DE2133796C3 - Stabile, konzentrierte, wäßrige Lösungen von basischen Oxazinfarbstoffen, ihre Herstellung und Verwendung - Google Patents
Stabile, konzentrierte, wäßrige Lösungen von basischen Oxazinfarbstoffen, ihre Herstellung und VerwendungInfo
- Publication number
- DE2133796C3 DE2133796C3 DE19712133796 DE2133796A DE2133796C3 DE 2133796 C3 DE2133796 C3 DE 2133796C3 DE 19712133796 DE19712133796 DE 19712133796 DE 2133796 A DE2133796 A DE 2133796A DE 2133796 C3 DE2133796 C3 DE 2133796C3
- Authority
- DE
- Germany
- Prior art keywords
- solutions
- dyes
- urea
- oxazine dyes
- basic oxazine
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 239000000975 dye Substances 0.000 title claims description 30
- BCHZICNRHXRCHY-UHFFFAOYSA-N 2h-oxazine Chemical compound N1OC=CC=C1 BCHZICNRHXRCHY-UHFFFAOYSA-N 0.000 title claims description 13
- 239000007864 aqueous solution Substances 0.000 title claims description 5
- 238000002360 preparation method Methods 0.000 title claims description 5
- 239000000243 solution Substances 0.000 claims description 17
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 10
- XSQUKJJJFZCRTK-UHFFFAOYSA-N Urea Chemical compound NC(N)=O XSQUKJJJFZCRTK-UHFFFAOYSA-N 0.000 claims description 7
- 239000004202 carbamide Substances 0.000 claims description 7
- 150000007933 aliphatic carboxylic acids Chemical class 0.000 claims description 5
- 150000003839 salts Chemical class 0.000 claims description 5
- 230000002378 acidificating effect Effects 0.000 claims description 3
- 150000001735 carboxylic acids Chemical class 0.000 claims description 3
- 239000000203 mixture Substances 0.000 claims description 3
- 239000003795 chemical substances by application Substances 0.000 claims description 2
- 238000004043 dyeing Methods 0.000 claims description 2
- 229920000642 polymer Polymers 0.000 claims description 2
- 239000000080 wetting agent Substances 0.000 claims description 2
- 238000000034 method Methods 0.000 claims 2
- 125000001931 aliphatic group Chemical group 0.000 claims 1
- 239000002518 antifoaming agent Substances 0.000 claims 1
- 239000002657 fibrous material Substances 0.000 claims 1
- 230000000855 fungicidal effect Effects 0.000 claims 1
- 239000000417 fungicide Substances 0.000 claims 1
- 238000010186 staining Methods 0.000 claims 1
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 description 6
- 239000000843 powder Substances 0.000 description 3
- 235000011054 acetic acid Nutrition 0.000 description 2
- 125000003118 aryl group Chemical group 0.000 description 2
- 125000002091 cationic group Chemical group 0.000 description 2
- 238000010790 dilution Methods 0.000 description 2
- 239000012895 dilution Substances 0.000 description 2
- XBDQKXXYIPTUBI-UHFFFAOYSA-N dimethylselenoniopropionate Natural products CCC(O)=O XBDQKXXYIPTUBI-UHFFFAOYSA-N 0.000 description 2
- JVTAAEKCZFNVCJ-UHFFFAOYSA-N lactic acid Chemical compound CC(O)C(O)=O JVTAAEKCZFNVCJ-UHFFFAOYSA-N 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- BDAGIHXWWSANSR-UHFFFAOYSA-N methanoic acid Natural products OC=O BDAGIHXWWSANSR-UHFFFAOYSA-N 0.000 description 2
- UHOVQNZJYSORNB-UHFFFAOYSA-N monobenzene Natural products C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 description 2
- 238000003860 storage Methods 0.000 description 2
- SMZOUWXMTYCWNB-UHFFFAOYSA-N 2-(2-methoxy-5-methylphenyl)ethanamine Chemical compound COC1=CC=C(C)C=C1CCN SMZOUWXMTYCWNB-UHFFFAOYSA-N 0.000 description 1
- NIXOWILDQLNWCW-UHFFFAOYSA-N 2-Propenoic acid Natural products OC(=O)C=C NIXOWILDQLNWCW-UHFFFAOYSA-N 0.000 description 1
- FCYVWWWTHPPJII-UHFFFAOYSA-N 2-methylidenepropanedinitrile Chemical compound N#CC(=C)C#N FCYVWWWTHPPJII-UHFFFAOYSA-N 0.000 description 1
- OSWFIVFLDKOXQC-UHFFFAOYSA-N 4-(3-methoxyphenyl)aniline Chemical compound COC1=CC=CC(C=2C=CC(N)=CC=2)=C1 OSWFIVFLDKOXQC-UHFFFAOYSA-N 0.000 description 1
- 239000004952 Polyamide Substances 0.000 description 1
- OFOBLEOULBTSOW-UHFFFAOYSA-N Propanedioic acid Natural products OC(=O)CC(O)=O OFOBLEOULBTSOW-UHFFFAOYSA-N 0.000 description 1
- 125000003277 amino group Chemical group 0.000 description 1
- 150000001450 anions Chemical group 0.000 description 1
- 125000003710 aryl alkyl group Chemical group 0.000 description 1
- 150000005840 aryl radicals Chemical class 0.000 description 1
- 150000001555 benzenes Chemical class 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 150000003841 chloride salts Chemical class 0.000 description 1
- 238000004040 coloring Methods 0.000 description 1
- 229920001577 copolymer Polymers 0.000 description 1
- 150000001991 dicarboxylic acids Chemical class 0.000 description 1
- 239000000428 dust Substances 0.000 description 1
- 238000010410 dusting Methods 0.000 description 1
- 239000000835 fiber Substances 0.000 description 1
- 238000005187 foaming Methods 0.000 description 1
- 235000019253 formic acid Nutrition 0.000 description 1
- 230000008014 freezing Effects 0.000 description 1
- 238000007710 freezing Methods 0.000 description 1
- 239000001257 hydrogen Substances 0.000 description 1
- 229910052739 hydrogen Inorganic materials 0.000 description 1
- 125000004435 hydrogen atom Chemical class [H]* 0.000 description 1
- 239000004310 lactic acid Substances 0.000 description 1
- 235000014655 lactic acid Nutrition 0.000 description 1
- 239000010985 leather Substances 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- VZCYOOQTPOCHFL-UPHRSURJSA-N maleic acid Chemical compound OC(=O)\C=C/C(O)=O VZCYOOQTPOCHFL-UPHRSURJSA-N 0.000 description 1
- 239000011976 maleic acid Substances 0.000 description 1
- 150000005451 methyl sulfates Chemical class 0.000 description 1
- 150000002763 monocarboxylic acids Chemical class 0.000 description 1
- 125000001624 naphthyl group Chemical class 0.000 description 1
- 229910052757 nitrogen Inorganic materials 0.000 description 1
- 125000004433 nitrogen atom Chemical group N* 0.000 description 1
- 239000003960 organic solvent Substances 0.000 description 1
- 229920002239 polyacrylonitrile Polymers 0.000 description 1
- 229920002647 polyamide Polymers 0.000 description 1
- 229920000728 polyester Polymers 0.000 description 1
- 229920005594 polymer fiber Polymers 0.000 description 1
- 230000002035 prolonged effect Effects 0.000 description 1
- 235000019260 propionic acid Nutrition 0.000 description 1
- IUVKMZGDUIUOCP-BTNSXGMBSA-N quinbolone Chemical compound O([C@H]1CC[C@H]2[C@H]3[C@@H]([C@]4(C=CC(=O)C=C4CC3)C)CC[C@@]21C)C1=CCCC1 IUVKMZGDUIUOCP-BTNSXGMBSA-N 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
- 125000000547 substituted alkyl group Chemical group 0.000 description 1
- 150000003467 sulfuric acid derivatives Chemical class 0.000 description 1
- 239000004753 textile Substances 0.000 description 1
- VZCYOOQTPOCHFL-UHFFFAOYSA-N trans-butenedioic acid Natural products OC(=O)C=CC(O)=O VZCYOOQTPOCHFL-UHFFFAOYSA-N 0.000 description 1
- 238000005303 weighing Methods 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
- C09B67/00—Influencing the physical, e.g. the dyeing or printing properties of dyestuffs without chemical reactions, e.g. by treating with solvents grinding or grinding assistants, coating of pigments or dyes; Process features in the making of dyestuff preparations; Dyestuff preparations of a special physical nature, e.g. tablets, films
- C09B67/0071—Process features in the making of dyestuff preparations; Dehydrating agents; Dispersing agents; Dustfree compositions
- C09B67/0075—Preparations with cationic dyes
- C09B67/0076—Preparations of cationic or basic dyes in liquid form
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Chemistry (AREA)
- Coloring (AREA)
Priority Applications (4)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE19712133796 DE2133796C3 (de) | 1971-07-07 | 1971-07-07 | Stabile, konzentrierte, wäßrige Lösungen von basischen Oxazinfarbstoffen, ihre Herstellung und Verwendung |
| GB3026472A GB1367812A (en) | 1971-07-07 | 1972-06-28 | Stable concentrated aqueous solutions of basic oxazine dyestuffs their preparation and use |
| CH1003672A CH538531A (de) | 1971-07-07 | 1972-07-04 | Verfahren zur Herstellung stabiler, konzentrierter, wässriger Lösungen von basischen Oxazinfarbstoffen |
| FR7224645A FR2144866B1 (enExample) | 1971-07-07 | 1972-07-07 |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE19712133796 DE2133796C3 (de) | 1971-07-07 | 1971-07-07 | Stabile, konzentrierte, wäßrige Lösungen von basischen Oxazinfarbstoffen, ihre Herstellung und Verwendung |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| DE2133796A1 DE2133796A1 (de) | 1973-02-01 |
| DE2133796B2 DE2133796B2 (de) | 1979-04-05 |
| DE2133796C3 true DE2133796C3 (de) | 1979-11-22 |
Family
ID=5812937
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE19712133796 Expired DE2133796C3 (de) | 1971-07-07 | 1971-07-07 | Stabile, konzentrierte, wäßrige Lösungen von basischen Oxazinfarbstoffen, ihre Herstellung und Verwendung |
Country Status (4)
| Country | Link |
|---|---|
| CH (1) | CH538531A (enExample) |
| DE (1) | DE2133796C3 (enExample) |
| FR (1) | FR2144866B1 (enExample) |
| GB (1) | GB1367812A (enExample) |
Families Citing this family (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB1551529A (en) * | 1977-05-10 | 1979-08-30 | Ici Ltd | Basic dyestuff liquid formulations |
| DE2843559A1 (de) * | 1977-10-21 | 1979-04-26 | Ici Ltd | Loesung eines basischen farbstoffs in einem waessrigen loesungsmittelmedium |
-
1971
- 1971-07-07 DE DE19712133796 patent/DE2133796C3/de not_active Expired
-
1972
- 1972-06-28 GB GB3026472A patent/GB1367812A/en not_active Expired
- 1972-07-04 CH CH1003672A patent/CH538531A/de not_active IP Right Cessation
- 1972-07-07 FR FR7224645A patent/FR2144866B1/fr not_active Expired
Also Published As
| Publication number | Publication date |
|---|---|
| DE2133796B2 (de) | 1979-04-05 |
| DE2133796A1 (de) | 1973-02-01 |
| GB1367812A (en) | 1974-09-25 |
| FR2144866A1 (enExample) | 1973-02-16 |
| CH538531A (de) | 1973-06-30 |
| FR2144866B1 (enExample) | 1977-01-14 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| OD | Request for examination | ||
| C3 | Grant after two publication steps (3rd publication) | ||
| 8339 | Ceased/non-payment of the annual fee |