DE484996C - Verfahren zur Darstellung der N-Oxyaethylderivate des 4-Amino-1-oxybenzols - Google Patents
Verfahren zur Darstellung der N-Oxyaethylderivate des 4-Amino-1-oxybenzolsInfo
- Publication number
- DE484996C DE484996C DEI29545D DEI0029545D DE484996C DE 484996 C DE484996 C DE 484996C DE I29545 D DEI29545 D DE I29545D DE I0029545 D DEI0029545 D DE I0029545D DE 484996 C DE484996 C DE 484996C
- Authority
- DE
- Germany
- Prior art keywords
- amino
- oxybenzene
- preparation
- derivatives
- oxyaethyl
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 238000000034 method Methods 0.000 title claims description 6
- 238000002360 preparation method Methods 0.000 title claims description 4
- 239000002253 acid Substances 0.000 claims description 5
- LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 claims description 4
- 150000003944 halohydrins Chemical class 0.000 claims description 3
- 239000002904 solvent Substances 0.000 claims description 3
- 239000011230 binding agent Substances 0.000 claims description 2
- WGCNASOHLSPBMP-UHFFFAOYSA-N hydroxyacetaldehyde Natural products OCC=O WGCNASOHLSPBMP-UHFFFAOYSA-N 0.000 claims description 2
- 239000003085 diluting agent Substances 0.000 claims 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 6
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 description 5
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 4
- WCUXLLCKKVVCTQ-UHFFFAOYSA-M Potassium chloride Chemical compound [Cl-].[K+] WCUXLLCKKVVCTQ-UHFFFAOYSA-M 0.000 description 4
- 239000013078 crystal Substances 0.000 description 4
- QAOWNCQODCNURD-UHFFFAOYSA-N sulfuric acid Substances OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 4
- UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 description 3
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 description 3
- KWYUFKZDYYNOTN-UHFFFAOYSA-M Potassium hydroxide Chemical compound [OH-].[K+] KWYUFKZDYYNOTN-UHFFFAOYSA-M 0.000 description 3
- SZIFAVKTNFCBPC-UHFFFAOYSA-N 2-chloroethanol Chemical compound OCCCl SZIFAVKTNFCBPC-UHFFFAOYSA-N 0.000 description 2
- HEDRZPFGACZZDS-UHFFFAOYSA-N Chloroform Chemical compound ClC(Cl)Cl HEDRZPFGACZZDS-UHFFFAOYSA-N 0.000 description 2
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 2
- 150000007513 acids Chemical class 0.000 description 2
- 125000003277 amino group Chemical group 0.000 description 2
- 238000009835 boiling Methods 0.000 description 2
- 239000007795 chemical reaction product Substances 0.000 description 2
- 238000010438 heat treatment Methods 0.000 description 2
- 125000004435 hydrogen atom Chemical group [H]* 0.000 description 2
- 238000002844 melting Methods 0.000 description 2
- 230000008018 melting Effects 0.000 description 2
- 239000001103 potassium chloride Substances 0.000 description 2
- 235000011164 potassium chloride Nutrition 0.000 description 2
- 229910000029 sodium carbonate Inorganic materials 0.000 description 2
- 239000000052 vinegar Substances 0.000 description 2
- 235000021419 vinegar Nutrition 0.000 description 2
- QAOWNCQODCNURD-UHFFFAOYSA-L Sulfate Chemical compound [O-]S([O-])(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-L 0.000 description 1
- 230000001476 alcoholic effect Effects 0.000 description 1
- 150000008064 anhydrides Chemical class 0.000 description 1
- 239000006227 byproduct Substances 0.000 description 1
- 239000003610 charcoal Substances 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 238000009833 condensation Methods 0.000 description 1
- 230000005494 condensation Effects 0.000 description 1
- 239000007859 condensation product Substances 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- 238000004042 decolorization Methods 0.000 description 1
- 238000007865 diluting Methods 0.000 description 1
- 230000029142 excretion Effects 0.000 description 1
- 239000000706 filtrate Substances 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 239000002244 precipitate Substances 0.000 description 1
- 238000001953 recrystallisation Methods 0.000 description 1
- 238000010992 reflux Methods 0.000 description 1
- 238000000926 separation method Methods 0.000 description 1
- 238000007086 side reaction Methods 0.000 description 1
Classifications
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F16—ENGINEERING ELEMENTS AND UNITS; GENERAL MEASURES FOR PRODUCING AND MAINTAINING EFFECTIVE FUNCTIONING OF MACHINES OR INSTALLATIONS; THERMAL INSULATION IN GENERAL
- F16N—LUBRICATING
- F16N21/00—Conduits; Junctions; Fittings for lubrication apertures
- F16N21/04—Nozzles for connection of lubricating equipment to nipples
Landscapes
- Engineering & Computer Science (AREA)
- General Engineering & Computer Science (AREA)
- Mechanical Engineering (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Priority Applications (11)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DEI29545D DE484996C (de) | 1926-11-19 | 1926-11-19 | Verfahren zur Darstellung der N-Oxyaethylderivate des 4-Amino-1-oxybenzols |
| DEI31254D DE486772C (de) | 1926-11-19 | 1927-05-23 | Verfahren zur Darstellung der N-Oxyaethylderivate des 4-Amino-1-oxybenzols |
| DEI31517D DE487445C (de) | 1926-11-19 | 1927-06-27 | Verfahren zur Darstellung der N-Oxyaethylderivate des 2-Amino-1-oxybenzols |
| DEI32029D DE488682C (de) | 1926-11-19 | 1927-08-26 | Verfahren zur Darstellung der N-Oxyaethylderivate des 2-Amino-1-oxybenzols |
| FR649761D FR649761A (fr) | 1926-11-19 | 1927-10-10 | Procédé de fabrication des dérivés n-oxyéthyliques du 4-amino-1-oxybenzol ou du 2-amino-1-oxybenzol |
| BE345504A BE345504A (enrdf_load_stackoverflow) | 1926-11-19 | 1927-10-12 | |
| DEI32645D DE487788C (de) | 1926-11-19 | 1927-11-12 | Verfahren zur Darstellung der N-Oxyaethylderivate von Kernsubstitutionsprodukten und Homologen des 4-Amino-1-oxybenzols |
| BE352034A BE352034A (enrdf_load_stackoverflow) | 1926-11-19 | 1928-06-13 | |
| FR35448D FR35448E (fr) | 1926-11-19 | 1928-06-19 | Procédé de fabrication des dérivés n-oxyéthyliques du 4-amino-1-oxy-benzol ou du 2-amino-1-oxybenzol |
| FR35829D FR35829E (fr) | 1926-11-19 | 1928-08-31 | Procédé de fabrication des dérivés n-oxyéthyliques du 4 amino-1-oxy-benzol et du 2 amino-1-oxybenzol |
| BE354050A BE354050R (enrdf_load_stackoverflow) | 1926-11-19 | 1928-09-06 |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DEI29545D DE484996C (de) | 1926-11-19 | 1926-11-19 | Verfahren zur Darstellung der N-Oxyaethylderivate des 4-Amino-1-oxybenzols |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| DE484996C true DE484996C (de) | 1929-10-25 |
Family
ID=7187351
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DEI29545D Expired DE484996C (de) | 1926-11-19 | 1926-11-19 | Verfahren zur Darstellung der N-Oxyaethylderivate des 4-Amino-1-oxybenzols |
Country Status (2)
| Country | Link |
|---|---|
| BE (1) | BE352034A (enrdf_load_stackoverflow) |
| DE (1) | DE484996C (enrdf_load_stackoverflow) |
-
1926
- 1926-11-19 DE DEI29545D patent/DE484996C/de not_active Expired
-
1928
- 1928-06-13 BE BE352034A patent/BE352034A/fr unknown
Also Published As
| Publication number | Publication date |
|---|---|
| BE352034A (enrdf_load_stackoverflow) | 1928-07-31 |
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