DE3209069A1 - Verfahren zur herstellung von terephthalsaeure - Google Patents

Verfahren zur herstellung von terephthalsaeure

Info

Publication number
DE3209069A1
DE3209069A1 DE19823209069 DE3209069A DE3209069A1 DE 3209069 A1 DE3209069 A1 DE 3209069A1 DE 19823209069 DE19823209069 DE 19823209069 DE 3209069 A DE3209069 A DE 3209069A DE 3209069 A1 DE3209069 A1 DE 3209069A1
Authority
DE
Germany
Prior art keywords
terephthalic acid
oxidation
oxidation zone
water
temperature
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
DE19823209069
Other languages
German (de)
English (en)
Other versions
DE3209069C2 (OSRAM
Inventor
Jacques D.V. Hanotier
Monique J.S. Lasnes Chapelle Saint Lambert Hanotier-Bridoux
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Labofina SA
Original Assignee
Labofina SA
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Labofina SA filed Critical Labofina SA
Publication of DE3209069A1 publication Critical patent/DE3209069A1/de
Application granted granted Critical
Publication of DE3209069C2 publication Critical patent/DE3209069C2/de
Granted legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/16—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation
    • C07C51/21—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen
    • C07C51/255—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen of compounds containing six-membered aromatic rings without ring-splitting
    • C07C51/265—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen of compounds containing six-membered aromatic rings without ring-splitting having alkyl side chains which are oxidised to carboxyl groups
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00—Technologies relating to chemical industry
    • Y02P20/50—Improvements relating to the production of bulk chemicals
    • Y02P20/52—Improvements relating to the production of bulk chemicals using catalysts, e.g. selective catalysts

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
DE19823209069 1981-03-16 1982-03-12 Verfahren zur herstellung von terephthalsaeure Granted DE3209069A1 (de)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
US06/244,141 US4334086A (en) 1981-03-16 1981-03-16 Production of terephthalic acid

Publications (2)

Publication Number Publication Date
DE3209069A1 true DE3209069A1 (de) 1982-11-18
DE3209069C2 DE3209069C2 (OSRAM) 1992-06-25

Family

ID=22921526

Family Applications (1)

Application Number Title Priority Date Filing Date
DE19823209069 Granted DE3209069A1 (de) 1981-03-16 1982-03-12 Verfahren zur herstellung von terephthalsaeure

Country Status (10)

Country Link
US (1) US4334086A (OSRAM)
JP (1) JPS57159739A (OSRAM)
AU (1) AU546031B2 (OSRAM)
BE (1) BE892498A (OSRAM)
CA (1) CA1180026A (OSRAM)
DE (1) DE3209069A1 (OSRAM)
FR (1) FR2501673B1 (OSRAM)
GB (1) GB2094800B (OSRAM)
IT (1) IT1150686B (OSRAM)
NL (1) NL193538C (OSRAM)

Families Citing this family (70)

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KR970000136B1 (ko) * 1993-09-28 1997-01-04 브이.피. 유리예프 고순도 벤젠디카르복실산 이성질체의 제조방법
IN182716B (OSRAM) * 1994-03-22 1999-07-03 Mitsui Petrochemical Ind
CN1064659C (zh) * 1994-05-11 2001-04-18 普拉塞尔技术有限公司 有机化学物质的增强氧化
US6642407B2 (en) 2001-05-18 2003-11-04 Exxon Mobil Chemical Patents Inc. Production, purification and polymerization of aromatic dicarboxylic acids
US7485747B2 (en) * 2001-06-04 2009-02-03 Eastman Chemical Company Two stage oxidation process for the production of aromatic dicarboxylic acids
KR100905829B1 (ko) * 2001-09-28 2009-07-02 다이셀 가가꾸 고교 가부시끼가이샤 Ｎ-치환 환상 이미드 화합물로 구성된 촉매, 및 이 촉매를이용한 유기 화합물의 제조 방법
US6649773B2 (en) 2002-03-22 2003-11-18 General Electric Company Method for the manufacture of halophthalic acids and anhydrides
US6657068B2 (en) 2002-03-22 2003-12-02 General Electric Company Liquid phase oxidation of halogenated ortho-xylenes
US6657067B2 (en) 2002-03-22 2003-12-02 General Electric Company Method for the manufacture of chlorophthalic anhydride
US7276625B2 (en) * 2002-10-15 2007-10-02 Eastman Chemical Company Process for production of a carboxylic acid/diol mixture suitable for use in polyester production
US7132566B2 (en) * 2003-09-22 2006-11-07 Eastman Chemical Company Process for the purification of a crude carboxylic acid slurry
MXPA05006120A (es) * 2002-12-09 2005-08-16 Eastman Chem Co Proceso para la purificacion oxidativa de acido tereftalico.
US7074954B2 (en) * 2002-12-09 2006-07-11 Eastman Chemical Company Process for the oxidative purification of terephthalic acid
US7161027B2 (en) * 2002-12-09 2007-01-09 Eastman Chemical Company Process for the oxidative purification of terephthalic acid
JP2004217586A (ja) * 2003-01-16 2004-08-05 Mitsubishi Gas Chem Co Inc 芳香族ポリカルボン酸及び該酸無水物の製造方法
US7193109B2 (en) * 2003-03-06 2007-03-20 Eastman Chemical Company Process for production of a carboxylic acid/diol mixture suitable for use in polyester production
JP4720112B2 (ja) * 2003-06-20 2011-07-13 三菱瓦斯化学株式会社 高純度芳香族ポリカルボン酸の製造法
US7214760B2 (en) * 2004-01-15 2007-05-08 Eastman Chemical Company Process for production of a carboxylic acid/diol mixture suitable for use in polyester production
US7546747B2 (en) * 2004-01-15 2009-06-16 Eastman Chemical Company Process for production of a dried carboxylic acid cake suitable for use in polyester production
US20050283022A1 (en) * 2004-06-18 2005-12-22 Sheppard Ronald B Filtrate preparation process for terephthalic acid filtrate treatment
US20060004223A1 (en) * 2004-06-30 2006-01-05 General Electric Company Method of making halophthalic acids and halophthalic anhydrides
US7541489B2 (en) * 2004-06-30 2009-06-02 Sabic Innovative Plastics Ip B.V. Method of making halophthalic acids and halophthalic anhydrides
US7361784B2 (en) * 2004-09-02 2008-04-22 Eastman Chemical Company Optimized liquid-phase oxidation
US7371894B2 (en) * 2004-09-02 2008-05-13 Eastman Chemical Company Optimized liquid-phase oxidation
US7504535B2 (en) 2004-09-02 2009-03-17 Eastman Chemical Company Optimized liquid-phase oxidation
US7692036B2 (en) 2004-11-29 2010-04-06 Eastman Chemical Company Optimized liquid-phase oxidation
US7572936B2 (en) 2004-09-02 2009-08-11 Eastman Chemical Company Optimized liquid-phase oxidation
US7507857B2 (en) * 2004-09-02 2009-03-24 Eastman Chemical Company Optimized liquid-phase oxidation
US7608733B2 (en) * 2004-09-02 2009-10-27 Eastman Chemical Company Optimized liquid-phase oxidation
US7589231B2 (en) * 2004-09-02 2009-09-15 Eastman Chemical Company Optimized liquid-phase oxidation
US7683210B2 (en) * 2004-09-02 2010-03-23 Eastman Chemical Company Optimized liquid-phase oxidation
US7381836B2 (en) * 2004-09-02 2008-06-03 Eastman Chemical Company Optimized liquid-phase oxidation
US7399882B2 (en) * 2004-09-02 2008-07-15 Eastman Chemical Company Optimized liquid-phase oxidation
US7482482B2 (en) * 2004-09-02 2009-01-27 Eastman Chemical Company Optimized liquid-phase oxidation
US7608732B2 (en) * 2005-03-08 2009-10-27 Eastman Chemical Company Optimized liquid-phase oxidation
US7741515B2 (en) 2004-09-02 2010-06-22 Eastman Chemical Company Optimized liquid-phase oxidation
US7568361B2 (en) * 2004-09-02 2009-08-04 Eastman Chemical Company Optimized liquid-phase oxidation
US20060047153A1 (en) * 2004-09-02 2006-03-02 Wonders Alan G Optimized liquid-phase oxidation
US7692037B2 (en) * 2004-09-02 2010-04-06 Eastman Chemical Company Optimized liquid-phase oxidation
US7586000B2 (en) * 2004-09-02 2009-09-08 Eastman Chemical Company Optimized liquid-phase oxidation
US7910769B2 (en) * 2004-09-02 2011-03-22 Eastman Chemical Company Optimized liquid-phase oxidation
US7582793B2 (en) 2004-09-02 2009-09-01 Eastman Chemical Company Optimized liquid-phase oxidation
US7495125B2 (en) * 2004-09-02 2009-02-24 Eastman Chemical Company Optimized liquid-phase oxidation
US7390921B2 (en) * 2004-09-02 2008-06-24 Eastman Chemical Company Optimized liquid-phase oxidation
US7563926B2 (en) * 2004-09-02 2009-07-21 Eastman Chemical Company Optimized liquid-phase oxidation
US7572932B2 (en) * 2004-09-02 2009-08-11 Eastman Chemical Company Optimized liquid-phase oxidation
US7615663B2 (en) * 2004-09-02 2009-11-10 Eastman Chemical Company Optimized production of aromatic dicarboxylic acids
US7598415B2 (en) * 2005-03-22 2009-10-06 Council Of Scientific & Industrial Research Process for the preparation of p-toluic acid by liquid phase oxidation of p-xylene in water
WO2006109999A1 (en) * 2005-04-14 2006-10-19 Amtpacific Co., Ltd. Recovering method of acetic acid from effluent of terephthalic acid production process
US7884232B2 (en) * 2005-06-16 2011-02-08 Eastman Chemical Company Optimized liquid-phase oxidation
US7358389B2 (en) * 2006-01-04 2008-04-15 Eastman Chemical Company Oxidation system employing internal structure for enhanced hydrodynamics
US7355068B2 (en) * 2006-01-04 2008-04-08 Eastman Chemical Company Oxidation system with internal secondary reactor
US20070179312A1 (en) * 2006-02-02 2007-08-02 O'meadhra Ruairi Seosamh Process for the purification of a crude carboxylic axid slurry
RU2008148178A (ru) * 2006-05-08 2010-06-20 Бп Корпорейшн Норт Америка Инк. (Us) Способ окисления ароматических соединений и катализатор, используемый в этом способе
KR20090097197A (ko) * 2006-12-21 2009-09-15 이 아이 듀폰 디 네모아 앤드 캄파니 할로겐화 방향족 이산의 합성 방법
CN101279904A (zh) * 2007-04-03 2008-10-08 波克股份有限公司 制造芳族羧酸的改进方法
CA2685468A1 (en) * 2007-05-04 2008-11-13 Bp Corporation North America Inc. Process and catalyst for oxidizing aromatic compounds
US8614350B2 (en) 2008-01-15 2013-12-24 Eastman Chemical Company Carboxylic acid production process employing solvent from esterification of lignocellulosic material
US8455680B2 (en) 2008-01-15 2013-06-04 Eastman Chemical Company Carboxylic acid production process employing solvent from esterification of lignocellulosic material
KR101278303B1 (ko) * 2008-01-25 2013-06-25 삼성석유화학(주) 다단계의 산화방식을 적용한 친환경적인 테레프탈산 제조방법
KR101194067B1 (ko) * 2008-01-25 2012-10-24 삼성석유화학(주) 테레프탈산 제조에서의 결정화 및 고액 분리 공정
US8466312B2 (en) * 2010-08-20 2013-06-18 Grupo Petrotemex, S.A. De C.V. Terephthalic acid purge filtration rate by controlling % water in filter feed slurry
KR101264603B1 (ko) * 2011-09-15 2013-05-24 강기준 에너지 기여 결합 증류를 이용한 방향족 화합물 산화반응시 반응기 배출물로부터 물을 분리하고 카르복실산을 회수하는 장치 및 방법
US9024059B2 (en) 2011-12-29 2015-05-05 Uop Llc Process for producing terephthalic acid
CN104011005A (zh) * 2011-12-29 2014-08-27 环球油品公司 制备对苯二酸的方法
US9156765B2 (en) 2011-12-29 2015-10-13 Uop Llc Process for oxidizing alkyl-aromatic compounds
US8927764B2 (en) 2011-12-29 2015-01-06 Uop Llc Process for producing terephthalic acid
US9085522B2 (en) 2011-12-29 2015-07-21 Uop Llc Process for producing terephthalic acid
CN111569454B (zh) * 2020-03-31 2021-07-09 南京延长反应技术研究院有限公司 对二甲苯制备对苯二甲酸的内置微界面氧化系统及方法
CN111389314B (zh) * 2020-03-31 2020-12-11 南京延长反应技术研究院有限公司 Px生产pta的内置微界面机组强化反应系统及工艺

Citations (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2907792A (en) * 1955-08-24 1959-10-06 Ici Ltd Oxidation of organic substances
US3064044A (en) * 1957-08-15 1962-11-13 Standard Oil Co Multistage oxidation system for preparing dicarboxylic acid
DE2362295A1 (de) * 1972-12-14 1974-06-20 Halcon International Inc Verfahren zur herstellung von isooder terephthalsaeure
DE2745918A1 (de) * 1976-10-26 1978-04-27 Labofina Sa Verfahren zur herstellung von terephthalsaeure
GB1555246A (en) * 1975-10-24 1979-11-07 Standard Oil Co Secondary oxidation of fluid effluent from primary oxidation of meta- or paraxylene
DE2928361A1 (de) * 1978-07-21 1980-02-28 Mitsubishi Gas Chemical Co Verfahren zur herstellung von hochreiner terephthalsaeure
DE2939510A1 (de) * 1978-10-02 1980-04-03 Labofina Sa Verfahren zur herstellung von terephthalsaeure

Family Cites Families (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2962361A (en) * 1957-08-12 1960-11-29 Standard Oil Co Continuous oxidation system for producing carboxylic acids
FR1417520A (fr) * 1963-12-11 1965-11-12 Standard Oil Co Perfectionnements apportés aux procédés pour la préparation d'acide téréphtalique
JPS5949212B2 (ja) * 1976-09-16 1984-12-01 三菱化学株式会社 テレフタル酸の製造法
NL188282C (nl) * 1977-04-04 1992-05-18 Montedison Spa Werkwijze voor de synthese van tereftaalzuur door oxyderen van p-xyleen in azijnzuuroplossing.
GB1583755A (en) * 1977-08-03 1981-02-04 Ici Ltd Terephthalic acid manufacture

Patent Citations (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2907792A (en) * 1955-08-24 1959-10-06 Ici Ltd Oxidation of organic substances
US3064044A (en) * 1957-08-15 1962-11-13 Standard Oil Co Multistage oxidation system for preparing dicarboxylic acid
DE2362295A1 (de) * 1972-12-14 1974-06-20 Halcon International Inc Verfahren zur herstellung von isooder terephthalsaeure
GB1555246A (en) * 1975-10-24 1979-11-07 Standard Oil Co Secondary oxidation of fluid effluent from primary oxidation of meta- or paraxylene
DE2745918A1 (de) * 1976-10-26 1978-04-27 Labofina Sa Verfahren zur herstellung von terephthalsaeure
DE2928361A1 (de) * 1978-07-21 1980-02-28 Mitsubishi Gas Chemical Co Verfahren zur herstellung von hochreiner terephthalsaeure
DE2939510A1 (de) * 1978-10-02 1980-04-03 Labofina Sa Verfahren zur herstellung von terephthalsaeure

Also Published As

Publication number Publication date
IT8220185A1 (it) 1983-09-16
US4334086A (en) 1982-06-08
IT1150686B (it) 1986-12-17
JPH0259820B2 (OSRAM) 1990-12-13
DE3209069C2 (OSRAM) 1992-06-25
BE892498A (fr) 1982-07-01
GB2094800A (en) 1982-09-22
IT8220185A0 (it) 1982-03-16
NL193538C (nl) 2000-01-04
AU546031B2 (en) 1985-08-08
NL8201046A (nl) 1982-10-18
GB2094800B (en) 1985-04-03
FR2501673B1 (fr) 1986-05-02
JPS57159739A (en) 1982-10-01
AU8041882A (en) 1982-11-04
FR2501673A1 (fr) 1982-09-17
CA1180026A (en) 1984-12-27
NL193538B (nl) 1999-09-01

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Legal Events

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8110 Request for examination paragraph 44
D2 Grant after examination
8364 No opposition during term of opposition