DE2220956C3 - Verfahren zur Herstellung von Pigmenten auf Basis von Eisenoxiden - Google Patents
Verfahren zur Herstellung von Pigmenten auf Basis von EisenoxidenInfo
- Publication number
- DE2220956C3 DE2220956C3 DE2220956A DE2220956A DE2220956C3 DE 2220956 C3 DE2220956 C3 DE 2220956C3 DE 2220956 A DE2220956 A DE 2220956A DE 2220956 A DE2220956 A DE 2220956A DE 2220956 C3 DE2220956 C3 DE 2220956C3
- Authority
- DE
- Germany
- Prior art keywords
- temperatures
- precipitate
- goethite
- zinc
- washed
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 239000000049 pigment Substances 0.000 title claims description 17
- UQSXHKLRYXJYBZ-UHFFFAOYSA-N iron oxide Inorganic materials [Fe]=O UQSXHKLRYXJYBZ-UHFFFAOYSA-N 0.000 title claims description 13
- 238000000034 method Methods 0.000 title claims description 13
- 235000013980 iron oxide Nutrition 0.000 title claims description 10
- VBMVTYDPPZVILR-UHFFFAOYSA-N iron(2+);oxygen(2-) Chemical class [O-2].[Fe+2] VBMVTYDPPZVILR-UHFFFAOYSA-N 0.000 title claims description 9
- 238000004519 manufacturing process Methods 0.000 title claims description 7
- XEEYBQQBJWHFJM-UHFFFAOYSA-N iron Substances [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 claims description 28
- XLOMVQKBTHCTTD-UHFFFAOYSA-N Zinc monoxide Chemical compound [Zn]=O XLOMVQKBTHCTTD-UHFFFAOYSA-N 0.000 claims description 16
- 229910052725 zinc Inorganic materials 0.000 claims description 14
- 239000011701 zinc Substances 0.000 claims description 14
- 229910052742 iron Inorganic materials 0.000 claims description 13
- 239000002244 precipitate Substances 0.000 claims description 13
- 229910052598 goethite Inorganic materials 0.000 claims description 12
- HCHKCACWOHOZIP-UHFFFAOYSA-N Zinc Chemical compound [Zn] HCHKCACWOHOZIP-UHFFFAOYSA-N 0.000 claims description 11
- AEIXRCIKZIZYPM-UHFFFAOYSA-M hydroxy(oxo)iron Chemical compound [O][Fe]O AEIXRCIKZIZYPM-UHFFFAOYSA-M 0.000 claims description 9
- 239000000463 material Substances 0.000 claims description 8
- 239000011787 zinc oxide Substances 0.000 claims description 8
- 239000012535 impurity Substances 0.000 claims description 7
- 239000007788 liquid Substances 0.000 claims description 7
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 claims description 6
- 229910052760 oxygen Inorganic materials 0.000 claims description 6
- 239000001301 oxygen Substances 0.000 claims description 6
- 238000001556 precipitation Methods 0.000 claims description 6
- 238000002386 leaching Methods 0.000 claims description 5
- 239000000047 product Substances 0.000 claims description 5
- 229910002588 FeOOH Inorganic materials 0.000 claims description 4
- QAOWNCQODCNURD-UHFFFAOYSA-L Sulfate Chemical compound [O-]S([O-])(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-L 0.000 claims description 4
- 230000003647 oxidation Effects 0.000 claims description 4
- 238000007254 oxidation reaction Methods 0.000 claims description 4
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 claims description 3
- 229910052739 hydrogen Inorganic materials 0.000 claims description 3
- 239000001257 hydrogen Substances 0.000 claims description 3
- 238000000926 separation method Methods 0.000 claims description 3
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 claims description 2
- PTFCDOFLOPIGGS-UHFFFAOYSA-N Zinc dication Chemical compound [Zn+2] PTFCDOFLOPIGGS-UHFFFAOYSA-N 0.000 claims description 2
- 238000000137 annealing Methods 0.000 claims description 2
- 238000001035 drying Methods 0.000 claims description 2
- 239000000706 filtrate Substances 0.000 claims description 2
- 239000001054 red pigment Substances 0.000 claims description 2
- 239000001052 yellow pigment Substances 0.000 claims description 2
- 239000000243 solution Substances 0.000 description 16
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 6
- 238000000605 extraction Methods 0.000 description 5
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 5
- 229910052802 copper Inorganic materials 0.000 description 4
- 238000004140 cleaning Methods 0.000 description 3
- 229910052595 hematite Inorganic materials 0.000 description 3
- 239000011019 hematite Substances 0.000 description 3
- LIKBJVNGSGBSGK-UHFFFAOYSA-N iron(3+);oxygen(2-) Chemical compound [O-2].[O-2].[O-2].[Fe+3].[Fe+3] LIKBJVNGSGBSGK-UHFFFAOYSA-N 0.000 description 3
- 239000000203 mixture Substances 0.000 description 3
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 2
- UIIMBOGNXHQVGW-UHFFFAOYSA-M Sodium bicarbonate Chemical compound [Na+].OC([O-])=O UIIMBOGNXHQVGW-UHFFFAOYSA-M 0.000 description 2
- 238000004458 analytical method Methods 0.000 description 2
- 238000011049 filling Methods 0.000 description 2
- YALHCTUQSQRCSX-UHFFFAOYSA-N sulfane sulfuric acid Chemical compound S.OS(O)(=O)=O YALHCTUQSQRCSX-UHFFFAOYSA-N 0.000 description 2
- 238000005406 washing Methods 0.000 description 2
- BVKZGUZCCUSVTD-UHFFFAOYSA-L Carbonate Chemical compound [O-]C([O-])=O BVKZGUZCCUSVTD-UHFFFAOYSA-L 0.000 description 1
- CWYNVVGOOAEACU-UHFFFAOYSA-N Fe2+ Chemical class [Fe+2] CWYNVVGOOAEACU-UHFFFAOYSA-N 0.000 description 1
- 208000032400 Retinal pigmentation Diseases 0.000 description 1
- 229910004298 SiO 2 Inorganic materials 0.000 description 1
- NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 description 1
- 238000002441 X-ray diffraction Methods 0.000 description 1
- 238000010521 absorption reaction Methods 0.000 description 1
- PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 description 1
- 229910052787 antimony Inorganic materials 0.000 description 1
- WATWJIUSRGPENY-UHFFFAOYSA-N antimony atom Chemical compound [Sb] WATWJIUSRGPENY-UHFFFAOYSA-N 0.000 description 1
- 229910052785 arsenic Inorganic materials 0.000 description 1
- RQNWIZPPADIBDY-UHFFFAOYSA-N arsenic atom Chemical compound [As] RQNWIZPPADIBDY-UHFFFAOYSA-N 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 239000003638 chemical reducing agent Substances 0.000 description 1
- 238000004040 coloring Methods 0.000 description 1
- 238000011109 contamination Methods 0.000 description 1
- 239000013078 crystal Substances 0.000 description 1
- 238000001914 filtration Methods 0.000 description 1
- 229910052732 germanium Inorganic materials 0.000 description 1
- GNPVGFCGXDBREM-UHFFFAOYSA-N germanium atom Chemical compound [Ge] GNPVGFCGXDBREM-UHFFFAOYSA-N 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-M hydroxide Chemical compound [OH-] XLYOFNOQVPJJNP-UHFFFAOYSA-M 0.000 description 1
- 150000004679 hydroxides Chemical class 0.000 description 1
- SZVJSHCCFOBDDC-UHFFFAOYSA-N iron(II,III) oxide Inorganic materials O=[Fe]O[Fe]O[Fe]=O SZVJSHCCFOBDDC-UHFFFAOYSA-N 0.000 description 1
- 238000007479 molecular analysis Methods 0.000 description 1
- 238000006386 neutralization reaction Methods 0.000 description 1
- 239000003921 oil Substances 0.000 description 1
- 238000004445 quantitative analysis Methods 0.000 description 1
- 239000012266 salt solution Substances 0.000 description 1
- 239000000377 silicon dioxide Substances 0.000 description 1
- 235000012239 silicon dioxide Nutrition 0.000 description 1
- 229910000030 sodium bicarbonate Inorganic materials 0.000 description 1
- 235000017557 sodium bicarbonate Nutrition 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 229910052717 sulfur Inorganic materials 0.000 description 1
- 239000011593 sulfur Substances 0.000 description 1
- 150000003467 sulfuric acid derivatives Chemical class 0.000 description 1
- 230000001131 transforming effect Effects 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09C—TREATMENT OF INORGANIC MATERIALS, OTHER THAN FIBROUS FILLERS, TO ENHANCE THEIR PIGMENTING OR FILLING PROPERTIES ; PREPARATION OF CARBON BLACK ; PREPARATION OF INORGANIC MATERIALS WHICH ARE NO SINGLE CHEMICAL COMPOUNDS AND WHICH ARE MAINLY USED AS PIGMENTS OR FILLERS
- C09C1/00—Treatment of specific inorganic materials other than fibrous fillers; Preparation of carbon black
- C09C1/22—Compounds of iron
- C09C1/24—Oxides of iron
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
- C01G49/00—Compounds of iron
- C01G49/02—Oxides; Hydroxides
- C01G49/06—Ferric oxide [Fe2O3]
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
- C01G49/00—Compounds of iron
- C01G49/02—Oxides; Hydroxides
- C01G49/08—Ferroso-ferric oxide [Fe3O4]
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2006/00—Physical properties of inorganic compounds
- C01P2006/60—Optical properties, e.g. expressed in CIELAB-values
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2006/00—Physical properties of inorganic compounds
- C01P2006/80—Compositional purity
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Compounds Of Iron (AREA)
- Pigments, Carbon Blacks, Or Wood Stains (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| BE6043279 | 1971-05-03 |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| DE2220956A1 DE2220956A1 (de) | 1972-12-07 |
| DE2220956B2 DE2220956B2 (de) | 1979-01-04 |
| DE2220956C3 true DE2220956C3 (de) | 1979-09-20 |
Family
ID=3874356
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE2220956A Expired DE2220956C3 (de) | 1971-05-03 | 1972-04-28 | Verfahren zur Herstellung von Pigmenten auf Basis von Eisenoxiden |
Country Status (16)
| Country | Link |
|---|---|
| US (1) | US3867516A (enExample) |
| JP (1) | JPS5117157B1 (enExample) |
| AU (1) | AU459235B2 (enExample) |
| BE (1) | BE766665A (enExample) |
| CA (1) | CA966260A (enExample) |
| DE (1) | DE2220956C3 (enExample) |
| ES (1) | ES401837A1 (enExample) |
| FI (1) | FI57269C (enExample) |
| FR (1) | FR2135141B1 (enExample) |
| GB (1) | GB1387910A (enExample) |
| IE (1) | IE36243B1 (enExample) |
| IT (1) | IT952691B (enExample) |
| NL (1) | NL164252C (enExample) |
| NO (1) | NO131843C (enExample) |
| ZA (1) | ZA722293B (enExample) |
| ZM (1) | ZM6872A1 (enExample) |
Families Citing this family (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS5328158B2 (enExample) * | 1974-02-22 | 1978-08-12 | ||
| US3919404A (en) * | 1974-06-28 | 1975-11-11 | Dow Chemical Co | Hydrothermal process for preparation of alpha iron oxide crystals |
| GB1509537A (en) * | 1974-09-13 | 1978-05-04 | Cominco Ltd | Treatment of zinc plant residues |
| DE2518283C3 (de) * | 1975-04-24 | 1979-02-15 | Bayer Ag, 5090 Leverkusen | Verfahren zur Herstellung von Eisenoxidschwarzpigmenten |
| DE3326632A1 (de) * | 1983-07-23 | 1985-02-07 | Bayer Ag, 5090 Leverkusen | Neue eisenoxidgelbpigmente mit niedrigem silking-effekt sowie deren herstellung |
| DE3500470A1 (de) * | 1985-01-09 | 1986-07-10 | Bayer Ag, 5090 Leverkusen | Verfahren zur herstellung heller farbreiner eisenoxidrotpigmente |
| DE3821341A1 (de) * | 1988-06-24 | 1989-12-28 | Bayer Ag | Neue hitzestabile eisenoxidschwarz-pigmente, verfahren zu ihrer herstellung sowie deren verwendung |
| DE4434969A1 (de) * | 1994-09-30 | 1996-04-04 | Bayer Ag | Hochtransparente, gelbe Eisenoxidpigmente, Verfahren zu ihrer Herstellung sowie deren Verwendung |
| CN102604434B (zh) * | 2012-02-21 | 2013-11-06 | 升华集团德清华源颜料有限公司 | 耐中温包覆型氧化铁黑的制备方法 |
Family Cites Families (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2754174A (en) * | 1956-07-10 | Treatment of salt solutions to | ||
| CA387570A (en) * | 1940-03-19 | W. Ayers Joseph | Hydrated iron compound and zinc sulphide | |
| US691324A (en) * | 1900-09-10 | 1902-01-14 | Elmer A Sperry | Pigment and the production thereof from ferrous liquors. |
| US1964683A (en) * | 1932-07-12 | 1934-06-26 | C K Williams & Company | Pigment |
| US2255607A (en) * | 1937-07-22 | 1941-09-09 | C K Williams & Co | Production of synthetic hydrated iron oxides |
| US2620261A (en) * | 1947-04-30 | 1952-12-02 | C K Williams & Co | Method of making iron oxide pigment |
| US2696426A (en) * | 1951-05-04 | 1954-12-07 | American Cyanamid Co | Process for the preparation of iron oxide pigments |
| US2904402A (en) * | 1955-12-30 | 1959-09-15 | Northern Pigment Company Ltd | Method of forming uniform uncontaminated iron oxide for pigment and other uses |
| BE673023A (enExample) * | 1965-04-30 | 1900-01-01 | ||
| US3549321A (en) * | 1968-04-25 | 1970-12-22 | Union Carbide Canada Ltd | Removal of iron from solution |
| US3687828A (en) * | 1970-06-25 | 1972-08-29 | American Zinc Co | Recovery of metal values |
-
1971
- 1971-05-03 BE BE766665A patent/BE766665A/xx unknown
-
1972
- 1972-03-28 FR FR7210807A patent/FR2135141B1/fr not_active Expired
- 1972-03-30 IE IE419/72A patent/IE36243B1/xx unknown
- 1972-04-04 CA CA138,878A patent/CA966260A/en not_active Expired
- 1972-04-05 ZA ZA722293A patent/ZA722293B/xx unknown
- 1972-04-10 AU AU40968/72A patent/AU459235B2/en not_active Expired
- 1972-04-10 US US242773A patent/US3867516A/en not_active Expired - Lifetime
- 1972-04-11 GB GB1667872A patent/GB1387910A/en not_active Expired
- 1972-04-12 ZM ZM68/72*UA patent/ZM6872A1/xx unknown
- 1972-04-17 IT IT49682/72A patent/IT952691B/it active
- 1972-04-17 ES ES401837A patent/ES401837A1/es not_active Expired
- 1972-04-18 NO NO1341/72A patent/NO131843C/no unknown
- 1972-04-24 JP JP47041175A patent/JPS5117157B1/ja active Pending
- 1972-04-28 FI FI1224/72A patent/FI57269C/fi active
- 1972-04-28 DE DE2220956A patent/DE2220956C3/de not_active Expired
- 1972-05-02 NL NL7205890.A patent/NL164252C/xx not_active IP Right Cessation
Also Published As
| Publication number | Publication date |
|---|---|
| CA966260A (en) | 1975-04-22 |
| AU4096872A (en) | 1973-10-18 |
| DE2220956A1 (de) | 1972-12-07 |
| ES401837A1 (es) | 1975-03-01 |
| FR2135141A1 (enExample) | 1972-12-15 |
| NL164252C (nl) | 1980-12-15 |
| AU459235B2 (en) | 1975-03-05 |
| IT952691B (it) | 1973-07-30 |
| NL164252B (nl) | 1980-07-15 |
| BE766665A (fr) | 1971-10-01 |
| ZA722293B (en) | 1972-12-27 |
| NO131843C (enExample) | 1975-08-13 |
| NL7205890A (enExample) | 1972-11-07 |
| FI57269C (fi) | 1980-07-10 |
| US3867516A (en) | 1975-02-18 |
| JPS5117157B1 (enExample) | 1976-05-31 |
| FR2135141B1 (enExample) | 1974-12-13 |
| FI57269B (fi) | 1980-03-31 |
| DE2220956B2 (de) | 1979-01-04 |
| IE36243B1 (en) | 1976-09-15 |
| GB1387910A (en) | 1975-03-19 |
| ZM6872A1 (en) | 1973-02-21 |
| NO131843B (enExample) | 1975-05-05 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C3 | Grant after two publication steps (3rd publication) | ||
| 8339 | Ceased/non-payment of the annual fee |