DE3008286C2 - Kontinuierliches Verfahren zur Herstellung von nicht vernetzten Orthophosphorsäuremonoestern der Stärke - Google Patents
Kontinuierliches Verfahren zur Herstellung von nicht vernetzten Orthophosphorsäuremonoestern der StärkeInfo
- Publication number
- DE3008286C2 DE3008286C2 DE3008286A DE3008286A DE3008286C2 DE 3008286 C2 DE3008286 C2 DE 3008286C2 DE 3008286 A DE3008286 A DE 3008286A DE 3008286 A DE3008286 A DE 3008286A DE 3008286 C2 DE3008286 C2 DE 3008286C2
- Authority
- DE
- Germany
- Prior art keywords
- starch
- cake
- solution
- impregnation
- salt
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 229920002472 Starch Polymers 0.000 title claims description 141
- 235000019698 starch Nutrition 0.000 title claims description 141
- 239000008107 starch Substances 0.000 title claims description 134
- NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 title claims description 24
- 235000011007 phosphoric acid Nutrition 0.000 title claims description 12
- 238000004519 manufacturing process Methods 0.000 title claims description 7
- 238000010924 continuous production Methods 0.000 title claims description 5
- 150000003013 phosphoric acid derivatives Chemical class 0.000 claims description 34
- 229920000881 Modified starch Polymers 0.000 claims description 14
- 238000006366 phosphorylation reaction Methods 0.000 claims description 13
- 235000019426 modified starch Nutrition 0.000 claims description 12
- 230000026731 phosphorylation Effects 0.000 claims description 12
- 229910000318 alkali metal phosphate Inorganic materials 0.000 claims description 8
- 238000001035 drying Methods 0.000 claims description 8
- 238000010438 heat treatment Methods 0.000 claims description 7
- 239000007864 aqueous solution Substances 0.000 claims description 4
- 239000000243 solution Substances 0.000 description 66
- 238000000034 method Methods 0.000 description 40
- 239000003153 chemical reaction reagent Substances 0.000 description 39
- 238000005470 impregnation Methods 0.000 description 34
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 29
- 239000002002 slurry Substances 0.000 description 20
- 150000003839 salts Chemical class 0.000 description 18
- 230000008569 process Effects 0.000 description 17
- 239000000047 product Substances 0.000 description 16
- 238000006243 chemical reaction Methods 0.000 description 15
- NBIIXXVUZAFLBC-UHFFFAOYSA-K phosphate Chemical compound [O-]P([O-])([O-])=O NBIIXXVUZAFLBC-UHFFFAOYSA-K 0.000 description 15
- UNXRWKVEANCORM-UHFFFAOYSA-I triphosphate(5-) Chemical class [O-]P([O-])(=O)OP([O-])(=O)OP([O-])([O-])=O UNXRWKVEANCORM-UHFFFAOYSA-I 0.000 description 15
- 235000019832 sodium triphosphate Nutrition 0.000 description 14
- OAICVXFJPJFONN-UHFFFAOYSA-N Phosphorus Chemical compound [P] OAICVXFJPJFONN-UHFFFAOYSA-N 0.000 description 13
- 229910052698 phosphorus Inorganic materials 0.000 description 13
- 239000011574 phosphorus Substances 0.000 description 13
- 239000007787 solid Substances 0.000 description 11
- 238000001914 filtration Methods 0.000 description 10
- 230000014759 maintenance of location Effects 0.000 description 10
- 229920002261 Corn starch Polymers 0.000 description 9
- 239000008120 corn starch Substances 0.000 description 9
- 239000000049 pigment Substances 0.000 description 9
- XPPKVPWEQAFLFU-UHFFFAOYSA-J diphosphate(4-) Chemical compound [O-]P([O-])(=O)OP([O-])([O-])=O XPPKVPWEQAFLFU-UHFFFAOYSA-J 0.000 description 8
- 238000002156 mixing Methods 0.000 description 8
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 7
- 229910052783 alkali metal Inorganic materials 0.000 description 7
- 125000002091 cationic group Chemical group 0.000 description 7
- 239000000706 filtrate Substances 0.000 description 7
- -1 Alkali metal tripolyphosphate salts Chemical class 0.000 description 6
- 239000013068 control sample Substances 0.000 description 6
- 239000000203 mixture Substances 0.000 description 6
- 239000007921 spray Substances 0.000 description 6
- 240000003183 Manihot esculenta Species 0.000 description 5
- 235000016735 Manihot esculenta subsp esculenta Nutrition 0.000 description 5
- 239000002253 acid Substances 0.000 description 5
- 238000009826 distribution Methods 0.000 description 5
- 230000035515 penetration Effects 0.000 description 5
- 238000002360 preparation method Methods 0.000 description 5
- 230000000717 retained effect Effects 0.000 description 5
- 239000000725 suspension Substances 0.000 description 5
- RAGSWDIQBBZLLL-UHFFFAOYSA-N 2-chloroethyl(diethyl)azanium;chloride Chemical compound Cl.CCN(CC)CCCl RAGSWDIQBBZLLL-UHFFFAOYSA-N 0.000 description 4
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 4
- 240000008042 Zea mays Species 0.000 description 4
- 235000016383 Zea mays subsp huehuetenangensis Nutrition 0.000 description 4
- 235000002017 Zea mays subsp mays Nutrition 0.000 description 4
- 238000007865 diluting Methods 0.000 description 4
- 235000009973 maize Nutrition 0.000 description 4
- 239000000463 material Substances 0.000 description 4
- 238000005507 spraying Methods 0.000 description 4
- 239000000126 substance Substances 0.000 description 4
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 3
- 229940037003 alum Drugs 0.000 description 3
- 235000011180 diphosphates Nutrition 0.000 description 3
- BNIILDVGGAEEIG-UHFFFAOYSA-L disodium hydrogen phosphate Chemical compound [Na+].[Na+].OP([O-])([O-])=O BNIILDVGGAEEIG-UHFFFAOYSA-L 0.000 description 3
- 239000004744 fabric Substances 0.000 description 3
- 239000012065 filter cake Substances 0.000 description 3
- 239000000843 powder Substances 0.000 description 3
- FQENQNTWSFEDLI-UHFFFAOYSA-J sodium diphosphate Chemical compound [Na+].[Na+].[Na+].[Na+].[O-]P([O-])(=O)OP([O-])([O-])=O FQENQNTWSFEDLI-UHFFFAOYSA-J 0.000 description 3
- 235000019818 tetrasodium diphosphate Nutrition 0.000 description 3
- 239000002351 wastewater Substances 0.000 description 3
- 229920000856 Amylose Polymers 0.000 description 2
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 description 2
- 229910019142 PO4 Inorganic materials 0.000 description 2
- 150000007513 acids Chemical class 0.000 description 2
- 230000009471 action Effects 0.000 description 2
- 150000001340 alkali metals Chemical class 0.000 description 2
- 235000013339 cereals Nutrition 0.000 description 2
- 239000007795 chemical reaction product Substances 0.000 description 2
- 150000001875 compounds Chemical class 0.000 description 2
- 238000011109 contamination Methods 0.000 description 2
- 238000010790 dilution Methods 0.000 description 2
- 239000012895 dilution Substances 0.000 description 2
- 229910000397 disodium phosphate Inorganic materials 0.000 description 2
- 235000019800 disodium phosphate Nutrition 0.000 description 2
- 150000002148 esters Chemical class 0.000 description 2
- 235000013305 food Nutrition 0.000 description 2
- 239000007788 liquid Substances 0.000 description 2
- 239000012452 mother liquor Substances 0.000 description 2
- 229910052757 nitrogen Inorganic materials 0.000 description 2
- 239000010452 phosphate Substances 0.000 description 2
- 239000002994 raw material Substances 0.000 description 2
- 239000012266 salt solution Substances 0.000 description 2
- 239000000523 sample Substances 0.000 description 2
- 239000010865 sewage Substances 0.000 description 2
- 238000001694 spray drying Methods 0.000 description 2
- 238000003860 storage Methods 0.000 description 2
- MELCWEWUZODSIS-UHFFFAOYSA-N 2-[2-(diethylamino)ethoxy]-n,n-diethylethanamine Chemical compound CCN(CC)CCOCCN(CC)CC MELCWEWUZODSIS-UHFFFAOYSA-N 0.000 description 1
- QGZKDVFQNNGYKY-UHFFFAOYSA-O Ammonium Chemical compound [NH4+] QGZKDVFQNNGYKY-UHFFFAOYSA-O 0.000 description 1
- QXNVGIXVLWOKEQ-UHFFFAOYSA-N Disodium Chemical compound [Na][Na] QXNVGIXVLWOKEQ-UHFFFAOYSA-N 0.000 description 1
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 1
- WHXSMMKQMYFTQS-UHFFFAOYSA-N Lithium Chemical compound [Li] WHXSMMKQMYFTQS-UHFFFAOYSA-N 0.000 description 1
- 238000005481 NMR spectroscopy Methods 0.000 description 1
- 240000007594 Oryza sativa Species 0.000 description 1
- 235000007164 Oryza sativa Nutrition 0.000 description 1
- ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 description 1
- 108091081062 Repeated sequence (DNA) Proteins 0.000 description 1
- 244000061456 Solanum tuberosum Species 0.000 description 1
- 235000002595 Solanum tuberosum Nutrition 0.000 description 1
- 240000006394 Sorghum bicolor Species 0.000 description 1
- 235000011684 Sorghum saccharatum Nutrition 0.000 description 1
- 235000021307 Triticum Nutrition 0.000 description 1
- 244000098338 Triticum aestivum Species 0.000 description 1
- MZVQCMJNVPIDEA-UHFFFAOYSA-N [CH2]CN(CC)CC Chemical group [CH2]CN(CC)CC MZVQCMJNVPIDEA-UHFFFAOYSA-N 0.000 description 1
- 238000010521 absorption reaction Methods 0.000 description 1
- 238000010306 acid treatment Methods 0.000 description 1
- 230000002411 adverse Effects 0.000 description 1
- 229910000147 aluminium phosphate Inorganic materials 0.000 description 1
- 238000004458 analytical method Methods 0.000 description 1
- 229920006320 anionic starch Polymers 0.000 description 1
- 230000008901 benefit Effects 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 238000009835 boiling Methods 0.000 description 1
- 239000013065 commercial product Substances 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- 238000009795 derivation Methods 0.000 description 1
- 150000002170 ethers Chemical class 0.000 description 1
- 239000011521 glass Substances 0.000 description 1
- 239000008187 granular material Substances 0.000 description 1
- 229910052739 hydrogen Inorganic materials 0.000 description 1
- 239000001257 hydrogen Substances 0.000 description 1
- 230000006872 improvement Effects 0.000 description 1
- 229910052816 inorganic phosphate Inorganic materials 0.000 description 1
- 229910052744 lithium Inorganic materials 0.000 description 1
- 125000005341 metaphosphate group Chemical group 0.000 description 1
- CXKWCBBOMKCUKX-UHFFFAOYSA-M methylene blue Chemical compound [Cl-].C1=CC(N(C)C)=CC2=[S+]C3=CC(N(C)C)=CC=C3N=C21 CXKWCBBOMKCUKX-UHFFFAOYSA-M 0.000 description 1
- 229960000907 methylthioninium chloride Drugs 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 239000000178 monomer Substances 0.000 description 1
- 235000016709 nutrition Nutrition 0.000 description 1
- 230000001590 oxidative effect Effects 0.000 description 1
- 238000004806 packaging method and process Methods 0.000 description 1
- 230000010287 polarization Effects 0.000 description 1
- 229910052700 potassium Inorganic materials 0.000 description 1
- 239000011591 potassium Substances 0.000 description 1
- 229920001592 potato starch Polymers 0.000 description 1
- 235000012015 potatoes Nutrition 0.000 description 1
- 238000003825 pressing Methods 0.000 description 1
- 230000001105 regulatory effect Effects 0.000 description 1
- 235000009566 rice Nutrition 0.000 description 1
- 229910052708 sodium Inorganic materials 0.000 description 1
- 239000011734 sodium Substances 0.000 description 1
- AJPJDKMHJJGVTQ-UHFFFAOYSA-M sodium dihydrogen phosphate Chemical compound [Na+].OP(O)([O-])=O AJPJDKMHJJGVTQ-UHFFFAOYSA-M 0.000 description 1
- BBMHARZCALWXSL-UHFFFAOYSA-M sodium dihydrogenphosphate monohydrate Chemical compound O.[Na+].OP(O)([O-])=O BBMHARZCALWXSL-UHFFFAOYSA-M 0.000 description 1
- 230000003068 static effect Effects 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
- 238000006467 substitution reaction Methods 0.000 description 1
- 239000002352 surface water Substances 0.000 description 1
- 238000009827 uniform distribution Methods 0.000 description 1
- 238000005406 washing Methods 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08B—POLYSACCHARIDES; DERIVATIVES THEREOF
- C08B31/00—Preparation of derivatives of starch
- C08B31/02—Esters
- C08B31/06—Esters of inorganic acids
- C08B31/066—Starch phosphates, e.g. phosphorylated starch
Landscapes
- Chemical & Material Sciences (AREA)
- Inorganic Chemistry (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Biochemistry (AREA)
- Materials Engineering (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Organic Chemistry (AREA)
- Polysaccharides And Polysaccharide Derivatives (AREA)
- Chemical Or Physical Treatment Of Fibers (AREA)
- Solid-Sorbent Or Filter-Aiding Compositions (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US06/031,507 US4216310A (en) | 1979-04-19 | 1979-04-19 | Continuous process for phosphorylating starch |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| DE3008286A1 DE3008286A1 (de) | 1980-10-30 |
| DE3008286C2 true DE3008286C2 (de) | 1984-01-05 |
Family
ID=21859847
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE3008286A Expired DE3008286C2 (de) | 1979-04-19 | 1980-03-04 | Kontinuierliches Verfahren zur Herstellung von nicht vernetzten Orthophosphorsäuremonoestern der Stärke |
Country Status (8)
| Country | Link |
|---|---|
| US (1) | US4216310A (oth) |
| JP (1) | JPS55142001A (oth) |
| CA (1) | CA1118773A (oth) |
| DE (1) | DE3008286C2 (oth) |
| FR (1) | FR2454446A1 (oth) |
| GB (1) | GB2047726B (oth) |
| IT (1) | IT1130925B (oth) |
| NL (1) | NL183935C (oth) |
Families Citing this family (19)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4876336A (en) * | 1986-08-13 | 1989-10-24 | National Starch And Chemical Corporation | Amphoteric starches and process for their preparation |
| US4964953A (en) * | 1986-08-13 | 1990-10-23 | National Starch And Chemical Investment Holding Corporation | Amphoteric starches and process for their preparation |
| JPS6348301A (ja) * | 1986-08-13 | 1988-03-01 | ナシヨナル・スターチ・アンド・ケミカル・インベストメント・ホルデイング・コーポレイシヨン | 改良された両性デンプンおよびそれらの製造方法 |
| US5122231A (en) * | 1990-06-08 | 1992-06-16 | Cargill, Incorporated | Cationic cross-linked starch for wet-end use in papermaking |
| US5329004A (en) * | 1991-12-12 | 1994-07-12 | National Starch And Chemical Investment Holding Corporation | Method of manufacturing cigarettes using high amylopectin starch phosphate material as an adhesive |
| CA2132685A1 (en) * | 1994-09-22 | 1996-03-23 | Robert T. Tyler | An aqueous alcoholic alkaline process for cationization of normal, waxy and high amylose starches from legume, cereal, tuber and root |
| ES2149251T3 (es) * | 1994-11-03 | 2000-11-01 | Vomm Impianti & Processi Srl | Metodo para la modificacion de almidon. |
| US5981445A (en) * | 1996-06-17 | 1999-11-09 | Corporation De I'ecole Polytechnique | Process of making fine ceramic powders from aqueous suspensions |
| JP4200537B2 (ja) * | 1998-03-06 | 2008-12-24 | 王子製紙株式会社 | 高いＣａ可溶化活性を有するリン酸結合澱粉とそのオリゴ糖組成物及びそれらの製造方法 |
| US6413372B1 (en) | 1999-04-20 | 2002-07-02 | National Starch And Chemical Investment Holding Corporation | Starch polymer combinations used in papermaking |
| JP4486188B2 (ja) * | 1999-09-30 | 2010-06-23 | 王子コーンスターチ株式会社 | 両性澱粉の製造方法 |
| US6428836B1 (en) | 2000-08-07 | 2002-08-06 | National Starch And Chemical Investment Holding Corporation | Starch phosphate ester composition, process and method of use in food |
| US6365002B1 (en) * | 2000-08-07 | 2002-04-02 | National Starch And Chemical Investment Holding Corporation | Amphoteric starches used in papermaking |
| DE60133298T2 (de) * | 2000-10-06 | 2009-03-05 | Coöperatie Avebe U.A. | Waschen und entwässern von suspensionen |
| US6461656B1 (en) * | 2001-01-26 | 2002-10-08 | Natinal Starch And Chemical Investment Holding Corporation | Starch phosphate ester for use as an expansion aid |
| US20030148011A1 (en) * | 2002-02-06 | 2003-08-07 | Trksak Ralph M. | Stabilizer for acidified milk beverages |
| CN100577687C (zh) * | 2007-04-09 | 2010-01-06 | 中国科学院广州化学研究所 | 一种磷酸酯化淀粉的制备方法 |
| KR20190051656A (ko) * | 2017-11-07 | 2019-05-15 | 삼성전자주식회사 | 식각 조성물, 실리콘 질화막의 식각 방법, 및 반도체 소자의 제조 방법 |
| BR112022023363A2 (pt) | 2020-05-28 | 2022-12-20 | Cargill Inc | Método para preparar uma mistura |
Family Cites Families (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2806026A (en) * | 1954-06-25 | 1957-09-10 | American Maize Prod Co | Process of preparing starch derivatives |
| US2824870A (en) * | 1954-09-16 | 1958-02-25 | Int Minerals & Chem Corp | Urea-modified alkali metal starch phosphates |
| FR1143043A (fr) * | 1955-09-09 | 1957-09-25 | Int Minerals & Chem Corp | Perfectionnements à un procédé de préparation de phosphates d'amidon |
| US2884413A (en) * | 1956-04-06 | 1959-04-28 | Corn Products Co | Orthophosphate esters of starch |
| US3132066A (en) * | 1961-05-04 | 1964-05-05 | Corn Products Co | Process of adding starch phosphates to paper pulp containing titanium dioxide to improve retention thereof |
| US3399200A (en) * | 1965-03-15 | 1968-08-27 | American Maize Prod Co | Method of producing starch phosphate products continuously |
| NL134024C (oth) * | 1965-11-17 | 1900-01-01 | ||
| US3793310A (en) * | 1972-11-24 | 1974-02-19 | Hubinger Co | Amphoteric starch and preparation and uses therefor |
| US4166173A (en) * | 1978-05-15 | 1979-08-28 | National Starch And Chemical Corporation | Process for phosphorylating starch in alkali metal tripolyphosphate salts |
-
1979
- 1979-04-19 US US06/031,507 patent/US4216310A/en not_active Expired - Lifetime
-
1980
- 1980-01-22 CA CA000344195A patent/CA1118773A/en not_active Expired
- 1980-02-26 NL NLAANVRAGE8001154,A patent/NL183935C/xx not_active IP Right Cessation
- 1980-03-04 DE DE3008286A patent/DE3008286C2/de not_active Expired
- 1980-03-06 IT IT20393/80A patent/IT1130925B/it active
- 1980-03-10 FR FR8005294A patent/FR2454446A1/fr active Granted
- 1980-03-19 GB GB8009163A patent/GB2047726B/en not_active Expired
- 1980-04-15 JP JP4879680A patent/JPS55142001A/ja active Pending
Also Published As
| Publication number | Publication date |
|---|---|
| FR2454446A1 (fr) | 1980-11-14 |
| NL183935C (nl) | 1989-03-01 |
| CA1118773A (en) | 1982-02-23 |
| NL183935B (nl) | 1988-10-03 |
| FR2454446B1 (oth) | 1983-11-18 |
| DE3008286A1 (de) | 1980-10-30 |
| GB2047726A (en) | 1980-12-03 |
| NL8001154A (nl) | 1980-10-21 |
| IT8020393A0 (it) | 1980-03-06 |
| US4216310A (en) | 1980-08-05 |
| GB2047726B (en) | 1982-12-08 |
| JPS55142001A (en) | 1980-11-06 |
| IT1130925B (it) | 1986-06-18 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| OAP | Request for examination filed | ||
| OD | Request for examination | ||
| 8128 | New person/name/address of the agent |
Representative=s name: GEYER, W., DIPL.-ING. DR.-ING. HAGEMANN, H., DIPL. |
|
| D2 | Grant after examination | ||
| 8328 | Change in the person/name/address of the agent |
Free format text: GEYER, W., DIPL.-ING. DR.-ING. HAGEMANN, H., DIPL.-CHEM. DR.RER.NAT., PAT.-ANW., 8000 MUENCHEN |
|
| 8364 | No opposition during term of opposition | ||
| 8328 | Change in the person/name/address of the agent |
Free format text: HAGEMANN, H., DIPL.-CHEM. DR.RER.NAT., PAT.-ANW., 8000 MUENCHEN |