DE2062399A1 - Kontinuierliches Verfahren zur Herstellung von Polychlorcyclopentanen - Google Patents
Kontinuierliches Verfahren zur Herstellung von PolychlorcyclopentanenInfo
- Publication number
- DE2062399A1 DE2062399A1 DE19702062399 DE2062399A DE2062399A1 DE 2062399 A1 DE2062399 A1 DE 2062399A1 DE 19702062399 DE19702062399 DE 19702062399 DE 2062399 A DE2062399 A DE 2062399A DE 2062399 A1 DE2062399 A1 DE 2062399A1
- Authority
- DE
- Germany
- Prior art keywords
- polychlorocyclopentane
- chlorine
- cyclopentadiene
- chlorination
- diluent
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 238000004519 manufacturing process Methods 0.000 title claims description 10
- 238000010924 continuous production Methods 0.000 title claims description 8
- ZSWFCLXCOIISFI-UHFFFAOYSA-N cyclopentadiene Chemical compound C1C=CC=C1 ZSWFCLXCOIISFI-UHFFFAOYSA-N 0.000 claims description 50
- 239000000460 chlorine Substances 0.000 claims description 30
- ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 claims description 24
- 229910052801 chlorine Inorganic materials 0.000 claims description 24
- 238000000034 method Methods 0.000 claims description 16
- 239000003085 diluting agent Substances 0.000 claims description 11
- 239000007788 liquid Substances 0.000 claims description 7
- 238000004064 recycling Methods 0.000 claims description 2
- 125000001511 cyclopentyl group Chemical class [H]C1([H])C([H])([H])C([H])([H])C([H])(*)C1([H])[H] 0.000 claims 3
- 238000005660 chlorination reaction Methods 0.000 description 22
- 239000000047 product Substances 0.000 description 12
- ZFMWDTNZPKDVBU-UHFFFAOYSA-N 1,2,3,4-tetrachlorocyclopentane Chemical compound ClC1CC(Cl)C(Cl)C1Cl ZFMWDTNZPKDVBU-UHFFFAOYSA-N 0.000 description 10
- 239000000203 mixture Substances 0.000 description 10
- 238000006243 chemical reaction Methods 0.000 description 9
- RPUFWOAXMFQSDJ-UHFFFAOYSA-N 1,1,2,3,3,4-hexachlorocyclopentane Chemical compound ClC1CC(Cl)(Cl)C(Cl)C1(Cl)Cl RPUFWOAXMFQSDJ-UHFFFAOYSA-N 0.000 description 5
- RGSFGYAAUTVSQA-UHFFFAOYSA-N Cyclopentane Chemical compound C1CCCC1 RGSFGYAAUTVSQA-UHFFFAOYSA-N 0.000 description 4
- 238000001816 cooling Methods 0.000 description 4
- PXHVJJICTQNCMI-UHFFFAOYSA-N Nickel Chemical compound [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 description 3
- 230000015572 biosynthetic process Effects 0.000 description 3
- 150000001940 cyclopentanes Chemical class 0.000 description 3
- VUNCWTMEJYMOOR-UHFFFAOYSA-N hexachlorocyclopentadiene Chemical compound ClC1=C(Cl)C(Cl)(Cl)C(Cl)=C1Cl VUNCWTMEJYMOOR-UHFFFAOYSA-N 0.000 description 3
- 239000006227 byproduct Substances 0.000 description 2
- 239000007795 chemical reaction product Substances 0.000 description 2
- 125000001309 chloro group Chemical group Cl* 0.000 description 2
- 238000001704 evaporation Methods 0.000 description 2
- 230000008020 evaporation Effects 0.000 description 2
- 230000005484 gravity Effects 0.000 description 2
- DMEGYFMYUHOHGS-UHFFFAOYSA-N heptamethylene Natural products C1CCCCCC1 DMEGYFMYUHOHGS-UHFFFAOYSA-N 0.000 description 2
- 229930195733 hydrocarbon Natural products 0.000 description 2
- 229920000642 polymer Polymers 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- VZGDMQKNWNREIO-UHFFFAOYSA-N tetrachloromethane Chemical compound ClC(Cl)(Cl)Cl VZGDMQKNWNREIO-UHFFFAOYSA-N 0.000 description 2
- PMJHHCWVYXUKFD-SNAWJCMRSA-N (E)-1,3-pentadiene Chemical compound C\C=C\C=C PMJHHCWVYXUKFD-SNAWJCMRSA-N 0.000 description 1
- 239000004215 Carbon black (E152) Substances 0.000 description 1
- XDTMQSROBMDMFD-UHFFFAOYSA-N Cyclohexane Chemical compound C1CCCCC1 XDTMQSROBMDMFD-UHFFFAOYSA-N 0.000 description 1
- 208000036365 Normal labour Diseases 0.000 description 1
- -1 alicyclic hydrocarbons Chemical class 0.000 description 1
- 125000001931 aliphatic group Chemical group 0.000 description 1
- 229910000413 arsenic oxide Inorganic materials 0.000 description 1
- 229960002594 arsenic trioxide Drugs 0.000 description 1
- 239000003054 catalyst Substances 0.000 description 1
- 150000008280 chlorinated hydrocarbons Chemical class 0.000 description 1
- 238000010276 construction Methods 0.000 description 1
- 230000001276 controlling effect Effects 0.000 description 1
- 239000002826 coolant Substances 0.000 description 1
- KTTMEOWBIWLMSE-UHFFFAOYSA-N diarsenic trioxide Chemical compound O1[As](O2)O[As]3O[As]1O[As]2O3 KTTMEOWBIWLMSE-UHFFFAOYSA-N 0.000 description 1
- 238000009792 diffusion process Methods 0.000 description 1
- 239000000539 dimer Substances 0.000 description 1
- 238000006471 dimerization reaction Methods 0.000 description 1
- 238000004880 explosion Methods 0.000 description 1
- 239000011521 glass Substances 0.000 description 1
- 150000002430 hydrocarbons Chemical class 0.000 description 1
- 239000013067 intermediate product Substances 0.000 description 1
- QSHDDOUJBYECFT-UHFFFAOYSA-N mercury Chemical compound [Hg] QSHDDOUJBYECFT-UHFFFAOYSA-N 0.000 description 1
- 238000012544 monitoring process Methods 0.000 description 1
- 229910052759 nickel Inorganic materials 0.000 description 1
- SNICXCGAKADSCV-UHFFFAOYSA-N nicotine Chemical compound CN1CCCC1C1=CC=CN=C1 SNICXCGAKADSCV-UHFFFAOYSA-N 0.000 description 1
- 230000002093 peripheral effect Effects 0.000 description 1
- 239000011541 reaction mixture Substances 0.000 description 1
- 230000001105 regulatory effect Effects 0.000 description 1
- 238000010517 secondary reaction Methods 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
- JLYXXMFPNIAWKQ-UHFFFAOYSA-N γ Benzene hexachloride Chemical compound ClC1C(Cl)C(Cl)C(Cl)C(Cl)C1Cl JLYXXMFPNIAWKQ-UHFFFAOYSA-N 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C17/00—Preparation of halogenated hydrocarbons
- C07C17/013—Preparation of halogenated hydrocarbons by addition of halogens
- C07C17/06—Preparation of halogenated hydrocarbons by addition of halogens combined with replacement of hydrogen atoms by halogens
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Physical Or Chemical Processes And Apparatus (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US238770A | 1970-01-12 | 1970-01-12 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| DE2062399A1 true DE2062399A1 (de) | 1971-07-22 |
Family
ID=21700533
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE19702062399 Pending DE2062399A1 (de) | 1970-01-12 | 1970-12-18 | Kontinuierliches Verfahren zur Herstellung von Polychlorcyclopentanen |
Country Status (8)
| Country | Link |
|---|---|
| US (1) | US3637479A (enExample) |
| JP (1) | JPS5133105B1 (enExample) |
| BE (1) | BE759165A (enExample) |
| CA (1) | CA948155A (enExample) |
| DE (1) | DE2062399A1 (enExample) |
| FR (1) | FR2076033B1 (enExample) |
| GB (1) | GB1313559A (enExample) |
| NL (1) | NL7100387A (enExample) |
Families Citing this family (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3914167A (en) * | 1974-08-26 | 1975-10-21 | Dow Chemical Co | Process for making cis-1,3-dichloropropene |
| JPS552579U (enExample) * | 1979-04-27 | 1980-01-09 | ||
| JPS60145810U (ja) * | 1984-03-09 | 1985-09-27 | 進士 三郎 | 履物のすべり止め具 |
| CN105884569B (zh) * | 2016-04-22 | 2019-03-12 | 北京宇极科技发展有限公司 | 制备1,2-二氯六氟环戊烯的方法 |
| CN116675592A (zh) * | 2022-02-22 | 2023-09-01 | 王智轩 | 一种氯气氯化环戊烷生产高纯度氯代环戊烷的方法 |
Family Cites Families (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2509160A (en) * | 1945-12-22 | 1950-05-23 | Purdue Research Foundation | Making hexachlorocyclopentadiene |
| US2561209A (en) * | 1947-12-30 | 1951-07-17 | Standard Oil Dev Co | Hydrogenated dicyclopentadiene insecticide |
| NL248810A (enExample) * | 1959-03-27 | |||
| US3329731A (en) * | 1965-03-22 | 1967-07-04 | Phillips Petroleum Co | Production of pure cyclic hydrocarbons |
| US3494844A (en) * | 1967-02-09 | 1970-02-10 | Phillips Petroleum Co | Continuous photohalogenation of hydrocarbons |
-
0
- BE BE759165D patent/BE759165A/xx unknown
-
1970
- 1970-01-12 US US2387A patent/US3637479A/en not_active Expired - Lifetime
- 1970-10-27 GB GB5105070A patent/GB1313559A/en not_active Expired
- 1970-11-12 JP JP45099765A patent/JPS5133105B1/ja active Pending
- 1970-12-11 FR FR7044774A patent/FR2076033B1/fr not_active Expired
- 1970-12-18 DE DE19702062399 patent/DE2062399A1/de active Pending
- 1970-12-29 CA CA101,677A patent/CA948155A/en not_active Expired
-
1971
- 1971-01-12 NL NL7100387A patent/NL7100387A/xx unknown
Also Published As
| Publication number | Publication date |
|---|---|
| GB1313559A (en) | 1973-04-11 |
| US3637479A (en) | 1972-01-25 |
| JPS5133105B1 (enExample) | 1976-09-17 |
| BE759165A (fr) | 1971-05-19 |
| FR2076033B1 (enExample) | 1974-04-26 |
| NL7100387A (enExample) | 1971-07-14 |
| FR2076033A1 (enExample) | 1971-10-15 |
| CA948155A (en) | 1974-05-28 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| DE3445896C1 (de) | Verfahren zur kontinuierlichen Herstellung von 1.2-Dichlorethan | |
| DE2062399A1 (de) | Kontinuierliches Verfahren zur Herstellung von Polychlorcyclopentanen | |
| EP0133668B1 (de) | Verfahren zur Herstellung von Jononen | |
| DE2538158C3 (de) | Verfahren zur Herstellung von monochlorbenzoylchlorid | |
| DE69103290T2 (de) | Kontinuierliches Verfahren zur Herstellung von Tetraphosphorpolysulfiden. | |
| DE69902965T2 (de) | Verfahren zur kontinuierlichen Herstellung von Mono und/oder Bis(Mono-, und/oder Di-, und/oder Trichlormethyl)benzolen | |
| DE2614139B2 (de) | Verfahren zur ansatzweisen oder kontinuierlichen Herstellung von o, a, a, a', o ' a '-Hexachlorxylol | |
| DE2443179A1 (de) | Verfahren zur herstellung von perchlormethylbenzol | |
| DE2847104A1 (de) | Verfahren zur herstellung von 2,2-bis (4-hydroxyphenyl)-propan aus den destillationsnebenprodukten desselben | |
| DE2364093C3 (de) | Verfahren zur Umwandlung von Trichloräthylen, das in 1,2-Dichloräthan enthalten ist | |
| DE1520113A1 (de) | Verfahren zur Polymerisation von AEthylen | |
| DE69421145T2 (de) | Herstellung von festen Perfluoralkylbromiden | |
| DE2359500C2 (de) | Verfahren zur Herstellung von 2,2-Bis-(4-dihydroxyphenyl)-propan | |
| DE2341321C3 (de) | Verfahren zur Herstellung von Acetylchlorid | |
| DE2740585A1 (de) | Verfahren zur herstellung von 1,1-difluor-1-chloraethan | |
| EP0900763B1 (de) | Verfahren zur Herstellung von Zinntetrachlorid | |
| DE858398C (de) | Verfahren zur Herstellung von Dichlorpropylenen | |
| DE4338195A1 (de) | Verfahren zur Herstellung von hochchlorierten Paraffinen | |
| DE1960063A1 (de) | Verfahren zur Herstellung von Allylchlorid | |
| DE902733C (de) | Verfahren zur Herstellung von Alkylmonochloriden durch kontinuierliche Chlorierung von Kohlenwasserstoffen | |
| DE2332170A1 (de) | Verfahren fuer die chlorierung von c tief 8-c tief 16-kohlenwasserstoffen in fluessiger phase | |
| DE4235405A1 (de) | Verfahren zur Herstellung von sehr harten PE-Wachsoxidaten | |
| DE1618593C3 (de) | Verfahren zur Herstellung von 2,3-Dichlor-1,4-naphthochinonen | |
| DE2058520C3 (de) | Substituierte Trifluoräthylmethyläther, Verfahren zu deren Herstellung sowie diese enthaltende inhalationsanästhetische Zusammensetzungen | |
| AT228776B (de) | Verfahren zur Herstellung von Isotope enthaltenden aromatischen Kohlenwasserstoffen |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| OHN | Withdrawal |