedimiento para la oxidacion directa de olefinas a oxidos de olefina.
JP4646409B2 (ja) 1999-04-08 2011-03-09 ダウ グローバル テクノロジーズ インコーポレイティド 酸化された金触媒を使用してオレフィンをオレフィンオキシドにハイドロ酸化するための方法
JP4395580B2 (ja) * 1999-04-28 2010-01-13 独立行政法人産業技術総合研究所 エポキシドの製造方法

Also Published As

Publication number Publication date
WO2001041926A1 (en) 2001-06-14
BR0016486A (pt) 2002-11-26
CN1151891C (zh) 2004-06-02
ES2213064T3 (es) 2004-08-16
KR20030003219A (ko) 2003-01-09
EP1283747A1 (en) 2003-02-19
EP1283747B1 (en) 2004-03-10
US7018948B2 (en) 2006-03-28
JP2003519560A (ja) 2003-06-24
AU770334B2 (en) 2004-02-19
CN1414884A (zh) 2003-04-30
ATE261341T1 (de) 2004-03-15
DE60008933D1 (de) 2004-04-15
US20030212283A1 (en) 2003-11-13
AU2256701A (en) 2001-06-18

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