DE1418569A1 - Verfahren zur Herstellung von Carbamaten - Google Patents
Verfahren zur Herstellung von CarbamatenInfo
- Publication number
- DE1418569A1 DE1418569A1 DE19611418569 DE1418569A DE1418569A1 DE 1418569 A1 DE1418569 A1 DE 1418569A1 DE 19611418569 DE19611418569 DE 19611418569 DE 1418569 A DE1418569 A DE 1418569A DE 1418569 A1 DE1418569 A1 DE 1418569A1
- Authority
- DE
- Germany
- Prior art keywords
- parts
- der
- orin
- bad
- tin
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 238000000034 method Methods 0.000 title claims description 6
- 238000004519 manufacturing process Methods 0.000 title description 2
- 150000004657 carbamic acid derivatives Chemical class 0.000 title 1
- 229910052783 alkali metal Inorganic materials 0.000 claims description 2
- 150000001340 alkali metals Chemical group 0.000 claims description 2
- 125000000217 alkyl group Chemical group 0.000 claims description 2
- ATJFFYVFTNAWJD-UHFFFAOYSA-N Tin Chemical compound [Sn] ATJFFYVFTNAWJD-UHFFFAOYSA-N 0.000 claims 1
- 239000000126 substance Substances 0.000 claims 1
- QHGNHLZPVBIIPX-UHFFFAOYSA-N tin(ii) oxide Chemical compound [Sn]=O QHGNHLZPVBIIPX-UHFFFAOYSA-N 0.000 claims 1
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 14
- 239000000047 product Substances 0.000 description 10
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 7
- 239000003921 oil Substances 0.000 description 7
- RAOIDOHSFRTOEL-UHFFFAOYSA-N tetrahydrothiophene Chemical compound C1CCSC1 RAOIDOHSFRTOEL-UHFFFAOYSA-N 0.000 description 6
- CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 description 4
- 150000001875 compounds Chemical class 0.000 description 4
- -1 2-n-butyl Chemical group 0.000 description 3
- WEVYAHXRMPXWCK-UHFFFAOYSA-N Acetonitrile Chemical compound CC#N WEVYAHXRMPXWCK-UHFFFAOYSA-N 0.000 description 3
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 3
- 238000001816 cooling Methods 0.000 description 3
- QPJDMGCKMHUXFD-UHFFFAOYSA-N cyanogen chloride Chemical compound ClC#N QPJDMGCKMHUXFD-UHFFFAOYSA-N 0.000 description 3
- 125000000623 heterocyclic group Chemical group 0.000 description 3
- 239000000203 mixture Substances 0.000 description 3
- VLKZOEOYAKHREP-UHFFFAOYSA-N n-Hexane Chemical compound CCCCCC VLKZOEOYAKHREP-UHFFFAOYSA-N 0.000 description 3
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 3
- HEDRZPFGACZZDS-UHFFFAOYSA-N Chloroform Chemical compound ClC(Cl)Cl HEDRZPFGACZZDS-UHFFFAOYSA-N 0.000 description 2
- 238000009835 boiling Methods 0.000 description 2
- 229910052799 carbon Inorganic materials 0.000 description 2
- 150000002500 ions Chemical class 0.000 description 2
- SLCVBVWXLSEKPL-UHFFFAOYSA-N neopentyl glycol Chemical compound OCC(C)(C)CO SLCVBVWXLSEKPL-UHFFFAOYSA-N 0.000 description 2
- OOFGXDQWDNJDIS-UHFFFAOYSA-N oxathiolane Chemical compound C1COSC1 OOFGXDQWDNJDIS-UHFFFAOYSA-N 0.000 description 2
- 239000007787 solid Substances 0.000 description 2
- IMLSAISZLJGWPP-UHFFFAOYSA-N 1,3-dithiolane Chemical compound C1CSCS1 IMLSAISZLJGWPP-UHFFFAOYSA-N 0.000 description 1
- 101150077194 CAP1 gene Proteins 0.000 description 1
- 235000007487 Calathea allouia Nutrition 0.000 description 1
- 244000278792 Calathea allouia Species 0.000 description 1
- VEXZGXHMUGYJMC-UHFFFAOYSA-M Chloride anion Chemical compound [Cl-] VEXZGXHMUGYJMC-UHFFFAOYSA-M 0.000 description 1
- 241000272184 Falconiformes Species 0.000 description 1
- 241000910494 Heth Species 0.000 description 1
- 241000594011 Leuciscus leuciscus Species 0.000 description 1
- 241001465754 Metazoa Species 0.000 description 1
- 101100107522 Mus musculus Slc1a5 gene Proteins 0.000 description 1
- 101100438378 Neurospora crassa (strain ATCC 24698 / 74-OR23-1A / CBS 708.71 / DSM 1257 / FGSC 987) fac-1 gene Proteins 0.000 description 1
- ISWSIDIOOBJBQZ-UHFFFAOYSA-N Phenol Chemical compound OC1=CC=CC=C1 ISWSIDIOOBJBQZ-UHFFFAOYSA-N 0.000 description 1
- YGYAWVDWMABLBF-UHFFFAOYSA-N Phosgene Chemical compound ClC(Cl)=O YGYAWVDWMABLBF-UHFFFAOYSA-N 0.000 description 1
- 241000208829 Sambucus Species 0.000 description 1
- 235000018735 Sambucus canadensis Nutrition 0.000 description 1
- 241001655798 Taku Species 0.000 description 1
- 241000130764 Tinea Species 0.000 description 1
- 208000002474 Tinea Diseases 0.000 description 1
- 235000007123 blue elder Nutrition 0.000 description 1
- 244000309466 calf Species 0.000 description 1
- 150000004649 carbonic acid derivatives Chemical class 0.000 description 1
- 241001233037 catfish Species 0.000 description 1
- 230000001055 chewing effect Effects 0.000 description 1
- 239000012141 concentrate Substances 0.000 description 1
- XAEWZDYWZHIUCT-UHFFFAOYSA-N desipramine hydrochloride Chemical compound [H+].[Cl-].C1CC2=CC=CC=C2N(CCCNC)C2=CC=CC=C21 XAEWZDYWZHIUCT-UHFFFAOYSA-N 0.000 description 1
- AAOVKJBEBIDNHE-UHFFFAOYSA-N diazepam Chemical compound N=1CC(=O)N(C)C2=CC=C(Cl)C=C2C=1C1=CC=CC=C1 AAOVKJBEBIDNHE-UHFFFAOYSA-N 0.000 description 1
- 238000010790 dilution Methods 0.000 description 1
- 239000012895 dilution Substances 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 235000007124 elderberry Nutrition 0.000 description 1
- 235000008995 european elder Nutrition 0.000 description 1
- 238000001704 evaporation Methods 0.000 description 1
- 230000008020 evaporation Effects 0.000 description 1
- 239000004744 fabric Substances 0.000 description 1
- 239000012065 filter cake Substances 0.000 description 1
- 238000001914 filtration Methods 0.000 description 1
- 239000011888 foil Substances 0.000 description 1
- 239000003292 glue Substances 0.000 description 1
- 150000004820 halides Chemical class 0.000 description 1
- QWPPOHNGKGFGJK-UHFFFAOYSA-N hypochlorous acid Chemical compound ClO QWPPOHNGKGFGJK-UHFFFAOYSA-N 0.000 description 1
- 239000012535 impurity Substances 0.000 description 1
- JEIPFZHSYJVQDO-UHFFFAOYSA-N iron(III) oxide Inorganic materials O=[Fe]O[Fe]=O JEIPFZHSYJVQDO-UHFFFAOYSA-N 0.000 description 1
- 125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 description 1
- 238000000199 molecular distillation Methods 0.000 description 1
- 239000005416 organic matter Substances 0.000 description 1
- OVSQVDMCBVZWGM-QSOFNFLRSA-N quercetin 3-O-beta-D-glucopyranoside Chemical compound O[C@@H]1[C@@H](O)[C@H](O)[C@@H](CO)O[C@H]1OC1=C(C=2C=C(O)C(O)=CC=2)OC2=CC(O)=CC(O)=C2C1=O OVSQVDMCBVZWGM-QSOFNFLRSA-N 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- JVBXVOWTABLYPX-UHFFFAOYSA-L sodium dithionite Chemical compound [Na+].[Na+].[O-]S(=O)S([O-])=O JVBXVOWTABLYPX-UHFFFAOYSA-L 0.000 description 1
- 239000000243 solution Substances 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
- 244000239635 ulla Species 0.000 description 1
- 210000004291 uterus Anatomy 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D339/00—Heterocyclic compounds containing rings having two sulfur atoms as the only ring hetero atoms
- C07D339/02—Five-membered rings
- C07D339/06—Five-membered rings having the hetero atoms in positions 1 and 3, e.g. cyclic dithiocarbonates
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D339/00—Heterocyclic compounds containing rings having two sulfur atoms as the only ring hetero atoms
- C07D339/08—Six-membered rings
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
- Heterocyclic Carbon Compounds Containing A Hetero Ring Having Nitrogen And Oxygen As The Only Ring Hetero Atoms (AREA)
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US4053960A | 1960-07-05 | 1960-07-05 | |
US11253161A | 1961-05-25 | 1961-05-25 |
Publications (1)
Publication Number | Publication Date |
---|---|
DE1418569A1 true DE1418569A1 (de) | 1969-03-27 |
Family
ID=26717162
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
DE19611418569 Pending DE1418569A1 (de) | 1960-07-05 | 1961-07-03 | Verfahren zur Herstellung von Carbamaten |
Country Status (7)
Country | Link |
---|---|
BE (1) | BE605636A (enrdf_load_stackoverflow) |
CH (1) | CH400661A (enrdf_load_stackoverflow) |
DE (1) | DE1418569A1 (enrdf_load_stackoverflow) |
DK (1) | DK102832C (enrdf_load_stackoverflow) |
ES (2) | ES268558A1 (enrdf_load_stackoverflow) |
GB (1) | GB920757A (enrdf_load_stackoverflow) |
NL (1) | NL266629A (enrdf_load_stackoverflow) |
-
0
- NL NL266629D patent/NL266629A/xx unknown
- BE BE605636D patent/BE605636A/xx unknown
-
1961
- 1961-06-23 ES ES0268558A patent/ES268558A1/es not_active Expired
- 1961-07-03 GB GB2389761A patent/GB920757A/en not_active Expired
- 1961-07-03 DE DE19611418569 patent/DE1418569A1/de active Pending
- 1961-07-03 DK DK273661A patent/DK102832C/da active
- 1961-07-03 CH CH777461A patent/CH400661A/de unknown
-
1962
- 1962-01-16 ES ES0273767A patent/ES273767A1/es not_active Expired
Also Published As
Publication number | Publication date |
---|---|
ES273767A1 (es) | 1962-05-01 |
GB920757A (en) | 1963-03-13 |
DK102832C (da) | 1965-10-11 |
ES268558A1 (es) | 1962-03-01 |
NL266629A (enrdf_load_stackoverflow) | |
CH400661A (de) | 1965-10-15 |
BE605636A (enrdf_load_stackoverflow) |
Similar Documents
Publication | Publication Date | Title |
---|---|---|
DE1670772B2 (de) | 4h-3,1-benzoxazin-derivate, deren salze und pharmazeutische praeparate | |
DE1418569A1 (de) | Verfahren zur Herstellung von Carbamaten | |
DE1159937B (de) | Verfahren zur Herstellung von Hydrindensulfonylharnstoffen | |
CH480305A (de) | Verfahren zur Herstellung von schwefelhaltigen Aminen | |
DE1912770B2 (de) | 4-substituierte 1-phenyl-5-halogenpyridazon-(6)-derivate | |
DE1645906A1 (de) | Piperidinverbindungen und Verfahren zu ihrer Herstellung | |
DE1232161B (de) | Verfahren zur Herstellung von basisch substituierten Dibenzo-oxepinen und deren Salzen | |
DE1545555C3 (enrdf_load_stackoverflow) | ||
DE2825445A1 (de) | Rifamycin-verbindungen | |
DE844897C (de) | Verfahren zur Herstellung von Diamidinderivaten | |
DE896492C (de) | Verfahren zur Herstellung von 2-Halogenarylamino-4-amino-1, 3, 5-triazinderivaten | |
AT265259B (de) | Verfahren zur Herstellung von neuen rechtsdrehenden und linksdrehenden Formen von 1-(β-Hydroxy- oder -Halogen-äthyl)-diphenylmethyl-piperidinen und ihren Salzen | |
DE1445821A1 (de) | Verfahren zur Herstellung von Derivaten des Cesphalosporin C. | |
DE1643784C (de) | Biologisch wirksame Isothiocyanate und Verfahren zu deren Herstellung | |
DE1054777B (de) | Akarizide Mittel | |
DE1795511C3 (de) | 3-Amino-5-phenyl-7-chlor-2,3dihydro-1 H-1,4-benzodiazepinon-(2) | |
DE1298092B (de) | Arylthiocarbamate | |
AT220619B (de) | Verfahren zur Herstellung von Aminoalkylbenzhydryläthern | |
DE2313845C3 (de) | Thiocarbaminsäurederivate und diese enthaltende Arzneimittelzubereitungen | |
AT165069B (de) | Verfahren zur Herstellung neuer Phenoxyacetamidine | |
DE763489C (de) | Verfahren zur Herstellung von ª-Aminoaethylestern substituierter Phenylessigsaeuren | |
DE1470221A1 (de) | Piperidinomethylverbindungen und Verfahren zu ihrer Herstellung | |
DE870160C (de) | Verfahren zur Herstellung von Penicillin-Verbindungen | |
DE1239318B (de) | Verfahren zur Herstellung von basisch substituierten Dibenzo-oxepinen bzw. Dibenzo-thiepinen und deren Hydrohalogeniden | |
DE1695370A1 (de) | Verfahren zur Herstellung von Thioamiden |