DE2058663C3 - - Google Patents
Info
- Publication number
- DE2058663C3 DE2058663C3 DE19702058663 DE2058663A DE2058663C3 DE 2058663 C3 DE2058663 C3 DE 2058663C3 DE 19702058663 DE19702058663 DE 19702058663 DE 2058663 A DE2058663 A DE 2058663A DE 2058663 C3 DE2058663 C3 DE 2058663C3
- Authority
- DE
- Germany
- Prior art keywords
- phenolic resin
- foams
- phenolic
- foam
- liquid
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 239000006260 foam Substances 0.000 claims description 35
- ISWSIDIOOBJBQZ-UHFFFAOYSA-N phenol group Chemical group C1(=CC=CC=C1)O ISWSIDIOOBJBQZ-UHFFFAOYSA-N 0.000 claims description 27
- 239000005011 phenolic resin Substances 0.000 claims description 25
- 229920001568 phenolic resin Polymers 0.000 claims description 24
- 238000005336 cracking Methods 0.000 claims description 19
- 229920005989 resin Polymers 0.000 claims description 19
- 239000011347 resin Substances 0.000 claims description 19
- 239000000203 mixture Substances 0.000 claims description 18
- 239000007788 liquid Substances 0.000 claims description 16
- 150000002430 hydrocarbons Chemical class 0.000 claims description 15
- 239000002253 acid Substances 0.000 claims description 12
- 238000005187 foaming Methods 0.000 claims description 11
- 238000000034 method Methods 0.000 claims description 11
- 239000004848 polyfunctional curative Substances 0.000 claims description 9
- 229920003987 resole Polymers 0.000 claims description 9
- 150000007513 acids Chemical class 0.000 claims description 8
- 239000007787 solid Substances 0.000 claims description 7
- KGBXLFKZBHKPEV-UHFFFAOYSA-N Boric acid Chemical compound OB(O)O KGBXLFKZBHKPEV-UHFFFAOYSA-N 0.000 claims description 6
- 239000004327 boric acid Substances 0.000 claims description 6
- 238000004519 manufacturing process Methods 0.000 claims description 6
- 229910052799 carbon Inorganic materials 0.000 claims description 5
- 230000000694 effects Effects 0.000 claims description 4
- 230000002349 favourable Effects 0.000 claims description 4
- 239000004094 surface-active agent Substances 0.000 claims description 4
- 125000003118 aryl group Chemical group 0.000 claims description 3
- 230000015572 biosynthetic process Effects 0.000 claims description 3
- OKTJSMMVPCPJKN-UHFFFAOYSA-N carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims description 3
- 238000005755 formation reaction Methods 0.000 claims description 3
- 239000000463 material Substances 0.000 claims description 3
- 239000000126 substance Substances 0.000 claims description 3
- 239000000654 additive Substances 0.000 claims description 2
- 239000003063 flame retardant Substances 0.000 claims description 2
- 238000009413 insulation Methods 0.000 claims description 2
- 239000012188 paraffin wax Substances 0.000 claims description 2
- -1 paraffins Chemical class 0.000 claims description 2
- 239000004604 Blowing Agent Substances 0.000 claims 3
- 239000002641 tar oil Substances 0.000 claims 2
- 239000004215 Carbon black (E152) Substances 0.000 claims 1
- ZOXJGFHDIHLPTG-UHFFFAOYSA-N boron Chemical compound [B] ZOXJGFHDIHLPTG-UHFFFAOYSA-N 0.000 claims 1
- 229910052796 boron Inorganic materials 0.000 claims 1
- 150000001639 boron compounds Chemical class 0.000 claims 1
- 238000004939 coking Methods 0.000 claims 1
- 230000001771 impaired Effects 0.000 claims 1
- 229910052760 oxygen Inorganic materials 0.000 claims 1
- MYMOFIZGZYHOMD-UHFFFAOYSA-N oxygen Chemical compound O=O MYMOFIZGZYHOMD-UHFFFAOYSA-N 0.000 claims 1
- 239000001301 oxygen Substances 0.000 claims 1
- 239000000843 powder Substances 0.000 claims 1
- 229920003002 synthetic resin Polymers 0.000 claims 1
- 239000000057 synthetic resin Substances 0.000 claims 1
- 239000003380 propellant Substances 0.000 description 8
- JOXIMZWYDAKGHI-UHFFFAOYSA-N P-Toluenesulfonic acid Chemical compound CC1=CC=C(S(O)(=O)=O)C=C1 JOXIMZWYDAKGHI-UHFFFAOYSA-N 0.000 description 6
- WSFSSNUMVMOOMR-UHFFFAOYSA-N formaldehyde Chemical compound O=C WSFSSNUMVMOOMR-UHFFFAOYSA-N 0.000 description 5
- 238000009835 boiling Methods 0.000 description 4
- 150000001875 compounds Chemical class 0.000 description 4
- 238000002156 mixing Methods 0.000 description 4
- VEXZGXHMUGYJMC-UHFFFAOYSA-N HCl Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 3
- 239000000284 extract Substances 0.000 description 3
- 239000001257 hydrogen Substances 0.000 description 3
- 229910052739 hydrogen Inorganic materials 0.000 description 3
- 239000002480 mineral oil Substances 0.000 description 3
- 239000003921 oil Substances 0.000 description 3
- OFBQJSOFQDEBGM-UHFFFAOYSA-N pentane Chemical compound CCCCC OFBQJSOFQDEBGM-UHFFFAOYSA-N 0.000 description 3
- 150000002989 phenols Chemical class 0.000 description 3
- HEMHJVSKTPXQMS-UHFFFAOYSA-M sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 3
- 239000000243 solution Substances 0.000 description 3
- 150000001299 aldehydes Chemical class 0.000 description 2
- UHOVQNZJYSORNB-UHFFFAOYSA-N benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 description 2
- 239000004359 castor oil Substances 0.000 description 2
- 235000019438 castor oil Nutrition 0.000 description 2
- 238000009833 condensation Methods 0.000 description 2
- 230000005494 condensation Effects 0.000 description 2
- 238000002474 experimental method Methods 0.000 description 2
- 239000007789 gas Substances 0.000 description 2
- 150000002431 hydrogen Chemical class 0.000 description 2
- IJGRMHOSHXDMSA-UHFFFAOYSA-N nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 2
- 239000003960 organic solvent Substances 0.000 description 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 2
- FEPBITJSIHRMRT-UHFFFAOYSA-N 4-hydroxybenzenesulfonic acid Chemical compound OC1=CC=C(S(O)(=O)=O)C=C1 FEPBITJSIHRMRT-UHFFFAOYSA-N 0.000 description 1
- SRSXLGNVWSONIS-UHFFFAOYSA-N Benzenesulfonic acid Chemical compound OS(=O)(=O)C1=CC=CC=C1 SRSXLGNVWSONIS-UHFFFAOYSA-N 0.000 description 1
- BVKZGUZCCUSVTD-UHFFFAOYSA-M Bicarbonate Chemical class OC([O-])=O BVKZGUZCCUSVTD-UHFFFAOYSA-M 0.000 description 1
- XWCDCDSDNJVCLO-UHFFFAOYSA-N Chlorofluoromethane Chemical compound FCCl XWCDCDSDNJVCLO-UHFFFAOYSA-N 0.000 description 1
- FBPFZTCFMRRESA-FSIIMWSLSA-N D-Glucitol Natural products OC[C@H](O)[C@H](O)[C@@H](O)[C@H](O)CO FBPFZTCFMRRESA-FSIIMWSLSA-N 0.000 description 1
- FBPFZTCFMRRESA-JGWLITMVSA-N D-glucitol Chemical compound OC[C@H](O)[C@@H](O)[C@H](O)[C@H](O)CO FBPFZTCFMRRESA-JGWLITMVSA-N 0.000 description 1
- HYBBIBNJHNGZAN-UHFFFAOYSA-N Furfural Chemical compound O=CC1=CC=CO1 HYBBIBNJHNGZAN-UHFFFAOYSA-N 0.000 description 1
- 229920002456 HOTAIR Polymers 0.000 description 1
- VKYKSIONXSXAKP-UHFFFAOYSA-N Hexamethylenetetramine Chemical compound C1N(C2)CN3CN1CN2C3 VKYKSIONXSXAKP-UHFFFAOYSA-N 0.000 description 1
- 229960004011 Methenamine Drugs 0.000 description 1
- 239000005662 Paraffin oil Substances 0.000 description 1
- 239000004698 Polyethylene (PE) Substances 0.000 description 1
- KNNPTLFTAWALOI-UHFFFAOYSA-N acetaldehyde;formaldehyde Chemical compound O=C.CC=O KNNPTLFTAWALOI-UHFFFAOYSA-N 0.000 description 1
- 239000003513 alkali Substances 0.000 description 1
- 239000007864 aqueous solution Substances 0.000 description 1
- 239000002585 base Substances 0.000 description 1
- 229940092714 benzenesulfonic acid Drugs 0.000 description 1
- 238000004364 calculation method Methods 0.000 description 1
- CURLTUGMZLYLDI-UHFFFAOYSA-N carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 description 1
- 239000001569 carbon dioxide Substances 0.000 description 1
- 229910002092 carbon dioxide Inorganic materials 0.000 description 1
- 150000004649 carbonic acid derivatives Chemical class 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 230000000875 corresponding Effects 0.000 description 1
- 150000001896 cresols Chemical class 0.000 description 1
- 239000010727 cylinder oil Substances 0.000 description 1
- 229950008597 drug INN Drugs 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 150000002148 esters Chemical class 0.000 description 1
- 150000002170 ethers Chemical class 0.000 description 1
- 239000008098 formaldehyde solution Substances 0.000 description 1
- 238000009472 formulation Methods 0.000 description 1
- 239000011521 glass Substances 0.000 description 1
- LYCAIKOWRPUZTN-UHFFFAOYSA-N glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 description 1
- 239000004312 hexamethylene tetramine Substances 0.000 description 1
- 235000010299 hexamethylene tetramine Nutrition 0.000 description 1
- UFHFLCQGNIYNRP-UHFFFAOYSA-N hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 description 1
- 229910000041 hydrogen chloride Inorganic materials 0.000 description 1
- 239000004615 ingredient Substances 0.000 description 1
- 229910052500 inorganic mineral Inorganic materials 0.000 description 1
- 239000011707 mineral Substances 0.000 description 1
- 235000010446 mineral oil Nutrition 0.000 description 1
- UFWIBTONFRDIAS-UHFFFAOYSA-N naphthalene Chemical compound C1=CC=CC2=CC=CC=C21 UFWIBTONFRDIAS-UHFFFAOYSA-N 0.000 description 1
- 229910052757 nitrogen Inorganic materials 0.000 description 1
- 235000014571 nuts Nutrition 0.000 description 1
- 229920002866 paraformaldehyde Polymers 0.000 description 1
- 239000003208 petroleum Substances 0.000 description 1
- 229940044654 phenolsulfonic acid Drugs 0.000 description 1
- 229920000573 polyethylene Polymers 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 239000011541 reaction mixture Substances 0.000 description 1
- 150000003839 salts Chemical class 0.000 description 1
- 239000011780 sodium chloride Substances 0.000 description 1
- 238000007711 solidification Methods 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
- 239000000600 sorbitol Substances 0.000 description 1
- LSNNMFCWUKXFEE-UHFFFAOYSA-N sulfonic acid Chemical group OS(O)=O LSNNMFCWUKXFEE-UHFFFAOYSA-N 0.000 description 1
- NINIDFKCEFEMDL-UHFFFAOYSA-N sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 description 1
- 229910052717 sulfur Inorganic materials 0.000 description 1
- 239000011593 sulfur Substances 0.000 description 1
- 150000003739 xylenols Chemical class 0.000 description 1
Priority Applications (13)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE2058663A DE2058663B2 (de) | 1970-11-28 | 1970-11-28 | Verfahren zur Herstellung von Phenolharzschaumstoffen |
| ES395888A ES395888A1 (es) | 1970-11-28 | 1971-10-09 | Procedimiento para la produccion de materiales espumados. |
| ZA717190A ZA717190B (en) | 1970-11-28 | 1971-10-27 | Process for the preparation of phenol-resin foam materials |
| IT54118/71A IT944958B (it) | 1970-11-28 | 1971-11-16 | Procedimento per la produzione di espansi di resina fenolica |
| US199771A US3694387A (en) | 1970-11-28 | 1971-11-17 | Phenolic resin foams |
| CH1698871A CH582206A5 (fr) | 1970-11-28 | 1971-11-23 | |
| GB5468571A GB1362393A (en) | 1970-11-28 | 1971-11-24 | Preparation of phenolic resin foams |
| FR7142248A FR2115403B1 (fr) | 1970-11-28 | 1971-11-25 | |
| BE775886A BE775886A (fr) | 1970-11-28 | 1971-11-26 | Procede pour l'obtention de produits cellulaires a base de resines phenoliques |
| SE7115187A SE388425B (sv) | 1970-11-28 | 1971-11-26 | Sett att framstella fenolhartsskumplaster med minskad benegenhet till krympning och sprickbildning |
| CA128,737A CA942000A (en) | 1970-11-28 | 1971-11-26 | Process for the production of phenol resin foams |
| NL7116271A NL7116271A (fr) | 1970-11-28 | 1971-11-26 | |
| AT1021971A AT314837B (de) | 1970-11-28 | 1971-11-26 | Phenolharzschaumstoffe auf Resol-Basis und Verfahren zur Herstellung derselben |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE2058663A DE2058663B2 (de) | 1970-11-28 | 1970-11-28 | Verfahren zur Herstellung von Phenolharzschaumstoffen |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| DE2058663A1 DE2058663A1 (de) | 1972-05-31 |
| DE2058663B2 DE2058663B2 (de) | 1975-08-28 |
| DE2058663C3 true DE2058663C3 (fr) | 1976-04-08 |
Family
ID=5789397
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE2058663A Granted DE2058663B2 (de) | 1970-11-28 | 1970-11-28 | Verfahren zur Herstellung von Phenolharzschaumstoffen |
Country Status (13)
| Country | Link |
|---|---|
| US (1) | US3694387A (fr) |
| AT (1) | AT314837B (fr) |
| BE (1) | BE775886A (fr) |
| CA (1) | CA942000A (fr) |
| CH (1) | CH582206A5 (fr) |
| DE (1) | DE2058663B2 (fr) |
| ES (1) | ES395888A1 (fr) |
| FR (1) | FR2115403B1 (fr) |
| GB (1) | GB1362393A (fr) |
| IT (1) | IT944958B (fr) |
| NL (1) | NL7116271A (fr) |
| SE (1) | SE388425B (fr) |
| ZA (1) | ZA717190B (fr) |
Families Citing this family (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS5927772B2 (ja) * | 1973-06-01 | 1984-07-07 | エツソ リサ−チ アンド エンジニアリング カンパニ− | 改良発泡フエノ−ル樹脂ボ−ド及びその成形方法 |
| US4001148A (en) * | 1974-03-21 | 1977-01-04 | Deutsche Texaco Aktiengesellschaft | Process for the production of flame-resistant phenolic resin foam plastics |
| US4045398A (en) * | 1975-11-24 | 1977-08-30 | Monsanto Company | Resole resin binder composition |
| US4122045A (en) * | 1976-05-24 | 1978-10-24 | Armstrong Cork Company | Non-punking non-corrosive phenolic foam containing sodium tetraborate |
| US4219623A (en) * | 1977-07-26 | 1980-08-26 | Reichhold Limited | Phenol formaldehyde resin foams |
| DE3031840C1 (de) * | 1980-08-23 | 1982-03-18 | Rütgerswerke AG, 6000 Frankfurt | Herstellung von Schaumstoffen |
| US4478958A (en) * | 1981-07-10 | 1984-10-23 | Kopper Company, Inc. | Method for preparing phenolic foams using anhydrous aryl sulfonic acid catalysts |
| US4444912A (en) * | 1981-07-10 | 1984-04-24 | Koppers Company, Inc. | Phenolic foam and composition and method for preparing the same |
| US4525492A (en) * | 1982-06-04 | 1985-06-25 | Fiberglas Canada Inc. | Modified phenolic foams |
| US4539338A (en) * | 1982-07-09 | 1985-09-03 | Koppers Company, Inc. | Phenol formaldehyde resoles for making phenolic foam |
| US4426462A (en) | 1982-07-27 | 1984-01-17 | Dynamit Nobel Ag | Method for the preparation of highly absorbent phenolic resin foams |
-
1970
- 1970-11-28 DE DE2058663A patent/DE2058663B2/de active Granted
-
1971
- 1971-10-09 ES ES395888A patent/ES395888A1/es not_active Expired
- 1971-10-27 ZA ZA717190A patent/ZA717190B/xx unknown
- 1971-11-16 IT IT54118/71A patent/IT944958B/it active
- 1971-11-17 US US199771A patent/US3694387A/en not_active Expired - Lifetime
- 1971-11-23 CH CH1698871A patent/CH582206A5/xx unknown
- 1971-11-24 GB GB5468571A patent/GB1362393A/en not_active Expired
- 1971-11-25 FR FR7142248A patent/FR2115403B1/fr not_active Expired
- 1971-11-26 BE BE775886A patent/BE775886A/fr unknown
- 1971-11-26 SE SE7115187A patent/SE388425B/xx unknown
- 1971-11-26 CA CA128,737A patent/CA942000A/en not_active Expired
- 1971-11-26 AT AT1021971A patent/AT314837B/de not_active IP Right Cessation
- 1971-11-26 NL NL7116271A patent/NL7116271A/xx unknown
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