DE2117650A1 - Difluorchlor- und Monofluordichlormethoxybenzoylfluoride - Google Patents
Difluorchlor- und MonofluordichlormethoxybenzoylfluorideInfo
- Publication number
- DE2117650A1 DE2117650A1 DE19712117650 DE2117650A DE2117650A1 DE 2117650 A1 DE2117650 A1 DE 2117650A1 DE 19712117650 DE19712117650 DE 19712117650 DE 2117650 A DE2117650 A DE 2117650A DE 2117650 A1 DE2117650 A1 DE 2117650A1
- Authority
- DE
- Germany
- Prior art keywords
- fluoride
- benzoyl
- chloride
- reaction
- hydrogen fluoride
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- -1 monofluorodichloromethoxybenzoyl fluorides Chemical class 0.000 title description 3
- KRHYYFGTRYWZRS-UHFFFAOYSA-N Fluorane Chemical compound F KRHYYFGTRYWZRS-UHFFFAOYSA-N 0.000 claims description 13
- 229910000040 hydrogen fluoride Inorganic materials 0.000 claims description 13
- 238000006243 chemical reaction Methods 0.000 claims description 10
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 claims description 8
- 150000001875 compounds Chemical class 0.000 claims description 5
- 239000000203 mixture Substances 0.000 claims description 4
- GSZSUDMISDEOIU-UHFFFAOYSA-N 2-(trichloromethoxy)benzoyl chloride Chemical compound ClC(=O)C1=CC=CC=C1OC(Cl)(Cl)Cl GSZSUDMISDEOIU-UHFFFAOYSA-N 0.000 claims description 3
- 238000002360 preparation method Methods 0.000 claims description 3
- 238000000034 method Methods 0.000 claims description 2
- PASDCCFISLVPSO-UHFFFAOYSA-N benzoyl chloride Chemical compound ClC(=O)C1=CC=CC=C1 PASDCCFISLVPSO-UHFFFAOYSA-N 0.000 claims 1
- PXHVJJICTQNCMI-UHFFFAOYSA-N Nickel Chemical compound [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 description 10
- 229910000041 hydrogen chloride Inorganic materials 0.000 description 7
- IXCSERBJSXMMFS-UHFFFAOYSA-N hydrogen chloride Substances Cl.Cl IXCSERBJSXMMFS-UHFFFAOYSA-N 0.000 description 7
- 239000007795 chemical reaction product Substances 0.000 description 6
- ZUGWMDCPYHCRQK-UHFFFAOYSA-N 3-(trichloromethoxy)benzoyl chloride Chemical compound ClC(=O)C1=CC=CC(OC(Cl)(Cl)Cl)=C1 ZUGWMDCPYHCRQK-UHFFFAOYSA-N 0.000 description 5
- 229910052759 nickel Inorganic materials 0.000 description 5
- 235000013877 carbamide Nutrition 0.000 description 3
- 150000003672 ureas Chemical class 0.000 description 3
- 238000010626 work up procedure Methods 0.000 description 3
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 2
- KRHYYFGTRYWZRS-UHFFFAOYSA-M Fluoride anion Chemical compound [F-] KRHYYFGTRYWZRS-UHFFFAOYSA-M 0.000 description 2
- 238000004587 chromatography analysis Methods 0.000 description 2
- 239000007789 gas Substances 0.000 description 2
- 239000007788 liquid Substances 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- 239000000463 material Substances 0.000 description 2
- 239000000376 reactant Substances 0.000 description 2
- ODNBVEIAQAZNNM-UHFFFAOYSA-N 1-(6-chloroimidazo[1,2-b]pyridazin-3-yl)ethanone Chemical compound C1=CC(Cl)=NN2C(C(=O)C)=CN=C21 ODNBVEIAQAZNNM-UHFFFAOYSA-N 0.000 description 1
- MZYJEGPJKMAHIT-UHFFFAOYSA-N 2-(trifluoromethoxy)benzoyl fluoride Chemical compound FC(=O)C1=CC=CC=C1OC(F)(F)F MZYJEGPJKMAHIT-UHFFFAOYSA-N 0.000 description 1
- LYJCNWQXQAONLO-UHFFFAOYSA-N 4-(trichloromethoxy)benzoyl chloride Chemical compound ClC(=O)C1=CC=C(OC(Cl)(Cl)Cl)C=C1 LYJCNWQXQAONLO-UHFFFAOYSA-N 0.000 description 1
- GUNJVIDCYZYFGV-UHFFFAOYSA-K Antimony trifluoride Inorganic materials F[Sb](F)F GUNJVIDCYZYFGV-UHFFFAOYSA-K 0.000 description 1
- BLTIBXDDPKDDKY-UHFFFAOYSA-N O=C(C(C=CC(F)=C1F)=C1OCCl)F Chemical class O=C(C(C=CC(F)=C1F)=C1OCCl)F BLTIBXDDPKDDKY-UHFFFAOYSA-N 0.000 description 1
- 229910000831 Steel Inorganic materials 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 150000007513 acids Chemical class 0.000 description 1
- 229910045601 alloy Inorganic materials 0.000 description 1
- 239000000956 alloy Substances 0.000 description 1
- 238000004458 analytical method Methods 0.000 description 1
- VMPVEPPRYRXYNP-UHFFFAOYSA-I antimony(5+);pentachloride Chemical compound Cl[Sb](Cl)(Cl)(Cl)Cl VMPVEPPRYRXYNP-UHFFFAOYSA-I 0.000 description 1
- 150000001540 azides Chemical class 0.000 description 1
- 230000015556 catabolic process Effects 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 239000000788 chromium alloy Substances 0.000 description 1
- 238000006731 degradation reaction Methods 0.000 description 1
- 230000008030 elimination Effects 0.000 description 1
- 238000003379 elimination reaction Methods 0.000 description 1
- 150000002222 fluorine compounds Chemical class 0.000 description 1
- 125000001153 fluoro group Chemical group F* 0.000 description 1
- 239000004009 herbicide Substances 0.000 description 1
- 239000012442 inert solvent Substances 0.000 description 1
- 239000012948 isocyanate Substances 0.000 description 1
- 150000002513 isocyanates Chemical class 0.000 description 1
- 229910052757 nitrogen Inorganic materials 0.000 description 1
- 239000000047 product Substances 0.000 description 1
- 230000008707 rearrangement Effects 0.000 description 1
- 229910001220 stainless steel Inorganic materials 0.000 description 1
- 239000010935 stainless steel Substances 0.000 description 1
- 229910001256 stainless steel alloy Inorganic materials 0.000 description 1
- 239000010959 steel Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C65/00—Compounds having carboxyl groups bound to carbon atoms of six—membered aromatic rings and containing any of the groups OH, O—metal, —CHO, keto, ether, groups, groups, or groups
- C07C65/32—Compounds having carboxyl groups bound to carbon atoms of six—membered aromatic rings and containing any of the groups OH, O—metal, —CHO, keto, ether, groups, groups, or groups containing keto groups
- C07C65/34—Compounds having carboxyl groups bound to carbon atoms of six—membered aromatic rings and containing any of the groups OH, O—metal, —CHO, keto, ether, groups, groups, or groups containing keto groups polycyclic
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
- C07C51/58—Preparation of carboxylic acid halides
- C07C51/60—Preparation of carboxylic acid halides by conversion of carboxylic acids or their anhydrides or esters, lactones, salts into halides with the same carboxylic acid part
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Priority Applications (4)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE19712117650 DE2117650A1 (de) | 1971-04-10 | 1971-04-10 | Difluorchlor- und Monofluordichlormethoxybenzoylfluoride |
| GB1610072A GB1327726A (en) | 1971-04-10 | 1972-04-07 | Difluorochloro-and monofluorodichloromethoxy-benzoyl fluorides and a process for their preparation |
| IT2295272A IT951275B (it) | 1971-04-10 | 1972-04-08 | Difluorocloro e monofluorodiclo rometossi benzoil fluorur |
| FR7212446A FR2132808B1 (enExample) | 1971-04-10 | 1972-04-10 |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE19712117650 DE2117650A1 (de) | 1971-04-10 | 1971-04-10 | Difluorchlor- und Monofluordichlormethoxybenzoylfluoride |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| DE2117650A1 true DE2117650A1 (de) | 1972-10-19 |
Family
ID=5804482
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE19712117650 Pending DE2117650A1 (de) | 1971-04-10 | 1971-04-10 | Difluorchlor- und Monofluordichlormethoxybenzoylfluoride |
Country Status (4)
| Country | Link |
|---|---|
| DE (1) | DE2117650A1 (enExample) |
| FR (1) | FR2132808B1 (enExample) |
| GB (1) | GB1327726A (enExample) |
| IT (1) | IT951275B (enExample) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4174349A (en) * | 1978-10-30 | 1979-11-13 | Allied Chemical Corporation | Preparation of fluoroorganic compounds with calcium fluoride |
| EP0071790A1 (de) * | 1981-08-01 | 1983-02-16 | BASF Aktiengesellschaft | Neue Fluormethylthiobenzoylfluoride und Verfahren zu ihrer Herstellung |
-
1971
- 1971-04-10 DE DE19712117650 patent/DE2117650A1/de active Pending
-
1972
- 1972-04-07 GB GB1610072A patent/GB1327726A/en not_active Expired
- 1972-04-08 IT IT2295272A patent/IT951275B/it active
- 1972-04-10 FR FR7212446A patent/FR2132808B1/fr not_active Expired
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4174349A (en) * | 1978-10-30 | 1979-11-13 | Allied Chemical Corporation | Preparation of fluoroorganic compounds with calcium fluoride |
| EP0071790A1 (de) * | 1981-08-01 | 1983-02-16 | BASF Aktiengesellschaft | Neue Fluormethylthiobenzoylfluoride und Verfahren zu ihrer Herstellung |
| US4590016A (en) * | 1981-08-01 | 1986-05-20 | Basf Aktiengesellschaft | Preparation of fluoromethylthiobenzoyl fluorides |
Also Published As
| Publication number | Publication date |
|---|---|
| FR2132808B1 (enExample) | 1978-01-20 |
| IT951275B (it) | 1973-06-30 |
| GB1327726A (en) | 1973-08-22 |
| FR2132808A1 (enExample) | 1972-11-24 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| DE1668842A1 (de) | Verfahren zur Herstellung von 1,1-Dichloraethan | |
| DE2117650A1 (de) | Difluorchlor- und Monofluordichlormethoxybenzoylfluoride | |
| CH633244A5 (de) | M-brom-benzotrifluoride. | |
| DE2418340A1 (de) | Verfahren zur herstellung von 3,5dichlorbenzoylchlorid | |
| EP0548682B1 (de) | Verfahren zur Herstellung von tertiären Phosphinen | |
| EP0136566A2 (de) | Verfahren zur Herstellung von 3,4-Dichlorbenzotrihalogeniden | |
| DE2644594A1 (de) | Fluorsubstitution in 1,1,1-trihalogenalkanen | |
| DE1518857C3 (enExample) | ||
| DE1928539A1 (de) | Hypochlorite und Verfahren zu ihrer Herstellung | |
| DE1108676B (de) | Verfahren zur Herstellung von 2-Brom-2-chlor-1, 1, 1-trifluoraethan | |
| DE2059597B2 (de) | Verfahren zur Herstellung von Carbonsäurechloriden ggf. chlorsubstituierter Carbonsäuren | |
| DE1069137B (de) | Verfahren zur Herstellung von Fluor und Chlor enthaltenden Essigsaurtechloriden | |
| DE2139964A1 (de) | Verfahren zur herstellung von pentafluoraethyljodid und heptafluorisopropyljodid | |
| DE575593C (de) | Verfahren zur Herstellung aromatischer, in der Seitenkette fluorierter Kohlenwasserstoffe | |
| DE1186844B (de) | Verfahren zur Herstellung von Trifluoracetylchlorid | |
| DE2336913A1 (de) | Perfluoralkyljodid-modifizierte monoallylaether | |
| DE972565C (de) | Verfahren zur Herstellung langkettiger Chlorkohlenwasserstoffe | |
| DE2013435A1 (de) | N1N Bis tnfluormethyl tetrafluor athylendiamin | |
| DE1932830C3 (de) | Verfahren zur Herstellung von N-Bis-chlorcarbonylaminen | |
| DE1670706A1 (de) | Verfahren zur Herstellung von 2-Chlorbenzthiazolen | |
| DE1418961C (de) | Verfahren zur Herstellung von Anlagerungsverbindungen aus Fluor enthaltenden Olefinen und Stickstoffmonoxid | |
| AT233551B (de) | Verfahren zur Herstellung chlorsubstituierter Methylisocyaniddichloride | |
| DE2013433C3 (de) | Verfahren zur Herstellung von Perfluor-23-diazahexa-2,4-dien | |
| DE1245349B (de) | Verfahren zur Herstellung von 2, 2-Dichlorbutan | |
| DE1245362B (de) | Verfahren zur Herstellung von Sorbinsaeurechlorid oder -bromid |