DE1567777B1 - Verfahren zur kontinuierlichen Herstellung von Schwefelkohlenstoff - Google Patents
Verfahren zur kontinuierlichen Herstellung von SchwefelkohlenstoffInfo
- Publication number
- DE1567777B1 DE1567777B1 DE1966P0041109 DEP0041109A DE1567777B1 DE 1567777 B1 DE1567777 B1 DE 1567777B1 DE 1966P0041109 DE1966P0041109 DE 1966P0041109 DE P0041109 A DEP0041109 A DE P0041109A DE 1567777 B1 DE1567777 B1 DE 1567777B1
- Authority
- DE
- Germany
- Prior art keywords
- sulfur
- carbon disulfide
- weight
- carbon
- preheated
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- QGJOPFRUJISHPQ-UHFFFAOYSA-N Carbon disulfide Chemical compound S=C=S QGJOPFRUJISHPQ-UHFFFAOYSA-N 0.000 title claims description 68
- 238000000034 method Methods 0.000 title claims description 18
- 238000010924 continuous production Methods 0.000 title claims description 3
- 229910052717 sulfur Inorganic materials 0.000 claims description 55
- 239000011593 sulfur Substances 0.000 claims description 55
- NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 claims description 54
- 150000001336 alkenes Chemical class 0.000 claims description 17
- JRZJOMJEPLMPRA-UHFFFAOYSA-N olefin Natural products CCCCCCCC=C JRZJOMJEPLMPRA-UHFFFAOYSA-N 0.000 claims description 14
- 239000000203 mixture Substances 0.000 claims description 10
- 239000003054 catalyst Substances 0.000 claims description 9
- 239000007795 chemical reaction product Substances 0.000 claims description 6
- 229930195735 unsaturated hydrocarbon Natural products 0.000 claims description 6
- 150000001993 dienes Chemical class 0.000 claims description 5
- 238000009833 condensation Methods 0.000 claims description 3
- 230000005494 condensation Effects 0.000 claims description 3
- 239000012808 vapor phase Substances 0.000 claims description 3
- 150000001338 aliphatic hydrocarbons Chemical class 0.000 claims description 2
- 238000002336 sorption--desorption measurement Methods 0.000 claims description 2
- 238000006243 chemical reaction Methods 0.000 description 21
- QQONPFPTGQHPMA-UHFFFAOYSA-N propylene Natural products CC=C QQONPFPTGQHPMA-UHFFFAOYSA-N 0.000 description 10
- 125000004805 propylene group Chemical group [H]C([H])([H])C([H])([*:1])C([H])([H])[*:2] 0.000 description 10
- 229930195733 hydrocarbon Natural products 0.000 description 9
- 229910052799 carbon Inorganic materials 0.000 description 8
- 150000002430 hydrocarbons Chemical class 0.000 description 8
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 7
- 230000015572 biosynthetic process Effects 0.000 description 7
- 239000000376 reactant Substances 0.000 description 7
- RWSOTUBLDIXVET-UHFFFAOYSA-N Dihydrogen sulfide Chemical compound S RWSOTUBLDIXVET-UHFFFAOYSA-N 0.000 description 6
- 238000004519 manufacturing process Methods 0.000 description 6
- VNWKTOKETHGBQD-UHFFFAOYSA-N methane Chemical compound C VNWKTOKETHGBQD-UHFFFAOYSA-N 0.000 description 6
- 239000007789 gas Substances 0.000 description 5
- 229910000037 hydrogen sulfide Inorganic materials 0.000 description 5
- 239000000047 product Substances 0.000 description 5
- 239000007858 starting material Substances 0.000 description 5
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 4
- KAKZBPTYRLMSJV-UHFFFAOYSA-N Butadiene Chemical compound C=CC=C KAKZBPTYRLMSJV-UHFFFAOYSA-N 0.000 description 4
- YTPLMLYBLZKORZ-UHFFFAOYSA-N Thiophene Chemical compound C=1C=CSC=1 YTPLMLYBLZKORZ-UHFFFAOYSA-N 0.000 description 4
- UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 description 3
- VGGSQFUCUMXWEO-UHFFFAOYSA-N Ethene Chemical compound C=C VGGSQFUCUMXWEO-UHFFFAOYSA-N 0.000 description 3
- 239000005977 Ethylene Substances 0.000 description 3
- 239000000463 material Substances 0.000 description 3
- XDAHMMVFVQFOIY-UHFFFAOYSA-N methanedithione;sulfane Chemical compound S.S=C=S XDAHMMVFVQFOIY-UHFFFAOYSA-N 0.000 description 3
- 239000011541 reaction mixture Substances 0.000 description 3
- 239000004215 Carbon black (E152) Substances 0.000 description 2
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 description 2
- RRHGJUQNOFWUDK-UHFFFAOYSA-N Isoprene Chemical compound CC(=C)C=C RRHGJUQNOFWUDK-UHFFFAOYSA-N 0.000 description 2
- ATUOYWHBWRKTHZ-UHFFFAOYSA-N Propane Chemical compound CCC ATUOYWHBWRKTHZ-UHFFFAOYSA-N 0.000 description 2
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 2
- 239000006227 byproduct Substances 0.000 description 2
- QGJOPFRUJISHPQ-NJFSPNSNSA-N carbon disulfide-14c Chemical compound S=[14C]=S QGJOPFRUJISHPQ-NJFSPNSNSA-N 0.000 description 2
- 239000003085 diluting agent Substances 0.000 description 2
- 238000004821 distillation Methods 0.000 description 2
- -1 ethylene, propylene Chemical group 0.000 description 2
- 238000010438 heat treatment Methods 0.000 description 2
- 239000001257 hydrogen Substances 0.000 description 2
- 229910052739 hydrogen Inorganic materials 0.000 description 2
- 239000007788 liquid Substances 0.000 description 2
- 229910052757 nitrogen Inorganic materials 0.000 description 2
- KMUONIBRACKNSN-UHFFFAOYSA-N potassium dichromate Chemical compound [K+].[K+].[O-][Cr](=O)(=O)O[Cr]([O-])(=O)=O KMUONIBRACKNSN-UHFFFAOYSA-N 0.000 description 2
- 238000000926 separation method Methods 0.000 description 2
- 229930192474 thiophene Natural products 0.000 description 2
- PMJHHCWVYXUKFD-SNAWJCMRSA-N (E)-1,3-pentadiene Chemical group C\C=C\C=C PMJHHCWVYXUKFD-SNAWJCMRSA-N 0.000 description 1
- 101710178035 Chorismate synthase 2 Proteins 0.000 description 1
- 101710152694 Cysteine synthase 2 Proteins 0.000 description 1
- OTMSDBZUPAUEDD-UHFFFAOYSA-N Ethane Chemical compound CC OTMSDBZUPAUEDD-UHFFFAOYSA-N 0.000 description 1
- 241000589614 Pseudomonas stutzeri Species 0.000 description 1
- DQLMKXXPBLQRCQ-UHFFFAOYSA-N [C].S=C=S Chemical compound [C].S=C=S DQLMKXXPBLQRCQ-UHFFFAOYSA-N 0.000 description 1
- 125000001931 aliphatic group Chemical group 0.000 description 1
- HSFWRNGVRCDJHI-UHFFFAOYSA-N alpha-acetylene Natural products C#C HSFWRNGVRCDJHI-UHFFFAOYSA-N 0.000 description 1
- PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 description 1
- 125000004429 atom Chemical group 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 238000007664 blowing Methods 0.000 description 1
- 238000009835 boiling Methods 0.000 description 1
- 239000011449 brick Substances 0.000 description 1
- 125000004432 carbon atom Chemical group C* 0.000 description 1
- 239000000969 carrier Substances 0.000 description 1
- 230000003197 catalytic effect Effects 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 238000004140 cleaning Methods 0.000 description 1
- 239000003245 coal Substances 0.000 description 1
- 238000005336 cracking Methods 0.000 description 1
- 150000002019 disulfides Chemical class 0.000 description 1
- 238000003920 environmental process Methods 0.000 description 1
- 125000002534 ethynyl group Chemical group [H]C#C* 0.000 description 1
- 230000001771 impaired effect Effects 0.000 description 1
- 239000012535 impurity Substances 0.000 description 1
- 238000009776 industrial production Methods 0.000 description 1
- 150000002898 organic sulfur compounds Chemical class 0.000 description 1
- 239000012188 paraffin wax Substances 0.000 description 1
- 239000012071 phase Substances 0.000 description 1
- PMJHHCWVYXUKFD-UHFFFAOYSA-N piperylene Natural products CC=CC=C PMJHHCWVYXUKFD-UHFFFAOYSA-N 0.000 description 1
- 229910052573 porcelain Inorganic materials 0.000 description 1
- 239000001294 propane Substances 0.000 description 1
- 239000012429 reaction media Substances 0.000 description 1
- 229920006395 saturated elastomer Polymers 0.000 description 1
- 229930195734 saturated hydrocarbon Natural products 0.000 description 1
- 239000000377 silicon dioxide Substances 0.000 description 1
- 239000011343 solid material Substances 0.000 description 1
- 230000006641 stabilisation Effects 0.000 description 1
- 238000011105 stabilization Methods 0.000 description 1
- 229910001220 stainless steel Inorganic materials 0.000 description 1
- 229940059867 sulfur containing product ectoparasiticides Drugs 0.000 description 1
- 239000011273 tar residue Substances 0.000 description 1
- 125000000383 tetramethylene group Chemical group [H]C([H])([*:1])C([H])([H])C([H])([H])C([H])([H])[*:2] 0.000 description 1
- 150000003568 thioethers Chemical class 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B32/00—Carbon; Compounds thereof
- C01B32/70—Compounds containing carbon and sulfur, e.g. thiophosgene
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Addition Polymer Or Copolymer, Post-Treatments, Or Chemical Modifications (AREA)
- Production Of Liquid Hydrocarbon Mixture For Refining Petroleum (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| FR47139A FR1482173A (fr) | 1966-04-07 | 1966-04-07 | Procédé de fabrication de sulfure de carbone |
| FR47948A FR91186E (fr) | 1966-04-07 | 1966-11-15 | Procédé de fabrication de sulfure de carbone |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| DE1567777B1 true DE1567777B1 (de) | 1970-09-24 |
Family
ID=26235534
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE1966P0041109 Pending DE1567777B1 (de) | 1966-04-07 | 1966-12-28 | Verfahren zur kontinuierlichen Herstellung von Schwefelkohlenstoff |
Country Status (9)
Families Citing this family (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| FR1573969A (US20100056889A1-20100304-C00004.png) * | 1968-03-26 | 1969-07-11 | ||
| US3932595A (en) * | 1971-03-02 | 1976-01-13 | Rhone-Progil | Process of manufacturing carbon bisulfide |
| US3927185A (en) * | 1973-04-30 | 1975-12-16 | Fmc Corp | Process for producing carbon disulfide |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE708201C (de) * | 1939-05-27 | 1941-07-15 | Dr Egbert Dittrich | Herstellung von Schwefelkohlenstoff aus Kohlenwasserstoffen und Schwefel |
| DE803114C (de) * | 1949-02-17 | 1951-03-01 | Basf Ag | Verfahren zur Herstellung von Schwefelkohlenstoff |
| DE848646C (de) * | 1949-11-29 | 1952-09-04 | Basf Ag | Verfahren zur Herstellung von Schwefelkohlenstoff und organischen Schwefelverbindungen |
Family Cites Families (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CA627423A (en) * | 1961-09-12 | A. Banks Arthur | Production of carbon disulphide | |
| CA584646A (en) * | 1959-10-06 | W. Timmerman Robert | Production of carbon disulfide | |
| US2369377A (en) * | 1940-12-28 | 1945-02-13 | Pure Oil Co | Method of preparing sulphur compounds |
| US2392629A (en) * | 1942-01-21 | 1946-01-08 | Little Inc A | Method of making carbon bisulphide |
| US2424894A (en) * | 1945-06-06 | 1947-07-29 | Little Inc A | Method of making carbon bisulfide |
| US2666690A (en) * | 1951-12-28 | 1954-01-19 | Food Machienry And Chemical Co | Process for the production of carbon disulfide |
| US3082069A (en) * | 1958-11-12 | 1963-03-19 | Ici Ltd | Method of preparing carbon disulfide and hydrogen sulphide |
| US3250595A (en) * | 1962-07-12 | 1966-05-10 | Fmc Corp | Method of producing carbon bisulfide |
-
1966
- 1966-04-07 FR FR47139A patent/FR1482173A/fr not_active Expired
- 1966-11-15 FR FR47948A patent/FR91186E/fr not_active Expired
- 1966-12-13 BE BE691135A patent/BE691135A/xx unknown
- 1966-12-13 GB GB55839/66A patent/GB1104125A/en not_active Expired
- 1966-12-21 NL NL6617967A patent/NL6617967A/xx unknown
- 1966-12-24 ES ES334913A patent/ES334913A1/es not_active Expired
- 1966-12-28 DE DE1966P0041109 patent/DE1567777B1/de active Pending
- 1966-12-29 US US605555A patent/US3436181A/en not_active Expired - Lifetime
- 1966-12-29 CS CS8376A patent/CS151444B2/cs unknown
- 1966-12-29 CS CS663135A patent/CS157749B2/cs unknown
-
1967
- 1967-01-13 AT AT39067A patent/AT268320B/de active
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE708201C (de) * | 1939-05-27 | 1941-07-15 | Dr Egbert Dittrich | Herstellung von Schwefelkohlenstoff aus Kohlenwasserstoffen und Schwefel |
| DE803114C (de) * | 1949-02-17 | 1951-03-01 | Basf Ag | Verfahren zur Herstellung von Schwefelkohlenstoff |
| DE848646C (de) * | 1949-11-29 | 1952-09-04 | Basf Ag | Verfahren zur Herstellung von Schwefelkohlenstoff und organischen Schwefelverbindungen |
Also Published As
| Publication number | Publication date |
|---|---|
| CS151444B2 (US20100056889A1-20100304-C00004.png) | 1973-10-19 |
| CS157749B2 (en) | 1974-09-16 |
| BE691135A (US20100056889A1-20100304-C00004.png) | 1967-05-16 |
| GB1104125A (en) | 1968-02-21 |
| US3436181A (en) | 1969-04-01 |
| NL6617967A (US20100056889A1-20100304-C00004.png) | 1967-10-09 |
| ES334913A1 (es) | 1968-03-01 |
| FR1482173A (fr) | 1967-05-26 |
| FR91186E (fr) | 1968-04-26 |
| AT268320B (de) | 1969-02-10 |
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