DE2133349C3 - Hochdruckreaktor zur Herstellung von Propionsäure - Google Patents
Hochdruckreaktor zur Herstellung von PropionsäureInfo
- Publication number
- DE2133349C3 DE2133349C3 DE2133349A DE2133349A DE2133349C3 DE 2133349 C3 DE2133349 C3 DE 2133349C3 DE 2133349 A DE2133349 A DE 2133349A DE 2133349 A DE2133349 A DE 2133349A DE 2133349 C3 DE2133349 C3 DE 2133349C3
- Authority
- DE
- Germany
- Prior art keywords
- pipe
- propionic acid
- reactor
- lined
- silver
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- XBDQKXXYIPTUBI-UHFFFAOYSA-N dimethylselenoniopropionate Natural products CCC(O)=O XBDQKXXYIPTUBI-UHFFFAOYSA-N 0.000 title claims description 26
- 235000019260 propionic acid Nutrition 0.000 title claims description 13
- IUVKMZGDUIUOCP-BTNSXGMBSA-N quinbolone Chemical compound O([C@H]1CC[C@H]2[C@H]3[C@@H]([C@]4(C=CC(=O)C=C4CC3)C)CC[C@@]21C)C1=CCCC1 IUVKMZGDUIUOCP-BTNSXGMBSA-N 0.000 title claims description 13
- 238000004519 manufacturing process Methods 0.000 title claims description 8
- BQCADISMDOOEFD-UHFFFAOYSA-N Silver Chemical compound [Ag] BQCADISMDOOEFD-UHFFFAOYSA-N 0.000 claims description 18
- VGGSQFUCUMXWEO-UHFFFAOYSA-N Ethene Chemical compound C=C VGGSQFUCUMXWEO-UHFFFAOYSA-N 0.000 claims description 16
- 239000005977 Ethylene Substances 0.000 claims description 16
- PXHVJJICTQNCMI-UHFFFAOYSA-N nickel Substances [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 claims description 13
- UGFAIRIUMAVXCW-UHFFFAOYSA-N Carbon monoxide Chemical compound [O+]#[C-] UGFAIRIUMAVXCW-UHFFFAOYSA-N 0.000 claims description 12
- 229910002091 carbon monoxide Inorganic materials 0.000 claims description 12
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 12
- 229910052759 nickel Inorganic materials 0.000 claims description 11
- 239000011541 reaction mixture Substances 0.000 claims description 6
- 229910052709 silver Inorganic materials 0.000 claims description 6
- 239000004332 silver Substances 0.000 claims description 6
- VUZPPFZMUPKLLV-UHFFFAOYSA-N methane;hydrate Chemical compound C.O VUZPPFZMUPKLLV-UHFFFAOYSA-N 0.000 claims description 5
- 229910000831 Steel Inorganic materials 0.000 claims description 4
- 239000000376 reactant Substances 0.000 claims description 4
- 239000010959 steel Substances 0.000 claims description 4
- 239000007788 liquid Substances 0.000 claims description 3
- OGSYQYXYGXIQFH-UHFFFAOYSA-N chromium molybdenum nickel Chemical compound [Cr].[Ni].[Mo] OGSYQYXYGXIQFH-UHFFFAOYSA-N 0.000 claims description 2
- 238000005260 corrosion Methods 0.000 description 7
- 230000007797 corrosion Effects 0.000 description 7
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 description 6
- 239000007791 liquid phase Substances 0.000 description 4
- OTMSDBZUPAUEDD-UHFFFAOYSA-N Ethane Chemical compound CC OTMSDBZUPAUEDD-UHFFFAOYSA-N 0.000 description 3
- 239000001569 carbon dioxide Substances 0.000 description 3
- 229910002092 carbon dioxide Inorganic materials 0.000 description 3
- NAVSKFYJNZQECG-UHFFFAOYSA-N nickel;propanoic acid Chemical compound [Ni].CCC(O)=O NAVSKFYJNZQECG-UHFFFAOYSA-N 0.000 description 3
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 2
- 239000006227 byproduct Substances 0.000 description 2
- 229940117927 ethylene oxide Drugs 0.000 description 2
- 239000007789 gas Substances 0.000 description 2
- 229910052751 metal Inorganic materials 0.000 description 2
- 239000002184 metal Substances 0.000 description 2
- 238000000034 method Methods 0.000 description 2
- 230000008439 repair process Effects 0.000 description 2
- 230000009286 beneficial effect Effects 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- 235000014113 dietary fatty acids Nutrition 0.000 description 1
- 230000003628 erosive effect Effects 0.000 description 1
- 229930195729 fatty acid Natural products 0.000 description 1
- 239000000194 fatty acid Substances 0.000 description 1
- -1 fatty acid nickel salts Chemical class 0.000 description 1
- 238000004508 fractional distillation Methods 0.000 description 1
- 239000008246 gaseous mixture Substances 0.000 description 1
- 238000011065 in-situ storage Methods 0.000 description 1
- 239000011261 inert gas Substances 0.000 description 1
- 238000012423 maintenance Methods 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 150000002815 nickel Chemical class 0.000 description 1
- 229910052757 nitrogen Inorganic materials 0.000 description 1
- 239000012071 phase Substances 0.000 description 1
- 150000003151 propanoic acid esters Chemical class 0.000 description 1
- 239000012429 reaction media Substances 0.000 description 1
- 229910001220 stainless steel Inorganic materials 0.000 description 1
- 239000010935 stainless steel Substances 0.000 description 1
- 239000007858 starting material Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
- C07C51/10—Preparation of carboxylic acids or their salts, halides or anhydrides by reaction with carbon monoxide
- C07C51/14—Preparation of carboxylic acids or their salts, halides or anhydrides by reaction with carbon monoxide on a carbon-to-carbon unsaturated bond in organic compounds
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
- C07C51/42—Separation; Purification; Stabilisation; Use of additives
- C07C51/487—Separation; Purification; Stabilisation; Use of additives by treatment giving rise to chemical modification
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Engineering & Computer Science (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- General Chemical & Material Sciences (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Priority Applications (17)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| BE785854D BE785854A (fr) | 1971-07-05 | Procede de preparation de l'acide propionique | |
| DE2133349A DE2133349C3 (de) | 1971-07-05 | 1971-07-05 | Hochdruckreaktor zur Herstellung von Propionsäure |
| FI1719/72A FI56668C (fi) | 1971-07-05 | 1972-06-15 | Vid framstaellning av propionsyra anvaendbar vertikal hoegtreaktor |
| NO2214/72A NO137781C (no) | 1971-07-05 | 1972-06-21 | Fremgangsmaate til fremstilling av propionsyre ved omsetning av etylen med karbonmonoksyd og vann |
| IT51070/72A IT958482B (it) | 1971-07-05 | 1972-06-22 | Procedimento per la produzione di acido propionico |
| US00266262A US3835185A (en) | 1971-07-05 | 1972-06-26 | Production of propionic acid |
| CA145,856A CA980793A (en) | 1971-07-05 | 1972-06-27 | Process for the production of propionic acid |
| FR7223823A FR2144708B1 (Direct) | 1971-07-05 | 1972-06-30 | |
| NL7209202A NL7209202A (Direct) | 1971-07-05 | 1972-06-30 | |
| DD164137A DD97413A5 (Direct) | 1971-07-05 | 1972-07-03 | |
| DK331472A DK133334C (da) | 1971-07-05 | 1972-07-04 | Fremgangsmade til fremstilling af propionsyre |
| GB3123472A GB1386883A (en) | 1971-07-05 | 1972-07-04 | Process for the production of propionic acid |
| PL1972156496A PL75746B1 (Direct) | 1971-07-05 | 1972-07-04 | |
| AT573572A AT316499B (de) | 1971-07-05 | 1972-07-04 | Verfahren zur Herstellung von Propionsäure |
| SE7208877A SE402909B (sv) | 1971-07-05 | 1972-07-05 | Cylindrisk hogtrycksreaktor for framstellning av propionsyra genom omsettning av eten med kolmonoxid och vatten |
| CS4767A CS177826B2 (Direct) | 1971-07-05 | 1972-07-05 | |
| SU762551552A SU673149A3 (en) | 1971-07-05 | 1976-10-21 | Reactor for obtaining propanoic acid |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE2133349A DE2133349C3 (de) | 1971-07-05 | 1971-07-05 | Hochdruckreaktor zur Herstellung von Propionsäure |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| DE2133349A1 DE2133349A1 (de) | 1973-01-25 |
| DE2133349B2 DE2133349B2 (de) | 1979-07-05 |
| DE2133349C3 true DE2133349C3 (de) | 1980-03-13 |
Family
ID=5812701
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE2133349A Expired DE2133349C3 (de) | 1971-07-05 | 1971-07-05 | Hochdruckreaktor zur Herstellung von Propionsäure |
Country Status (17)
| Country | Link |
|---|---|
| US (1) | US3835185A (Direct) |
| AT (1) | AT316499B (Direct) |
| BE (1) | BE785854A (Direct) |
| CA (1) | CA980793A (Direct) |
| CS (1) | CS177826B2 (Direct) |
| DD (1) | DD97413A5 (Direct) |
| DE (1) | DE2133349C3 (Direct) |
| DK (1) | DK133334C (Direct) |
| FI (1) | FI56668C (Direct) |
| FR (1) | FR2144708B1 (Direct) |
| GB (1) | GB1386883A (Direct) |
| IT (1) | IT958482B (Direct) |
| NL (1) | NL7209202A (Direct) |
| NO (1) | NO137781C (Direct) |
| PL (1) | PL75746B1 (Direct) |
| SE (1) | SE402909B (Direct) |
| SU (1) | SU673149A3 (Direct) |
Families Citing this family (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| RU2616623C1 (ru) * | 2016-06-21 | 2017-04-18 | ФЕДЕРАЛЬНОЕ ГОСУДАРСТВЕННОЕ БЮДЖЕТНОЕ УЧРЕЖДЕНИЕ НАУКИ ИНСТИТУТ ОРГАНИЧЕСКОЙ ХИМИИ им. Н.Д. ЗЕЛИНСКОГО РОССИЙСКОЙ АКАДЕМИИ НАУК (ИОХ РАН) | Двухстадийный способ получения пропионовой кислоты |
Family Cites Families (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CA582745A (en) * | 1959-09-08 | Koch Herbert | Catalytic process for the production of carboxylic acids from olefins and carbon monoxide | |
| US2748167A (en) * | 1952-11-05 | 1956-05-29 | Eastman Kodak Co | Process of producing oxygenated organic compounds |
-
0
- BE BE785854D patent/BE785854A/xx unknown
-
1971
- 1971-07-05 DE DE2133349A patent/DE2133349C3/de not_active Expired
-
1972
- 1972-06-15 FI FI1719/72A patent/FI56668C/fi active
- 1972-06-21 NO NO2214/72A patent/NO137781C/no unknown
- 1972-06-22 IT IT51070/72A patent/IT958482B/it active
- 1972-06-26 US US00266262A patent/US3835185A/en not_active Expired - Lifetime
- 1972-06-27 CA CA145,856A patent/CA980793A/en not_active Expired
- 1972-06-30 NL NL7209202A patent/NL7209202A/xx not_active Application Discontinuation
- 1972-06-30 FR FR7223823A patent/FR2144708B1/fr not_active Expired
- 1972-07-03 DD DD164137A patent/DD97413A5/xx unknown
- 1972-07-04 DK DK331472A patent/DK133334C/da not_active IP Right Cessation
- 1972-07-04 PL PL1972156496A patent/PL75746B1/pl unknown
- 1972-07-04 GB GB3123472A patent/GB1386883A/en not_active Expired
- 1972-07-04 AT AT573572A patent/AT316499B/de not_active IP Right Cessation
- 1972-07-05 SE SE7208877A patent/SE402909B/xx unknown
- 1972-07-05 CS CS4767A patent/CS177826B2/cs unknown
-
1976
- 1976-10-21 SU SU762551552A patent/SU673149A3/ru active
Also Published As
| Publication number | Publication date |
|---|---|
| CS177826B2 (Direct) | 1977-08-31 |
| IT958482B (it) | 1973-10-20 |
| FI56668C (fi) | 1980-03-10 |
| PL75746B1 (Direct) | 1974-12-31 |
| SE402909B (sv) | 1978-07-24 |
| DD97413A5 (Direct) | 1973-05-05 |
| DE2133349B2 (de) | 1979-07-05 |
| FR2144708A1 (Direct) | 1973-02-16 |
| FR2144708B1 (Direct) | 1976-08-06 |
| SU673149A3 (en) | 1979-07-05 |
| NO137781C (no) | 1978-04-26 |
| AT316499B (de) | 1974-07-10 |
| BE785854A (fr) | 1973-01-05 |
| DK133334C (da) | 1976-09-27 |
| NL7209202A (Direct) | 1973-01-09 |
| DK133334B (da) | 1976-05-03 |
| CA980793A (en) | 1975-12-30 |
| US3835185A (en) | 1974-09-10 |
| FI56668B (fi) | 1979-11-30 |
| DE2133349A1 (de) | 1973-01-25 |
| GB1386883A (en) | 1975-03-12 |
| NO137781B (no) | 1978-01-16 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C3 | Grant after two publication steps (3rd publication) | ||
| 8330 | Complete disclaimer |