DE2128956A1 - Beta-chlorpropionsaeure-fluoralkylester - Google Patents
Beta-chlorpropionsaeure-fluoralkylesterInfo
- Publication number
- DE2128956A1 DE2128956A1 DE19712128956 DE2128956A DE2128956A1 DE 2128956 A1 DE2128956 A1 DE 2128956A1 DE 19712128956 DE19712128956 DE 19712128956 DE 2128956 A DE2128956 A DE 2128956A DE 2128956 A1 DE2128956 A1 DE 2128956A1
- Authority
- DE
- Germany
- Prior art keywords
- weight
- parts
- chloropropionic acid
- mixtures
- hour
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 239000000203 mixture Substances 0.000 claims description 23
- 150000001298 alcohols Chemical class 0.000 claims description 9
- 238000000034 method Methods 0.000 claims description 6
- 150000001875 compounds Chemical class 0.000 claims description 4
- JEQDSBVHLKBEIZ-UHFFFAOYSA-N 2-chloropropanoyl chloride Chemical compound CC(Cl)C(Cl)=O JEQDSBVHLKBEIZ-UHFFFAOYSA-N 0.000 claims description 3
- 238000002360 preparation method Methods 0.000 claims description 2
- 239000000460 chlorine Substances 0.000 description 13
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 13
- ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 description 9
- 229910052801 chlorine Inorganic materials 0.000 description 9
- 238000006243 chemical reaction Methods 0.000 description 8
- 150000002148 esters Chemical class 0.000 description 8
- -1 ß-chloropropionic acid fluoroalkyl ester Chemical class 0.000 description 7
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 6
- 239000012071 phase Substances 0.000 description 5
- NGNBDVOYPDDBFK-UHFFFAOYSA-N 2-[2,4-di(pentan-2-yl)phenoxy]acetyl chloride Chemical compound CCCC(C)C1=CC=C(OCC(Cl)=O)C(C(C)CCC)=C1 NGNBDVOYPDDBFK-UHFFFAOYSA-N 0.000 description 4
- INUNLMUAPJVRME-UHFFFAOYSA-N 3-chloropropanoyl chloride Chemical compound ClCCC(Cl)=O INUNLMUAPJVRME-UHFFFAOYSA-N 0.000 description 4
- YCKRFDGAMUMZLT-UHFFFAOYSA-N Fluorine atom Chemical compound [F] YCKRFDGAMUMZLT-UHFFFAOYSA-N 0.000 description 4
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 4
- NIXOWILDQLNWCW-UHFFFAOYSA-N acrylic acid group Chemical group C(C=C)(=O)O NIXOWILDQLNWCW-UHFFFAOYSA-N 0.000 description 4
- 229910052731 fluorine Inorganic materials 0.000 description 4
- 239000011737 fluorine Substances 0.000 description 4
- IXCSERBJSXMMFS-UHFFFAOYSA-N hydrogen chloride Substances Cl.Cl IXCSERBJSXMMFS-UHFFFAOYSA-N 0.000 description 4
- 229910000041 hydrogen chloride Inorganic materials 0.000 description 4
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 3
- ZMANZCXQSJIPKH-UHFFFAOYSA-N Triethylamine Chemical compound CCN(CC)CC ZMANZCXQSJIPKH-UHFFFAOYSA-N 0.000 description 3
- 229910052757 nitrogen Inorganic materials 0.000 description 3
- SMZOUWXMTYCWNB-UHFFFAOYSA-N 2-(2-methoxy-5-methylphenyl)ethanamine Chemical compound COC1=CC=C(C)C=C1CCN SMZOUWXMTYCWNB-UHFFFAOYSA-N 0.000 description 2
- 150000001252 acrylic acid derivatives Chemical class 0.000 description 2
- 125000005396 acrylic acid ester group Chemical group 0.000 description 2
- 238000001816 cooling Methods 0.000 description 2
- 238000005886 esterification reaction Methods 0.000 description 2
- 239000007791 liquid phase Substances 0.000 description 2
- 229920000642 polymer Polymers 0.000 description 2
- 239000005871 repellent Substances 0.000 description 2
- 238000003756 stirring Methods 0.000 description 2
- 238000005809 transesterification reaction Methods 0.000 description 2
- GAWAYYRQGQZKCR-REOHCLBHSA-N (S)-2-chloropropanoic acid Chemical class C[C@H](Cl)C(O)=O GAWAYYRQGQZKCR-REOHCLBHSA-N 0.000 description 1
- PQUXFUBNSYCQAL-UHFFFAOYSA-N 1-(2,3-difluorophenyl)ethanone Chemical compound CC(=O)C1=CC=CC(F)=C1F PQUXFUBNSYCQAL-UHFFFAOYSA-N 0.000 description 1
- NIXOWILDQLNWCW-UHFFFAOYSA-M Acrylate Chemical compound [O-]C(=O)C=C NIXOWILDQLNWCW-UHFFFAOYSA-M 0.000 description 1
- 229940048053 acrylate Drugs 0.000 description 1
- HFBMWMNUJJDEQZ-UHFFFAOYSA-N acryloyl chloride Chemical compound ClC(=O)C=C HFBMWMNUJJDEQZ-UHFFFAOYSA-N 0.000 description 1
- 125000005250 alkyl acrylate group Chemical group 0.000 description 1
- 239000008346 aqueous phase Substances 0.000 description 1
- 238000009835 boiling Methods 0.000 description 1
- 239000007795 chemical reaction product Substances 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 238000000576 coating method Methods 0.000 description 1
- 238000004821 distillation Methods 0.000 description 1
- 230000032050 esterification Effects 0.000 description 1
- 238000007710 freezing Methods 0.000 description 1
- 230000008014 freezing Effects 0.000 description 1
- 239000007789 gas Substances 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 229920001519 homopolymer Polymers 0.000 description 1
- 239000011261 inert gas Substances 0.000 description 1
- 239000012442 inert solvent Substances 0.000 description 1
- 239000003112 inhibitor Substances 0.000 description 1
- 239000000543 intermediate Substances 0.000 description 1
- 150000002500 ions Chemical class 0.000 description 1
- 239000003960 organic solvent Substances 0.000 description 1
- 230000002940 repellent Effects 0.000 description 1
- 230000000630 rising effect Effects 0.000 description 1
- 238000000926 separation method Methods 0.000 description 1
- 229940047670 sodium acrylate Drugs 0.000 description 1
- 150000003510 tertiary aliphatic amines Chemical class 0.000 description 1
- 238000010626 work up procedure Methods 0.000 description 1
Landscapes
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Materials Applied To Surfaces To Minimize Adherence Of Mist Or Water (AREA)
Priority Applications (10)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE19712128956 DE2128956A1 (de) | 1971-06-11 | 1971-06-11 | Beta-chlorpropionsaeure-fluoralkylester |
| GB2632972A GB1336512A (en) | 1971-06-11 | 1972-06-06 | Beta-chloropropionic acid fluoroalkyl esters |
| NL7207657A NL7207657A (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html) | 1971-06-11 | 1972-06-06 | |
| CH847272A CH570963A5 (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html) | 1971-06-11 | 1972-06-07 | |
| SU1795551A SU447883A3 (ru) | 1971-06-11 | 1972-06-09 | Способ получения фторалкильных эфиров -хлорпропионовой кислоты |
| JP5698772A JPS5536653B1 (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html) | 1971-06-11 | 1972-06-09 | |
| AT498272A AT317862B (de) | 1971-06-11 | 1972-06-09 | Verfahren zur Herstellung neuer β-Chlorpropionsäurefluoralkylester |
| IT2550072A IT956426B (it) | 1971-06-11 | 1972-06-09 | Fluoroalchilesteri dell acido beta cloropropionico |
| FR7221042A FR2140675B1 (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html) | 1971-06-11 | 1972-06-12 | |
| BE784764A BE784764A (fr) | 1971-06-11 | 1972-06-12 | Beta-chloropropionates de fluoralkyles |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE19712128956 DE2128956A1 (de) | 1971-06-11 | 1971-06-11 | Beta-chlorpropionsaeure-fluoralkylester |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| DE2128956A1 true DE2128956A1 (de) | 1973-01-04 |
Family
ID=5810460
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE19712128956 Pending DE2128956A1 (de) | 1971-06-11 | 1971-06-11 | Beta-chlorpropionsaeure-fluoralkylester |
Country Status (10)
Families Citing this family (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP4653657B2 (ja) | 2003-05-23 | 2011-03-16 | 三井化学株式会社 | （メタ）アクリル酸エステル化合物およびその用途 |
-
1971
- 1971-06-11 DE DE19712128956 patent/DE2128956A1/de active Pending
-
1972
- 1972-06-06 GB GB2632972A patent/GB1336512A/en not_active Expired
- 1972-06-06 NL NL7207657A patent/NL7207657A/xx not_active Application Discontinuation
- 1972-06-07 CH CH847272A patent/CH570963A5/xx not_active IP Right Cessation
- 1972-06-09 IT IT2550072A patent/IT956426B/it active
- 1972-06-09 SU SU1795551A patent/SU447883A3/ru active
- 1972-06-09 AT AT498272A patent/AT317862B/de not_active IP Right Cessation
- 1972-06-09 JP JP5698772A patent/JPS5536653B1/ja active Pending
- 1972-06-12 BE BE784764A patent/BE784764A/xx unknown
- 1972-06-12 FR FR7221042A patent/FR2140675B1/fr not_active Expired
Also Published As
| Publication number | Publication date |
|---|---|
| NL7207657A (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html) | 1972-12-13 |
| JPS5536653B1 (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html) | 1980-09-22 |
| CH570963A5 (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html) | 1975-12-31 |
| IT956426B (it) | 1973-10-10 |
| BE784764A (fr) | 1972-12-12 |
| GB1336512A (en) | 1973-11-07 |
| AT317862B (de) | 1974-09-25 |
| FR2140675A1 (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html) | 1973-01-19 |
| SU447883A3 (ru) | 1974-10-25 |
| FR2140675B1 (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html) | 1977-12-23 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| OHW | Rejection |