DE1617246C3 - Verfahren zur Herstellung von rieselfähigen Waschpulvermischungen - Google Patents
Verfahren zur Herstellung von rieselfähigen WaschpulvermischungenInfo
- Publication number
- DE1617246C3 DE1617246C3 DE1617246A DE1617246A DE1617246C3 DE 1617246 C3 DE1617246 C3 DE 1617246C3 DE 1617246 A DE1617246 A DE 1617246A DE 1617246 A DE1617246 A DE 1617246A DE 1617246 C3 DE1617246 C3 DE 1617246C3
- Authority
- DE
- Germany
- Prior art keywords
- washing
- perborate
- spray
- production
- powder
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 238000000034 method Methods 0.000 title claims description 28
- 238000005406 washing Methods 0.000 title claims description 22
- 239000000843 powder Substances 0.000 title claims description 15
- 239000000203 mixture Substances 0.000 title claims description 13
- 238000004519 manufacturing process Methods 0.000 title claims description 9
- 239000007921 spray Substances 0.000 claims description 30
- 239000003599 detergent Substances 0.000 claims description 19
- 239000008187 granular material Substances 0.000 claims description 19
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 17
- 239000000126 substance Substances 0.000 claims description 16
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 claims description 13
- 239000000155 melt Substances 0.000 claims description 13
- 239000001301 oxygen Substances 0.000 claims description 13
- 229910052760 oxygen Inorganic materials 0.000 claims description 13
- 239000013543 active substance Substances 0.000 claims description 10
- 239000000047 product Substances 0.000 claims description 8
- 238000002156 mixing Methods 0.000 claims description 7
- 239000002002 slurry Substances 0.000 claims description 7
- 238000005507 spraying Methods 0.000 claims description 7
- 239000004615 ingredient Substances 0.000 claims description 6
- 239000002245 particle Substances 0.000 claims description 6
- 150000001875 compounds Chemical class 0.000 claims description 5
- 239000000470 constituent Substances 0.000 claims description 5
- 229960001922 sodium perborate Drugs 0.000 claims description 5
- YKLJGMBLPUQQOI-UHFFFAOYSA-M sodium;oxidooxy(oxo)borane Chemical compound [Na+].[O-]OB=O YKLJGMBLPUQQOI-UHFFFAOYSA-M 0.000 claims description 5
- 239000000654 additive Substances 0.000 claims description 4
- 239000007795 chemical reaction product Substances 0.000 claims description 4
- 238000000354 decomposition reaction Methods 0.000 claims description 4
- 238000009826 distribution Methods 0.000 claims description 4
- 238000001035 drying Methods 0.000 claims description 4
- 239000000428 dust Substances 0.000 claims description 4
- 239000007788 liquid Substances 0.000 claims description 3
- FYYHWMGAXLPEAU-UHFFFAOYSA-N Magnesium Chemical compound [Mg] FYYHWMGAXLPEAU-UHFFFAOYSA-N 0.000 claims description 2
- HCHKCACWOHOZIP-UHFFFAOYSA-N Zinc Chemical compound [Zn] HCHKCACWOHOZIP-UHFFFAOYSA-N 0.000 claims description 2
- 238000007664 blowing Methods 0.000 claims description 2
- 229910052793 cadmium Inorganic materials 0.000 claims description 2
- BDOSMKKIYDKNTQ-UHFFFAOYSA-N cadmium atom Chemical compound [Cd] BDOSMKKIYDKNTQ-UHFFFAOYSA-N 0.000 claims description 2
- 239000003795 chemical substances by application Substances 0.000 claims description 2
- 239000007791 liquid phase Substances 0.000 claims description 2
- 239000011777 magnesium Substances 0.000 claims description 2
- 229910052749 magnesium Inorganic materials 0.000 claims description 2
- 230000035515 penetration Effects 0.000 claims description 2
- 238000002360 preparation method Methods 0.000 claims description 2
- 230000000717 retained effect Effects 0.000 claims description 2
- 239000007790 solid phase Substances 0.000 claims description 2
- 239000003381 stabilizer Substances 0.000 claims description 2
- 229910052725 zinc Inorganic materials 0.000 claims description 2
- 239000011701 zinc Substances 0.000 claims description 2
- 150000002927 oxygen compounds Chemical class 0.000 claims 5
- 238000002425 crystallisation Methods 0.000 claims 2
- 230000008025 crystallization Effects 0.000 claims 2
- 230000018109 developmental process Effects 0.000 claims 2
- 238000001694 spray drying Methods 0.000 claims 2
- AEMRFAOFKBGASW-UHFFFAOYSA-N Glycolic acid Chemical class OCC(O)=O AEMRFAOFKBGASW-UHFFFAOYSA-N 0.000 claims 1
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 claims 1
- 229910019142 PO4 Inorganic materials 0.000 claims 1
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 claims 1
- 238000004220 aggregation Methods 0.000 claims 1
- 230000002776 aggregation Effects 0.000 claims 1
- 230000032683 aging Effects 0.000 claims 1
- 238000007605 air drying Methods 0.000 claims 1
- 125000000129 anionic group Chemical group 0.000 claims 1
- 230000015572 biosynthetic process Effects 0.000 claims 1
- 239000007844 bleaching agent Substances 0.000 claims 1
- 239000001913 cellulose Substances 0.000 claims 1
- 229920002678 cellulose Polymers 0.000 claims 1
- 238000006243 chemical reaction Methods 0.000 claims 1
- 230000001419 dependent effect Effects 0.000 claims 1
- 239000000945 filler Substances 0.000 claims 1
- 230000036571 hydration Effects 0.000 claims 1
- 238000006703 hydration reaction Methods 0.000 claims 1
- 239000001257 hydrogen Substances 0.000 claims 1
- 229910052739 hydrogen Inorganic materials 0.000 claims 1
- 238000010348 incorporation Methods 0.000 claims 1
- 238000009994 optical bleaching Methods 0.000 claims 1
- 150000002978 peroxides Chemical class 0.000 claims 1
- 235000021317 phosphate Nutrition 0.000 claims 1
- 150000003013 phosphoric acid derivatives Chemical class 0.000 claims 1
- 108090000623 proteins and genes Proteins 0.000 claims 1
- 238000005204 segregation Methods 0.000 claims 1
- 238000000926 separation method Methods 0.000 claims 1
- 239000000243 solution Substances 0.000 claims 1
- 230000006641 stabilisation Effects 0.000 claims 1
- 238000011105 stabilization Methods 0.000 claims 1
- 239000004094 surface-active agent Substances 0.000 claims 1
- 239000000080 wetting agent Substances 0.000 claims 1
- MHAJPDPJQMAIIY-UHFFFAOYSA-N Hydrogen peroxide Chemical compound OO MHAJPDPJQMAIIY-UHFFFAOYSA-N 0.000 description 4
- 238000002844 melting Methods 0.000 description 4
- 230000008018 melting Effects 0.000 description 4
- BTBUEUYNUDRHOZ-UHFFFAOYSA-N Borate Chemical compound [O-]B([O-])[O-] BTBUEUYNUDRHOZ-UHFFFAOYSA-N 0.000 description 2
- TWRXJAOTZQYOKJ-UHFFFAOYSA-L Magnesium chloride Chemical compound [Mg+2].[Cl-].[Cl-] TWRXJAOTZQYOKJ-UHFFFAOYSA-L 0.000 description 2
- 229910004298 SiO 2 Inorganic materials 0.000 description 2
- 239000013078 crystal Substances 0.000 description 2
- 238000004090 dissolution Methods 0.000 description 2
- 238000005029 sieve analysis Methods 0.000 description 2
- 239000011734 sodium Substances 0.000 description 2
- 238000003756 stirring Methods 0.000 description 2
- 238000003860 storage Methods 0.000 description 2
- 150000004685 tetrahydrates Chemical class 0.000 description 2
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 1
- 239000004698 Polyethylene Substances 0.000 description 1
- 239000004115 Sodium Silicate Substances 0.000 description 1
- PMZURENOXWZQFD-UHFFFAOYSA-L Sodium Sulfate Chemical compound [Na+].[Na+].[O-]S([O-])(=O)=O PMZURENOXWZQFD-UHFFFAOYSA-L 0.000 description 1
- 238000013459 approach Methods 0.000 description 1
- 239000011248 coating agent Substances 0.000 description 1
- 238000000576 coating method Methods 0.000 description 1
- 238000010924 continuous production Methods 0.000 description 1
- 239000006185 dispersion Substances 0.000 description 1
- 239000004744 fabric Substances 0.000 description 1
- 239000012467 final product Substances 0.000 description 1
- 239000012530 fluid Substances 0.000 description 1
- 239000003292 glue Substances 0.000 description 1
- 229910001629 magnesium chloride Inorganic materials 0.000 description 1
- 159000000003 magnesium salts Chemical class 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 239000004033 plastic Substances 0.000 description 1
- 229920003023 plastic Polymers 0.000 description 1
- -1 polyethylene Polymers 0.000 description 1
- 229920000573 polyethylene Polymers 0.000 description 1
- 230000002028 premature Effects 0.000 description 1
- 230000000750 progressive effect Effects 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 229910052708 sodium Inorganic materials 0.000 description 1
- NTHWMYGWWRZVTN-UHFFFAOYSA-N sodium silicate Chemical compound [Na+].[Na+].[O-][Si]([O-])=O NTHWMYGWWRZVTN-UHFFFAOYSA-N 0.000 description 1
- 229910052911 sodium silicate Inorganic materials 0.000 description 1
- 229910052938 sodium sulfate Inorganic materials 0.000 description 1
- 235000011152 sodium sulphate Nutrition 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 238000001228 spectrum Methods 0.000 description 1
- 239000000725 suspension Substances 0.000 description 1
- CDVLCTOFEIEUDH-UHFFFAOYSA-K tetrasodium;phosphate Chemical compound [Na+].[Na+].[Na+].[Na+].[O-]P([O-])([O-])=O CDVLCTOFEIEUDH-UHFFFAOYSA-K 0.000 description 1
- 238000005979 thermal decomposition reaction Methods 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/39—Organic or inorganic per-compounds
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B15/00—Peroxides; Peroxyhydrates; Peroxyacids or salts thereof; Superoxides; Ozonides
- C01B15/055—Peroxyhydrates; Peroxyacids or salts thereof
- C01B15/12—Peroxyhydrates; Peroxyacids or salts thereof containing boron
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D11/00—Special methods for preparing compositions containing mixtures of detergents
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D11/00—Special methods for preparing compositions containing mixtures of detergents
- C11D11/02—Preparation in the form of powder by spray drying
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Inorganic Chemistry (AREA)
- Detergent Compositions (AREA)
- Glanulating (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DED0052634 | 1967-03-25 | ||
| FR145244 | 1968-03-25 |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| DE1617246A1 DE1617246A1 (de) | 1972-04-20 |
| DE1617246B2 DE1617246B2 (de) | 1974-06-20 |
| DE1617246C3 true DE1617246C3 (de) | 1975-02-20 |
Family
ID=25972575
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE1617246A Expired DE1617246C3 (de) | 1967-03-25 | 1967-03-25 | Verfahren zur Herstellung von rieselfähigen Waschpulvermischungen |
Country Status (8)
Families Citing this family (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3819526A (en) * | 1970-12-23 | 1974-06-25 | Philadelphia Quartz Co | Coated detergent compositions |
| DE2431529C2 (de) * | 1974-07-01 | 1982-11-18 | Henkel KGaA, 4000 Düsseldorf | Verfahren zur Herstellung sprühgetrockneter, nichtionische Tenside enthaltender Waschmittel |
| GB2041966A (en) * | 1977-11-29 | 1980-09-17 | Procter & Gamble | Detergent tablet having a hydrated salt coating and process for preparing the tablet |
-
1967
- 1967-03-25 DE DE1617246A patent/DE1617246C3/de not_active Expired
-
1968
- 1968-03-08 NL NL6803364.A patent/NL157054B/xx unknown
- 1968-03-19 GB GB03175/68A patent/GB1220998A/en not_active Expired
- 1968-03-19 CH CH398268A patent/CH498928A/de not_active IP Right Cessation
- 1968-03-20 BE BE712532D patent/BE712532A/xx unknown
- 1968-03-25 FR FR145244A patent/FR1601093A/fr not_active Expired
- 1968-03-25 AT AT294868A patent/AT297895B/de not_active IP Right Cessation
- 1968-03-27 US US716333A patent/US3562164A/en not_active Expired - Lifetime
Also Published As
| Publication number | Publication date |
|---|---|
| NL6803364A (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html) | 1968-09-26 |
| DE1617246B2 (de) | 1974-06-20 |
| CH498928A (de) | 1970-11-15 |
| DE1617246A1 (de) | 1972-04-20 |
| AT297895B (de) | 1972-04-10 |
| GB1220998A (en) | 1971-01-27 |
| NL157054B (nl) | 1978-06-15 |
| FR1601093A (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html) | 1970-08-10 |
| US3562164A (en) | 1971-02-09 |
| BE712532A (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html) | 1968-07-31 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| EP0037026B1 (de) | Verfahren zur Herstellung eines lagerstabilen, leichtlöslichen Granulates mit einem Gehalt an Bleichaktivatoren | |
| DE69404543T2 (de) | Stabilisiertes Natriumpercarbonatteilchen | |
| DE4435743C2 (de) | Verfahren zur Herstellung eines Mehrkomponenten-Granulates | |
| DE68921858T2 (de) | Verfahren zur Herstellung von Bleichmittelgranulaten. | |
| EP0191396A1 (de) | Verfahren zur Herstellung eines rieselfähigen Granulats | |
| DE19608000B4 (de) | Verfahren zur Herstellung von körnigem Natriumpercarbonat | |
| DE3036325A1 (de) | Verfahren zur verhinderung der gelierung von bicarbonat-carbonat-silikat seifenmischeraufschlaemmungen | |
| DE2024476A1 (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html) | ||
| DE69104124T2 (de) | Verfahren zur Herstellung von stabilisiertem Natriumperkarbonat. | |
| DE1144866B (de) | Verfahren zur Herstellung eines koernigen Reinigungsmittels | |
| DE1617246C3 (de) | Verfahren zur Herstellung von rieselfähigen Waschpulvermischungen | |
| DE1297587B (de) | Verfahren zur Herstellung eines schnelloeslichen agglomerierten Natriumperborats | |
| DE4110510A1 (de) | Niederalkalische, chlor- und phosphatfreie maschinengeschirrspuelmittel in form von schwerpulvern und -granulaten | |
| WO1984003708A1 (en) | Granular free flowing detergent composition and separation method thereof | |
| DE2925137A1 (de) | Homogene, staubfreie und rieselfaehige wasch- und reinigungsmittelgranulate, sowie verfahren zu deren herstellung | |
| AT213373B (de) | Verfahren zur Herstellung von Granulaten kondensierter Phosphatperhydrate | |
| DE2024439A1 (de) | Verfahren zur Herstellung von Agglomeraten aus kondensierten Alkaliphosphaten | |
| DE2822765B2 (de) | Granuliertes Rohmaterial zur Herstellung von Reinigungsmitteln und Verfahren zu seiner Herstellung | |
| DE1229978B (de) | Bleichmittel | |
| EP0822974B1 (de) | Lagerstabiles, bleichaktivatoren enthaltendes granulat und seine herstellung | |
| DE2547203C2 (de) | Pulverförmige, nichtionische Tenside und Seife enthaltende Wasch- und Reinigungsmittel, sowie Verfahren zu deren Herstellung | |
| DE2337262A1 (de) | Freifliessende phosphatestermischung, verfahren zu deren herstellung und deren verwendung | |
| DE1617050C3 (de) | Kontinuierliches Verfahren zur Herstellung von Waschmitteln mit niedrigem Schüttgewicht | |
| DE1594867C3 (de) | Verfahren zur Herstellung eines granulierten Bleichmittels | |
| DE1125580B (de) | Verfahren zur Herstellung einheitlicher nicht staeubender Wasch- und Reinigungsmittel |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C3 | Grant after two publication steps (3rd publication) | ||
| EHJ | Ceased/non-payment of the annual fee |